CN103642549B - A kind of clean biometric diesel oil and preparation method thereof - Google Patents
A kind of clean biometric diesel oil and preparation method thereof Download PDFInfo
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- CN103642549B CN103642549B CN201310575275.3A CN201310575275A CN103642549B CN 103642549 B CN103642549 B CN 103642549B CN 201310575275 A CN201310575275 A CN 201310575275A CN 103642549 B CN103642549 B CN 103642549B
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- 239000002283 diesel fuel Substances 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000000654 additive Substances 0.000 claims abstract description 27
- 230000000996 additive effect Effects 0.000 claims abstract description 27
- 239000012075 bio-oil Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 36
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 30
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 17
- 239000003549 soybean oil Substances 0.000 claims description 13
- 235000012424 soybean oil Nutrition 0.000 claims description 13
- ZEMPKEQAKRGZGQ-AAKVHIHISA-N 2,3-bis[[(z)-12-hydroxyoctadec-9-enoyl]oxy]propyl (z)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCCC(O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(O)CCCCCC)COC(=O)CCCCCCC\C=C/CC(O)CCCCCC ZEMPKEQAKRGZGQ-AAKVHIHISA-N 0.000 claims description 12
- 235000019483 Peanut oil Nutrition 0.000 claims description 12
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 12
- 239000000312 peanut oil Substances 0.000 claims description 12
- GEYOCULIXLDCMW-UHFFFAOYSA-N 1,2-phenylenediamine Chemical compound NC1=CC=CC=C1N GEYOCULIXLDCMW-UHFFFAOYSA-N 0.000 claims description 10
- 229910002651 NO3 Inorganic materials 0.000 claims description 10
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 10
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 10
- 150000002148 esters Chemical class 0.000 claims description 10
- 239000000194 fatty acid Substances 0.000 claims description 10
- 229930195729 fatty acid Natural products 0.000 claims description 10
- 150000004665 fatty acids Chemical class 0.000 claims description 10
- -1 isooctyl Chemical group 0.000 claims description 10
- 150000003014 phosphoric acid esters Chemical class 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 239000002551 biofuel Substances 0.000 abstract description 10
- 239000002994 raw material Substances 0.000 abstract description 8
- 239000000446 fuel Substances 0.000 abstract description 6
- 239000003225 biodiesel Substances 0.000 abstract description 3
- 230000032258 transport Effects 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 description 6
- 238000002485 combustion reaction Methods 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000002803 fossil fuel Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Abstract
The present invention relates to technical field prepared by fuel biodiesel, be specifically related to a kind of clean biometric diesel oil and preparation method thereof.It consists of following component by weight: bio oil 20-30 part, short chain alcohol 5-20 part, diesel oil 30-40 part, additive 5-8 part, water 2-40 part.Each index of this biofuel is all significantly better than GB, and overall performance is superior, and preparation technology is simple, and raw material sources are extensive, and cost is low, economical and practical, transports and stores safer.
Description
Technical field
The present invention relates to technical field prepared by fuel biodiesel, be specifically related to a kind of clean biometric diesel oil and preparation method thereof.
Background technology
At present, along with the quick growth of economy and the raising day by day of living standards of the people, the environmental consciousness of people constantly strengthens, and the research of the clean biometric energy has caused to be paid close attention to widely.Biofuel is a kind of green recyclable fuel containing oxygen, substantially not sulfur-bearing and aromatic hydrocarbon.It is a kind of oil fuel of improvement, and primarily of carbon hydrogen element composition, after burning, expellant gas objectionable constituent are little, are the clean biometric fuel of alternative petrifaction diesel.
Compared with traditional fossil fuel, biofuel has unique advantage, is mainly reflected in the following aspects: one is nontoxic easy decomposition, good environmental protection; Two is that biofuel oxygen level is high, and combustion processes oxygen requirement is few, and its burning, ignition characteristic are better than petrifaction diesel; Three is that biofuel cetane value is higher, and the capability of antidetonance is better than petrifaction diesel; Four is that its flash-point is higher, is conducive to transporting safely.These advantages make biofuel become the focus of Recent study, greatly develop biofuel significant, but it are scarcely out of swaddling-clothes, and also have many problem demanding prompt solutions, therefore, a kind of high-quality clean biometric diesel oil is extremely urgent.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of clean biometric diesel oil, its method is simple, and cost is low, and prepared diesel combustion efficiency is high, clean environment firendly.
Technical scheme of the present invention:
A kind of clean biometric diesel oil, it consists of following component by weight: bio oil 20-30 part, short chain alcohol 5-20 part, diesel oil 30-40 part, additive 5-8 part, water 2-40 part.
As preferably, described bio oil is: one or more in Viscotrol C, rapeseed oil, peanut oil, soybean oil; Further preferably, described bio oil is the mixture of Viscotrol C, rapeseed oil, peanut oil, soybean oil, and wherein, the weight percentage of each component is Viscotrol C 25%, rapeseed oil 25%, peanut oil 25%, soybean oil 25%.
As preferably, described short chain alcohol is the mixture of methyl alcohol and ethanol, and wherein the weight percentage of each component is methyl alcohol 40%, ethanol 60%.
As preferably, described additive is made up of following component by weight percentage: dialkyl diphenylamine 5-10%, longer chain fatty acid 5-20%, phosphoric acid ester 5-15%, O-Phenylene Diamine 5-20%, isooctyl ester nitrate 2-4%, toluene 31-78%, by obtained for above-mentioned raw materials mixing additive.
A preparation method for clean biometric diesel oil, concrete steps are as follows: take each material according to following proportioning, are sequentially added in reactor, start agitator, and stir 20-30min, make it fully mix, filtration gets product; Described proportioning is: bio oil 20-30 part, short chain alcohol 5-20 part, diesel oil 30-40 part, additive 5-8 part, water 2-40 part; Described bio oil is the mixture of Viscotrol C, rapeseed oil, peanut oil, soybean oil, and wherein, the weight percentage of each component is Viscotrol C 25%, rapeseed oil 25%, peanut oil 25%, soybean oil 25%; Described short chain alcohol is the mixture of methyl alcohol and ethanol, and wherein the weight percentage of each component is methyl alcohol 40%, ethanol 60%; Described additive is mixed by following component by weight percentage and forms: dialkyl diphenylamine 5-10%, longer chain fatty acid 5-20%, phosphoric acid ester 5-15%, O-Phenylene Diamine 5-20%, isooctyl ester nitrate 2-4%, toluene 31-78%.
Beneficial effect of the present invention is:
The applicant is by large quantifier elimination, provide a kind of formula of biodiesel of ratio optimization, by rational proportion and the interaction of each component, serve the effect coordinating synergy, make the biofuel efficiency of combustion that obtains high, sufficient combustion is nontoxic, free from environmental pollution, be alternative clean biometric fuel, each index of this biofuel is all significantly better than GB.When the weight percentage of component each in bio oil is Viscotrol C 25%, rapeseed oil 25%, peanut oil 25%, soybean oil 25%, the overall performance of performance is more excellent, and this is also the result that each component coordinates synergy.
In a word, clean biometric diesel oil of the present invention, overall performance is superior, and preparation technology is simple, and raw material sources are extensive, and cost is low, economical and practical, transports and stores safer.
the index of the biofuel that the present invention obtains is as shown in table 1.
Table 1 performance index
embodiment:
In order to understand technical scheme of the present invention better, be described in detail further below by way of specific embodiment.
embodiment 1
A kind of clean biometric diesel oil, take soybean oil 25 parts, methyl alcohol 10 parts, diesel oil 30 parts, additive 5 parts, 30 parts, water, adds in reactor successively, stirs 25min, makes it fully mix, filter to obtain refined biometric diesel oil.
Wherein, additive is dialkyl diphenylamine 5%, longer chain fatty acid 5%, phosphoric acid ester 5%, O-Phenylene Diamine 5%, isooctyl ester nitrate 2%, toluene 78%.
The index of the refined biometric diesel oil obtained is as shown in table 2.
Table 2 performance index
embodiment 2
A kind of clean biometric diesel oil, take Viscotrol C 20 parts, ethanol 10 parts, diesel oil 35 parts, additive 6 parts, 29 parts, water, adds in reactor successively, stirs 20min, makes it fully mix, filter to obtain refined biometric diesel oil.
Wherein, additive is dialkyl diphenylamine 10%, longer chain fatty acid 10%, phosphoric acid ester 15%, O-Phenylene Diamine 11%, isooctyl ester nitrate 4%, toluene 50%, by obtained for above-mentioned raw materials mixing additive.
The index of the refined biometric diesel oil obtained is as shown in table 3.
Table 3 performance index
embodiment 3
A kind of clean biometric diesel oil, take rapeseed oil 30 parts, methyl alcohol 15 parts, diesel oil 30 parts, additive 5 parts, 20 parts, water, adds in reactor successively, stirs 25min, makes it fully mix, filter to obtain refined biometric diesel oil.
Wherein, additive is dialkyl diphenylamine 10%, longer chain fatty acid 20%, phosphoric acid ester 15%, O-Phenylene Diamine 20%, isooctyl ester nitrate 4%, toluene 31%, by obtained for above-mentioned raw materials mixing additive.
The index of the refined biometric diesel oil obtained is as shown in table 4.
Table 4 performance index
embodiment 4
A kind of clean biometric diesel oil, take peanut oil 25 parts, methyl alcohol 20 parts, diesel oil 40 parts, additive 7 parts, 8 parts, water, adds in reactor successively, stirs 30min, makes it fully mix, filter to obtain refined biometric diesel oil.
Wherein, additive is dialkyl diphenylamine 7%, longer chain fatty acid 15%, phosphoric acid ester 10%, O-Phenylene Diamine 12%, isooctyl ester nitrate 3%, toluene 53%, by obtained for above-mentioned raw materials mixing additive.
The index of the refined biometric diesel oil obtained is as shown in table 5.
Table 5 performance index
embodiment 5
A kind of clean biometric diesel oil, take bio oil 20 parts, ethanol 10 parts, methyl alcohol 5 parts, diesel oil 35 parts, additive 5 parts, 25 parts, water, adds in reactor successively, stirs 20min, makes it fully mix, filter to obtain refined biometric diesel oil.
Described bio oil is Viscotrol C 25%, rapeseed oil 25%, peanut oil 25%, soybean oil 25%.
Wherein, additive is dialkyl diphenylamine 8%, longer chain fatty acid 17%, phosphoric acid ester 8%, O-Phenylene Diamine 10%, isooctyl ester nitrate 3%, toluene 54%, by obtained for above-mentioned raw materials mixing additive.
The index of the refined biometric diesel oil obtained is as shown in table 6.
Table 6 performance index
embodiment 6
A kind of clean biometric diesel oil, take soybean oil 20 parts, ethanol 15 parts, diesel oil 40 parts, additive 8 parts, 19 parts, water, adds in reactor successively, stirs 30min, makes it fully mix, filter to obtain refined biometric diesel oil.
Wherein, additive is dialkyl diphenylamine 5%, longer chain fatty acid 8%, phosphoric acid ester 10%, O-Phenylene Diamine 7%, isooctyl ester nitrate 4%, toluene 66%, by obtained for above-mentioned raw materials mixing additive.
The index of the refined biometric diesel oil obtained is as shown in table 7.
Table 7 performance index
。
Claims (2)
1. a clean biometric diesel oil, it consists of following component by weight: bio oil 20-30 part, short chain alcohol 5-20 part, diesel oil 30-40 part, additive 5-8 part, water 2-40 part; Described bio oil is the mixture of Viscotrol C, rapeseed oil, peanut oil, soybean oil, and wherein, the weight percentage of each component is Viscotrol C 25%, rapeseed oil 25%, peanut oil 25%, soybean oil 25%; Described short chain alcohol is the mixture of methyl alcohol and ethanol, and wherein the weight percentage of each component is methyl alcohol 40%, ethanol 60%; Described additive is mixed by following component by weight percentage and forms: dialkyl diphenylamine 5-10%, longer chain fatty acid 5-20%, phosphoric acid ester 5-15%, O-Phenylene Diamine 5-20%, isooctyl ester nitrate 2-4%, toluene 31-78%.
2. the preparation method of a kind of clean biometric diesel oil as claimed in claim 1, concrete steps are as follows: take each material according to following proportioning, are sequentially added in reactor, start agitator, and stir 20-30min, make it fully mix, filtration gets product; Described proportioning is: bio oil 20-30 part, short chain alcohol 5-20 part, diesel oil 30-40 part, additive 5-8 part, water 2-40 part; Described bio oil is the mixture of Viscotrol C, rapeseed oil, peanut oil, soybean oil, and wherein, the weight percentage of each component is Viscotrol C 25%, rapeseed oil 25%, peanut oil 25%, soybean oil 25%; Described short chain alcohol is the mixture of methyl alcohol and ethanol, and wherein the weight percentage of each component is methyl alcohol 40%, ethanol 60%; Described additive is mixed by following component by weight percentage and forms: dialkyl diphenylamine 5-10%, longer chain fatty acid 5-20%, phosphoric acid ester 5-15%, O-Phenylene Diamine 5-20%, isooctyl ester nitrate 2-4%, toluene 31-78%.
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| CN201310575275.3A CN103642549B (en) | 2013-11-18 | 2013-11-18 | A kind of clean biometric diesel oil and preparation method thereof |
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| CN201310575275.3A CN103642549B (en) | 2013-11-18 | 2013-11-18 | A kind of clean biometric diesel oil and preparation method thereof |
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| CN103642549B true CN103642549B (en) | 2015-09-23 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107880958A (en) * | 2017-11-24 | 2018-04-06 | 广西丰泰能源科技有限公司 | One kind emulsification biodiesel |
| CN107964429A (en) * | 2017-11-24 | 2018-04-27 | 广西丰泰能源科技有限公司 | A kind of clean biometric diesel oil |
| CN109294638A (en) * | 2018-10-10 | 2019-02-01 | 浙江佑驰能源科技有限公司 | Diesel engine vent gas clean synergistic agent and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1958745A (en) * | 2006-10-09 | 2007-05-09 | 陈志红 | Environmental protective diesel oil, and preparation method |
| CN102585937A (en) * | 2012-02-03 | 2012-07-18 | 临沂实能德环保燃料化工有限责任公司 | Compound additive applied in biodiesel |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1958745A (en) * | 2006-10-09 | 2007-05-09 | 陈志红 | Environmental protective diesel oil, and preparation method |
| CN102585937A (en) * | 2012-02-03 | 2012-07-18 | 临沂实能德环保燃料化工有限责任公司 | Compound additive applied in biodiesel |
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