CN103386286A - Recyclable reaction vessel system - Google Patents
Recyclable reaction vessel system Download PDFInfo
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- CN103386286A CN103386286A CN2013102762645A CN201310276264A CN103386286A CN 103386286 A CN103386286 A CN 103386286A CN 2013102762645 A CN2013102762645 A CN 2013102762645A CN 201310276264 A CN201310276264 A CN 201310276264A CN 103386286 A CN103386286 A CN 103386286A
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Abstract
The invention belongs to the field of industrial chemical production equipment, and specifically relates to a reaction-vessel condensation-reaction circulation system used in industrial chemical production reactions. The recyclable reaction vessel system comprises a reaction vessel and a condensation circulation apparatus connected with the reaction vessel, and the condensation circulation apparatus comprises a buffer tank and a condensation glass tank which are both connected with the reaction vessel and are connected with each other. The recyclable reaction vessel system of the invention helps to realize that a gaseous material in the reaction vessel enters into the buffer tank, successively enters into the condensation glass tank from the buffer tank, and is liquefied in the condensation glass tank or reflows into the reaction vessel for a reaction, and helps to realize circulation of forward flow, condensation and backflow of the material in the circulation reaction vessel system.
Description
Technical field
The invention belongs to industrial chemical production equipment field, relate in particular the reactor condensation reaction circulatory system of using in a kind of Chemical Manufacture reaction.
Technical background
In the reactor of Chemical Manufacture, often need to reaction or gaseous feed after condensation liquefaction through reactor reaction, in the prior art, this class reaction cycle device all can not be well with gas liquefaction, circulation can not be well realized, the cleaning of condenser and the recovery of waste material can not be realized.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of a kind of reactor system of gaseous liquefied and reflux cycle reaction that can realization response.
For solving the problems of the technologies described above, the invention provides a kind of reactor system capable of circulation, comprise reactor and the condensation circulating device that is connected with reactor, condensation circulating device comprises surge tank and the anti-condensation glass tank that is connected with reactor, is connected between surge tank and anti-condensation glass tank.
Preferably, the surge tank position is higher than the anti-condensation glass tank, and anti-condensation glass tank position is higher than reactor.
Preferably, be provided with pump between reactor and surge tank.
Preferably, the surge tank top is connected with the anti-condensation glass tank top by pipeline one.
Preferably, set up pipeline two on pipeline one separately, pipeline two is connected with return water pipe.
Preferably, the anti-condensation glass pot bottom is connected with the reactor top by glass tube one.
Preferably, set up glass tube two on glass tube one separately, glass tube two is connected with return water pipe.
Preferably, the anti-condensation glass pot bottom also is provided with the pipeline three that is connected with air duct.
adopt the beneficial effect of technique scheme to be: a kind of reactor system capable of circulation, comprise reactor and the condensation circulating device that is connected with reactor, condensation circulating device comprises surge tank and the anti-condensation glass tank that is connected with reactor, be connected between surge tank and anti-condensation glass tank, adopt this connected mode, can enter surge tank by the interior gaseous material of realization response still, entering into the anti-condensation glass tank from surge tank, liquefy in the anti-condensation glass tank or be back in reactor, react, realize the drag flow of material in circular response still system, the circulation of condensation and backflow, the surge tank position is higher than the anti-condensation glass tank, anti-condensation glass tank position is higher than reactor, with reactor, surge tank and anti-condensation glass tank adopt the installation of this position relationship, be convenient to the circulation of material, be provided with pump between reactor and surge tank, utilize pump that the gaseous state material in reactor is pumped into surge tank, the surge tank top is connected with the anti-condensation glass tank top by pipeline one, make the material of gaseous state enter from the anti-condensation glass tank top, make and have enough cooling liquid processes, make gas material fully to liquefy, set up pipeline two on pipeline one separately, described pipeline two is connected with return water pipe, be convenient to reclaim the waste water of the steam liquefied in the anti-condensation glass tank, the anti-condensation glass pot bottom is connected with the reactor top by glass tube one, adopt glass tube one, the glass main component is quartzy, comparatively stable, material reaction after being not easy to liquefy, set up glass tube two on glass tube one separately, described glass tube two is connected with return water pipe, be convenient to reclaim the waste water after liquefaction, the anti-condensation glass pot bottom also is provided with the pipeline three that is connected with air duct, can guarantee the pressure balance that the anti-condensation glass tank is inside and outside after making whole system quit work.
Description of drawings
Fig. 1 is the structural representation of a kind of reactor system capable of circulation of the present invention,
Wherein, 1, reactor, 2, glass tube two, 3, return water pipe, 4, pump, 5, pipeline two, 6, pipeline one, 7, surge tank, 9, the anti-condensation glass tank, 10, pipeline three, 11, air duct, 12, glass tube one.
The specific embodiment
Below in conjunction with Figure of description, technical scheme of the present invention and structure are described, so that those skilled in the art understand.
as shown in Figure 1, a kind of reactor system capable of circulation, comprise reactor 1 and the condensation circulating device that is connected with reactor 1, condensation circulating device comprises surge tank 7 and the anti-condensation glass tank 9 that is connected with reactor 1, surge tank 7 is connected with 9, anti-condensation glass tank, surge tank 7 positions are higher than anti-condensation glass tank 9, anti-condensation glass tank 9 positions are higher than reactor 1, 7 of reactor 1 and surge tanks are provided with pump 4, surge tank 7 tops are connected with anti-condensation glass tank 9 tops by pipeline 1, set up pipeline 25 on pipeline 1 separately, pipeline 25 is connected with return water pipe 3, anti-condensation glass tank 9 bottoms are connected with reactor 1 top by glass tube 1, set up glass tube 22 on glass tube 1 separately, glass tube 22 is connected with return water pipe 3, anti-condensation glass tank 9 bottoms also are provided with the pipeline 3 10 that is connected with air duct 11.
adopt the beneficial effect of technique scheme to be: a kind of reactor system capable of circulation, comprise reactor and the condensation circulating device that is connected with reactor, condensation circulating device comprises surge tank and the anti-condensation glass tank that is connected with reactor, be connected between surge tank and anti-condensation glass tank, adopt this connected mode, can enter surge tank by the interior gaseous material of realization response still, entering into the anti-condensation glass tank from surge tank, liquefy in the anti-condensation glass tank or be back in reactor, react, realize the drag flow of material in circular response still system, the circulation of condensation and backflow, the surge tank position is higher than the anti-condensation glass tank, anti-condensation glass tank position is higher than reactor, with reactor, surge tank and anti-condensation glass tank adopt the installation of this position relationship, be convenient to the circulation of material, be provided with pump between reactor and surge tank, utilize pump that the gaseous state material in reactor is pumped into surge tank, the surge tank top is connected with the anti-condensation glass tank top by pipeline one, make the material of gaseous state enter from the anti-condensation glass tank top, make and have enough cooling liquid processes, make gas material fully to liquefy, set up pipeline two on pipeline one separately, described pipeline two is connected with return water pipe, be convenient to reclaim the waste water of the steam liquefied in the anti-condensation glass tank, the anti-condensation glass pot bottom is connected with the reactor top by glass tube one, adopt glass tube one, the glass main component is quartzy, comparatively stable, material reaction after being not easy to liquefy, set up glass tube two on glass tube one separately, described glass tube two is connected with return water pipe, be convenient to reclaim the waste water after liquefaction, the anti-condensation glass pot bottom also is provided with the pipeline three that is connected with air duct, can guarantee the pressure balance that the anti-condensation glass tank is inside and outside after making whole system quit work.
Adopt the reactor system a kind of capable of circulation of technical solution of the present invention, can enter surge tank by the interior gaseous material of realization response still, entering into the anti-condensation glass tank from surge tank, liquefy in the anti-condensation glass tank or be back in reactor, react, realize the circulation of drag flow, condensation and the backflow of material in circular response still system.
Above-mentionedly by reference to the accompanying drawings invention is exemplarily described; obviously specific implementation of the present invention is not subject to the restrictions described above; as long as this non-essential improvement that has adopted method design of the present invention and technical scheme to carry out; or without improving the design that will invent and technical scheme, directly apply to other occasions, all within protection scope of the present invention.
Claims (8)
1. reactor system capable of circulation, comprise reactor and the condensation circulating device that is connected with reactor, and it is characterized in that: described condensation circulating device comprises surge tank and the anti-condensation glass tank that is connected with reactor, is connected between described surge tank and anti-condensation glass tank.
2. a kind of reactor system capable of circulation according to claim 1, it is characterized in that: described surge tank position is higher than the anti-condensation glass tank, and described anti-condensation glass tank position is higher than reactor.
3. a kind of reactor system capable of circulation according to claim 2, is characterized in that: be provided with pump between described reactor and surge tank.
4. a kind of reactor system capable of circulation according to claim 2 is characterized in that: described surge tank top is connected with the anti-condensation glass tank top by pipeline one.
5. a kind of reactor system capable of circulation according to claim 4, it is characterized in that: set up pipeline two separately on described pipeline one, described pipeline two is connected with return water pipe.
6. a kind of reactor system capable of circulation according to claim 4 is characterized in that: described anti-condensation glass pot bottom is connected with the reactor top by glass tube one.
7. a kind of reactor system capable of circulation according to claim 6, it is characterized in that: set up glass tube two separately on described glass tube one, described glass tube two is connected with return water pipe.
8. a kind of reactor system capable of circulation according to claim 6, it is characterized in that: described anti-condensation glass pot bottom also is provided with the pipeline three that is connected with air duct.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310276264.5A CN103386286B (en) | 2013-07-01 | 2013-07-01 | Recyclable reaction vessel system |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310276264.5A CN103386286B (en) | 2013-07-01 | 2013-07-01 | Recyclable reaction vessel system |
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| CN103386286A true CN103386286A (en) | 2013-11-13 |
| CN103386286B CN103386286B (en) | 2015-04-01 |
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| CN201310276264.5A Active CN103386286B (en) | 2013-07-01 | 2013-07-01 | Recyclable reaction vessel system |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106552554A (en) * | 2015-09-30 | 2017-04-05 | 江苏创新石化有限公司 | A kind of amine liquid recovery system of compounding neutralization corrosion inhibiter |
| CN110818579A (en) * | 2018-08-08 | 2020-02-21 | 青岛海湾精细化工有限公司 | Cooling crystallization method and device for N-acetoacetanilide compound |
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| CN201610417U (en) * | 2009-12-25 | 2010-10-20 | 潍坊中业油脂有限公司 | Chlorination reaction device for chloroactic acid production |
| CN102489233A (en) * | 2011-12-16 | 2012-06-13 | 中国石油化工股份有限公司 | Novel production equipment of propionic acid peroxide as well as safety protection method and application thereof |
| CN202398358U (en) * | 2011-12-20 | 2012-08-29 | 迈克斯(如东)化工有限公司 | Terbacil material punching prevention system |
| CN203525678U (en) * | 2013-07-01 | 2014-04-09 | 安徽省旌德县天益医药化工厂 | Circulatory reaction kettle system |
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2013
- 2013-07-01 CN CN201310276264.5A patent/CN103386286B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2002161071A (en) * | 2000-11-28 | 2002-06-04 | Nippon Shokubai Co Ltd | Method for producing dehydration reaction product and dehydration reaction device used therefor |
| CN201610417U (en) * | 2009-12-25 | 2010-10-20 | 潍坊中业油脂有限公司 | Chlorination reaction device for chloroactic acid production |
| CN102489233A (en) * | 2011-12-16 | 2012-06-13 | 中国石油化工股份有限公司 | Novel production equipment of propionic acid peroxide as well as safety protection method and application thereof |
| CN202398358U (en) * | 2011-12-20 | 2012-08-29 | 迈克斯(如东)化工有限公司 | Terbacil material punching prevention system |
| CN203525678U (en) * | 2013-07-01 | 2014-04-09 | 安徽省旌德县天益医药化工厂 | Circulatory reaction kettle system |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106552554A (en) * | 2015-09-30 | 2017-04-05 | 江苏创新石化有限公司 | A kind of amine liquid recovery system of compounding neutralization corrosion inhibiter |
| CN110818579A (en) * | 2018-08-08 | 2020-02-21 | 青岛海湾精细化工有限公司 | Cooling crystallization method and device for N-acetoacetanilide compound |
| CN110818579B (en) * | 2018-08-08 | 2022-09-16 | 青岛海湾精细化工有限公司 | Cooling crystallization method and device for N-acetoacetanilide compound |
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| CN103386286B (en) | 2015-04-01 |
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Effective date of registration: 20180611 Address after: 043100 Shanxi Xinjiang County Coal Chemical Industrial Park, Yuncheng (Shanxi Heng Qiang Chemical Co., Ltd.) Patentee after: Shanxi Kai Li Fine Chemicals Technology Co., Ltd. Address before: 242000 Guanyin Pavilion, Jingyang Town, Jingde County, Xuancheng, Anhui, China Patentee before: Anhui Province Shengde County Tianyi Pharmaceutical Chemical Factory |