CN103642370B - A kind of iron oxide black automobile chassis antirust paint and preparation method thereof - Google Patents
A kind of iron oxide black automobile chassis antirust paint and preparation method thereof Download PDFInfo
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- CN103642370B CN103642370B CN201310413143.0A CN201310413143A CN103642370B CN 103642370 B CN103642370 B CN 103642370B CN 201310413143 A CN201310413143 A CN 201310413143A CN 103642370 B CN103642370 B CN 103642370B
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Abstract
The invention provides a kind of iron oxide black automobile chassis antirust paint, it is prepared from by the raw material components of following weight portion: unsaturated polyester resin 55-60, diethylenetriamine 6-8, iron oxide black 15-18, silica flour 12-15, Kaolin 5-8, boron carbide 4-5, chlorinated polyethylene 5-8, quartz sand 8-10, vinyl three ('beta '-methoxy ethyoxyl) silane 3-5, methyl ethyl ketone peroxide 10-12, dimethylbenzene 32-35, film-forming resin 3-4.Advantages of nontoxic raw materials of the present invention, and environmental friendliness, therefore produce and human body is poisoned little by use process, and environmental pollution is low；Formula adds film-forming resin, improves the compatibility of each composition, substantially increase film-formation result.The paint film of gained is water-fast, antiseptic property is excellent, and adhesive strength is firm, alkaline-resisting, resistance to water is the most excellent.
Description
Technical field
The present invention relates to metal rust preventing technical field, be specifically related to a kind of iron oxide black automobile chassis antirust paint and
Preparation method.
Background technology
Metal erosion is the extremely serious problem that people face.The whole world is scrapped because of metal erosion every year
Metal reach more than several hundred million tons, economic loss accounts for the 1.5%～2.5% of total value of production in national economy.Metal rusting is
A kind of corrosion that the most universal, loss is maximum.Antirust work is always one of great scientific research task both domestic and external, people
Work out the corrosion that many kinds of measures prevents and suppresses metal, with coating antirust be a kind of effective method.
Summary of the invention
It is an object of the invention to provide a kind of iron oxide black automobile chassis antirust paint and preparation method thereof, to multiple gold
Accessory has antirust function.
Technical scheme is as follows:
A kind of iron oxide black automobile chassis antirust paint, it is characterised in that it is by the raw material components system of following weight portion
For forming:
Unsaturated polyester resin 55-60, diethylenetriamine 6-8, iron oxide black 15-18, silica flour 12-15, height
Ridge soil 5-8, boron carbide 4-5, chlorinated polyethylene 5-8, quartz sand 8-10, vinyl three ('beta '-methoxy ethoxy
Base) silane 3-5, methyl ethyl ketone peroxide 10-12, dimethylbenzene 32-35, film-forming resin 3-4.
Described iron oxide black automobile chassis antirust paint, it is characterised in that: described film-forming resin is by following weight
The raw material of part is prepared from:
Alcohol ester 12 15-18, methyl ethyl ketone peroxide 1-2, silane resin acceptor kh-550 1-1.3, acrylic acid-2-hydroxyl
Base propyl ester 2-3, schmigel 1-1.4, tea polyphenols 1-2, polyisobutylene 1-1.4, ethyl acetate 12-14, Ilicis Purpureae
Oil 1-2；
Preparation method is by 2-hydroxypropyl acrylate, schmigel, tea polyphenols, polyisobutylene, ethyl acetate
Mixing, adds methyl ethyl ketone peroxide, stirring reaction 45-60 minute, then, is warming up to 70-80 DEG C, adds silicon
Alkane coupling agent KH550, alcohol ester 12, continue stirring reaction 60-90 minute, then, add other residual components,
Stir 30-40 minute, with 500 mesh filter-cloth filterings and get final product.
The preparation method of described iron oxide black automobile chassis antirust paint, it is characterised in that comprise the following steps:
(1) first methyl ethyl ketone peroxide and part dimethylbenzene are joined reactor mix homogeneously；
(2) unsaturated polyester resin, diethylenetriamine are then sequentially added, boron carbide, chlorinated polyethylene, stone
Sand, controls temperature and is 45-50 DEG C, first stirs 8-10 minute with the speed of 300-500r/min, the most again
Stir 20-25 minute with the speed of 600-800r/min, then the rest materials in formula is all joined still
In, with speed high speed dispersion 20-25 minute of 1200-1500r/min, then by scattered mixed material
Put into and grind in sand mill, then filter with 400 mesh filter cloths,.
Beneficial effects of the present invention:
Advantages of nontoxic raw materials of the present invention, and environmental friendliness, therefore produce and human body is poisoned little by use process, and to ring
Environment pollution is low, adds film-forming resin, improve the compatibility of each composition, substantially increase film-formation result in formula.
The paint film of gained is water-fast, antiseptic property is excellent, and adhesive strength is firm, alkaline-resisting, resistance to water is the most excellent.
Detailed description of the invention:
Embodiment
A kind of iron oxide black automobile chassis antirust paint, it is prepared from by the raw material components of following weight (kg):
Unsaturated polyester resin 58, diethylenetriamine 6, iron oxide black 17, silica flour 14, Kaolin 6, carbon
Change boron 4, chlorinated polyethylene 7, quartz sand 9, vinyl three ('beta '-methoxy ethyoxyl) silane 4, peroxidating
Butanone 11, dimethylbenzene 34, film-forming resin 3；
Concrete preparation method, comprises the following steps:
1, the preparation of film-forming resin:
By weight (kg) weigh alcohol ester 12, methyl ethyl ketone peroxide 2, silane resin acceptor kh-550 2, third
Olefin(e) acid-2-hydroxy propyl ester 3, schmigel 1.4, tea polyphenols 1.2, polyisobutylene 1.4, ethyl acetate 12, Ilicis Purpureae
Oil 1.5；
Preparation method: by 2-hydroxypropyl acrylate, schmigel, tea polyphenols, polyisobutylene, ethyl acetate
Mixing, adds methyl ethyl ketone peroxide, stirring reaction 55 minutes, then, is warming up to 70 DEG C, adds silane coupled
Agent KH550, alcohol ester 12, continue stirring reaction 80 minutes, then, add other residual components, stir 35
Minute, with 500 mesh filter-cloth filterings and get final product.
2, the preparation of iron oxide black automobile chassis antirust paint, makes according to the following steps:
(1) first methyl ethyl ketone peroxide and part dimethylbenzene are joined reactor mix homogeneously；
(2) unsaturated polyester resin, diethylenetriamine are then sequentially added, boron carbide, chlorinated polyethylene, quartz
Sand, controls temperature and is 45-50 DEG C, first stirs 8-10 minute with the speed of 300-500r/min, the most again with
The speed of 600-800r/min stirs 20-25 minute, then the rest materials in formula is all joined in still,
With speed high speed dispersion 20-25 minute of 1200-1500r/min, then scattered mixed material is put into sand
Grind in grinding machine, then filter with 400 mesh filter cloths,.
Test data
The antirust paint preparing above-described embodiment is according to standard: HG/T2244-1991 " lathe priming paint " surveys
Examination, result such as table 1 below.
The testing result of table 1 antirust paint
Claims (1)
1. an iron oxide black automobile chassis antirust paint, it is characterized in that, it is prepared from by the raw material components of following weight portion: unsaturated polyester resin 55-60, diethylenetriamine 6-8, iron oxide black 15-18, silica flour 12-15, Kaolin 5-8, boron carbide 4-5, chlorinated polyethylene 5-8, quartz sand 8-10, vinyl three ('beta '-methoxy ethyoxyl) silane 3-5, methyl ethyl ketone peroxide 10-12, dimethylbenzene 32-35, film-forming resin 3-4；
Described film-forming resin is prepared from by the raw material of following weight portion: alcohol ester 12 15-18, methyl ethyl ketone peroxide 1-2, silane resin acceptor kh-550 1-1.3,2-hydroxypropyl acrylate 2-3, schmigel 1-1.4, tea polyphenols 1-2, polyisobutylene 1-1.4, ethyl acetate 12-14, wintergreen oil 1-2；The preparation method of film-forming resin is: by 2-hydroxypropyl acrylate, schmigel, tea polyphenols, polyisobutylene, ethyl acetate mixing, add methyl ethyl ketone peroxide, stirring reaction 45-60 minute, then, is warming up to 70-80 DEG C, add silane resin acceptor kh-550, alcohol ester 12, continue stirring reaction 60-90 minute, then, add other residual components, stir 30-40 minute, with 500 mesh filter-cloth filterings and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310413143.0A CN103642370B (en) | 2013-09-10 | 2013-09-10 | A kind of iron oxide black automobile chassis antirust paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310413143.0A CN103642370B (en) | 2013-09-10 | 2013-09-10 | A kind of iron oxide black automobile chassis antirust paint and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103642370A CN103642370A (en) | 2014-03-19 |
| CN103642370B true CN103642370B (en) | 2016-08-10 |
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| CN201310413143.0A Active CN103642370B (en) | 2013-09-10 | 2013-09-10 | A kind of iron oxide black automobile chassis antirust paint and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101845277A (en) * | 2010-05-14 | 2010-09-29 | 濮阳楠 | Polytetrafluoroethylene modified vinyl floor coating |
| CN102702867A (en) * | 2012-06-02 | 2012-10-03 | 安庆菱湖涂料有限公司 | Modified high chlorinated polythene long-acting anti-corrosive paint and preparation method thereof |
| CN102850899A (en) * | 2011-07-01 | 2013-01-02 | 湖南晟通科技集团有限公司 | Light cured alkali resistant coating |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100210745A1 (en) * | 2002-09-09 | 2010-08-19 | Reactive Surfaces, Ltd. | Molecular Healing of Polymeric Materials, Coatings, Plastics, Elastomers, Composites, Laminates, Adhesives, and Sealants by Active Enzymes |
-
2013
- 2013-09-10 CN CN201310413143.0A patent/CN103642370B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101845277A (en) * | 2010-05-14 | 2010-09-29 | 濮阳楠 | Polytetrafluoroethylene modified vinyl floor coating |
| CN102850899A (en) * | 2011-07-01 | 2013-01-02 | 湖南晟通科技集团有限公司 | Light cured alkali resistant coating |
| CN102702867A (en) * | 2012-06-02 | 2012-10-03 | 安庆菱湖涂料有限公司 | Modified high chlorinated polythene long-acting anti-corrosive paint and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103642370A (en) | 2014-03-19 |
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Address after: No. 3636 Qifeng Road, Shizishan Economic Development Zone, Tongling City, Anhui Province, 244031 Patentee after: Tongling Side Technology Co.,Ltd. Address before: No. 3636 Qifeng Road, Shizishan Economic Development Zone, Tongling City, Anhui Province, 244031 Patentee before: TONGLING SIDE TECHNOLOGY Co.,Ltd. |
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