CN103666562B - Unpowered circulation single still multiple reactor clorafin reaction unit - Google Patents
Unpowered circulation single still multiple reactor clorafin reaction unit Download PDFInfo
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- CN103666562B CN103666562B CN201310603865.2A CN201310603865A CN103666562B CN 103666562 B CN103666562 B CN 103666562B CN 201310603865 A CN201310603865 A CN 201310603865A CN 103666562 B CN103666562 B CN 103666562B
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- Prior art keywords
- reactor
- interchanger
- clorafin
- reaction unit
- reaction
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 24
- 238000005660 chlorination reaction Methods 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 239000000463 material Substances 0.000 abstract description 5
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 abstract description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052801 chlorine Inorganic materials 0.000 abstract description 3
- 239000000460 chlorine Substances 0.000 abstract description 3
- 238000009434 installation Methods 0.000 abstract description 3
- 239000012188 paraffin wax Substances 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 2
- 238000002309 gasification Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 abstract 1
- 238000007634 remodeling Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 4
- 239000011521 glass Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Unpowered circulation single still multiple reactor clorafin reaction unit, announcement be clorafin reaction unit, be specially a kind of single still multiple reactor clorafin reaction unit.Interchanger is provided with, in the bottom of upper interchanger with lower interchanger in the bottom of chlorinating container.Device is provided with four chlorination reactors side by side, the remodeling method of this device is that whiteruss material is sent into reactor from reactor, then chlorine is entered reactor body from reactor bottom, carry out blistering reaction, after compressed air handling, obtain paraffin wax product.But the operation scheme of apparatus of the present invention is that the pressure difference of gasification reaction formation after utilizing the thermopositive reaction performance of whiteruss and reactor bottom to pass into liquid chlorine is to realize the circulation of material.So namely, eliminate impeller pump.Not only make device structure be simplified, but also reduce the consumption of the energy, decrease operator and be equipped with, thus reduce the production cost of enterprise, solve existing installation Problems existing.
Description
Technical field
What the present invention announced is clorafin reaction unit, is specially a kind of single still multiple reactor clorafin reaction unit.
Background technology
The clorafin reaction unit used in production reality at present, be single still single reactor structure, namely a chlorinating container is for a reactor job.Artificial the expending of the energy will be increased like this, add the production cost of large enterprises.In addition, existing reaction unit arranges impeller pump in the bottom of reaction kettle body.Utilize the power of impeller pump to be forced to send into reactor by whiteruss material, then chlorine is passed into from reactor bottom, carry out blistering reaction.Obtain reaction solution after reaction terminates, then obtain clorafin product after compressed air handling.Due to impeller pump, not only make equipment become complex structure, in operation, controlling unit is many, but also adds energy consumption.Increase the production cost of enterprise.
Summary of the invention
For above-mentioned situation, the object of this invention is to provide a kind of unpowered circulation single still multiple reactor clorafin reaction unit, simplified apparatus, save the energy, solve existing installation Problems existing.
Technical scheme of the present invention is as follows;
The present invention is made up of chlorinating container, interchanger and chlorination reactor, is provided with interchanger in the bottom of chlorinating container, in the bottom of upper interchanger with lower interchanger.Upper and lower interchanger is connected in parallel by pipeline and chlorinating container.Device is provided with A chlorination reactor, B chlorination reactor, C chlorination reactor and D chlorination reactor side by side.The water inlet end of upper interchanger connects A chlorination reactor and B chlorination reactor respectively by pipeline.The water inlet end of lower interchanger connects C chlorination reactor and D chlorination reactor respectively by pipeline.Four reactors are connected with chlorinating container by pipeline.The production method of apparatus of the present invention is roughly the same with existing apparatus, is also whiteruss material is sent into reactor from reactor, then chlorine is entered reactor body from reactor bottom, carries out blistering reaction, obtains paraffin wax product after compressed air handling.But the operation scheme of apparatus of the present invention is that the pressure difference of gasification reaction formation after utilizing the thermopositive reaction performance of whiteruss and reactor bottom to pass into liquid chlorine is to realize the circulation of material.When raw material liq paraffin in the reaction, be positioned at reactor top for thermal response liquid, proportion is relatively light.Reaction solution through chuck cooling post-reactor bottom is cold reaction solution, and proportion is larger.Because cold and hot liquids proportion is different, hot liquid rises, and cold liquid supplements and forms a natural circulation simultaneously.Also have after reactor bottom passes into liquid chlorine, liquid chlorine vaporizing, forms certain pressure in system, reactor pressure is now large, reacting kettle inner pressure is little, utilizes this pressure difference, makes vasoliniment form natural circulation by pressure general goal to the little flowing of pressure.So namely, eliminate impeller pump.Not only make device structure be simplified, but also reduce the consumption of the energy, decrease operator and be equipped with, thus reduce the production cost of enterprise, solve existing installation Problems existing.
Accompanying drawing explanation
Accompanying drawing is structural representation of the present invention
Interchanger 4-A chlorination reactor 5-B chlorination reactor 6-C chlorination reactor 7-D chlorination reactor under interchanger 3-on 1-chlorinating container 2-
Embodiment
Below in conjunction with accompanying drawing, the invention will be further described, and the present invention is made up of chlorinating container, interchanger and chlorination reactor, is provided with interchanger 2 in the bottom of chlorinating container 1, in the bottom of upper interchanger with lower interchanger 3.Upper and lower interchanger is connected in parallel by pipeline and chlorinating container.Device is provided with A chlorination reactor 4, B chlorination reactor 5, C chlorination reactor 6 and D chlorination reactor 7 side by side.The water inlet end of upper interchanger connects A chlorination reactor 4 and B chlorination reactor 5 respectively by pipeline.The water inlet end of lower interchanger connects C chlorination reactor 6 and D chlorination reactor 7 respectively by pipeline.Four reactors are connected with chlorinating container by pipeline.Chlorination tank is lass lining manufacture, and volume is 2000L.Interchanger is glass manufacture specification is 3 cubic metres.Chlorination reactor is glass manufacture, and specification is 3.5m × φ 280mm.
Claims (1)
1. unpowered circulation single still multiple reactor clorafin reaction unit, by chlorinating container, interchanger and chlorination reactor are formed, it is characterized in that: be provided with upper interchanger (2) in the bottom of chlorinating container (1), in the bottom of upper interchanger with lower interchanger (3), on, lower interchanger is connected in parallel by pipeline and chlorinating container, device is provided with A chlorination reactor (4) side by side, B chlorination reactor (5), C chlorination reactor (6) and D chlorination reactor (7), four reactors are connected with chlorinating container by pipeline, the water inlet end of upper interchanger connects A chlorination reactor (4) and B chlorination reactor (5) respectively by pipeline, the water inlet end of lower interchanger connects C chlorination reactor (6) and D chlorination reactor (7) respectively by pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310603865.2A CN103666562B (en) | 2013-11-13 | 2013-11-13 | Unpowered circulation single still multiple reactor clorafin reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310603865.2A CN103666562B (en) | 2013-11-13 | 2013-11-13 | Unpowered circulation single still multiple reactor clorafin reaction unit |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103666562A CN103666562A (en) | 2014-03-26 |
| CN103666562B true CN103666562B (en) | 2015-11-25 |
Family
ID=50305345
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310603865.2A Active CN103666562B (en) | 2013-11-13 | 2013-11-13 | Unpowered circulation single still multiple reactor clorafin reaction unit |
Country Status (1)
| Country | Link |
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| CN (1) | CN103666562B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB815454A (en) * | 1956-11-05 | 1959-06-24 | Diamond Alkali Co | Improvements in or relating to chlorinated paraffins |
| CN2455720Y (en) * | 2000-11-29 | 2001-10-24 | 王宏力 | Chlorinated paraffin producing apparatus with external circulation heat exchanger |
| CN1424381A (en) * | 2002-12-18 | 2003-06-18 | 宁波市镇海众利化工有限公司 | Devices for continuously producing chlorinated paraffin |
-
2013
- 2013-11-13 CN CN201310603865.2A patent/CN103666562B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB815454A (en) * | 1956-11-05 | 1959-06-24 | Diamond Alkali Co | Improvements in or relating to chlorinated paraffins |
| CN2455720Y (en) * | 2000-11-29 | 2001-10-24 | 王宏力 | Chlorinated paraffin producing apparatus with external circulation heat exchanger |
| CN1424381A (en) * | 2002-12-18 | 2003-06-18 | 宁波市镇海众利化工有限公司 | Devices for continuously producing chlorinated paraffin |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103666562A (en) | 2014-03-26 |
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Effective date of registration: 20160819 Address after: 115000 Liaoning city of Yingkou Province coastal industrial base, East New Street Management Committee Patentee after: Yingkou Tanyun Chemicals Research Institute Corp. Address before: 115000 Liaoning Province, Yingkou City Station District Yijing international No. seven 1-8-15 Patentee before: Lv Debin |
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| CP01 | Change in the name or title of a patent holder | ||
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Address after: 115000 East 1 Xinlian Street, Yingkou Coastal Industrial Base Management Committee, Liaoning Province Patentee after: Tianyuan Junrong (Liaoning) Chemical Research Institute New Material Incubator Co., Ltd. Address before: 115000 East 1 Xinlian Street, Yingkou Coastal Industrial Base Management Committee, Liaoning Province Patentee before: Yingkou Tanyun Chemicals Research Institute Corp. |
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| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 115000 East 1 Xinlian Street, Yingkou Coastal Industrial Base Management Committee, Liaoning Province Patentee after: Tianyuan aviation materials (Yingkou) Technology Co.,Ltd. Address before: 115000 East 1 Xinlian Street, Yingkou Coastal Industrial Base Management Committee, Liaoning Province Patentee before: TIANYUAN JUNRONG (LIAONING) CHEMICAL RESEARCH INSTITUTE NEW MATERIAL INCUBATOR Co.,Ltd. |