CN103627909B - Copper and its alloy melt spun field of force combined filtration method - Google Patents

Copper and its alloy melt spun field of force combined filtration method Download PDF

Info

Publication number
CN103627909B
CN103627909B CN201310659022.4A CN201310659022A CN103627909B CN 103627909 B CN103627909 B CN 103627909B CN 201310659022 A CN201310659022 A CN 201310659022A CN 103627909 B CN103627909 B CN 103627909B
Authority
CN
China
Prior art keywords
filter
copper
alloy melt
compound filter
thickness
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201310659022.4A
Other languages
Chinese (zh)
Other versions
CN103627909A (en
Inventor
戴斌煜
王薇薇
商景利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nanchang Hangkong University
Original Assignee
Nanchang Hangkong University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nanchang Hangkong University filed Critical Nanchang Hangkong University
Priority to CN201310659022.4A priority Critical patent/CN103627909B/en
Publication of CN103627909A publication Critical patent/CN103627909A/en
Application granted granted Critical
Publication of CN103627909B publication Critical patent/CN103627909B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Manufacture And Refinement Of Metals (AREA)
  • Filtering Materials (AREA)

Abstract

A kind of Copper and its alloy melt spun field of force combined filtration method, it is characterized in that comprising the steps: 1. prefabricated a kind of iron and steel or ceramic running channel, it is made up of sprue and cross gate, cross gate top circle hole centreline overlaps with sprue medullary ray, brushing refractory paint in running channel, abundant oven dry, placement of multiple layers ceramic filter (device) in cross gate, stack by the descending order in aperture of ceramic filter (device) from the inside to the outside, charcoal particle or charcoal lump is placed in the middle of ceramic filter (device), composition compound filter, this compound filter total thickness is 20 ~ 200mm, 2. compound filter is fixed on the turning axle of centrifugal device, 3. before cast, compound filter is preheated to more than 500 DEG C, 4. start centrifugal device, compound filter is rotated, rotating speed is in 10 ~ 2000r/min simultaneously, and then inject copper melts or copper alloy melt, copper melts or copper alloy melt carry out combined filtration through compound filter under centrifugal action.Advantage of the present invention is: environmental pollution is little, simple to operate, is easy to control, can removal of impurities, again can deoxidation.

Description

Copper and its alloy melt spun field of force combined filtration method
Technical field
The present invention relates to a kind of metal melt filtering method, particularly relate to a kind of Copper and its alloy melt spun field of force combined filtration method.
Background technology
Copper and alloy thereof are widely used in the fields such as electrical equipment, traffic, light industry, machinofacture, building industry, national defence.Aluminium is only second in the consumption of China's nonferrous materials.But Copper and its alloy is oxidizable in fusion process, air-breathing and gettering, copper alloy melt is produced and pollutes, reduce the manufacturability of material and the performance of product.Cleaning molten is the gordian technique ensureing alloy material metallurgical quality.The object of copper alloy cleaning molten, mainly by carrying out degasification, deoxidation, impurity elimination process to copper alloy melt, removing the gas in melt and inclusion, improving the purity closing copper alloy melt.The advantage of foam ceramic filter is that it can remove the diameter inclusion particle more much smaller than its through-hole diameter.Foam ceramic filter relies on mechanical grading, filter cake mechanism, deep-bed filtration three kinds of mechanism and make aluminium alloy sublimate.Alloy melt filtration, purification effect depend on the size of ceramic foam filter hole, melt flow through the length of distance, the direction of motion conversion of melt number of times etc. relevant.The aperture of ceramic foam filter is less, and filtration, purification effect is better, but aperture is tiny, and the resistance of melt flow is large; Equally, ceramic foam filter thickness is larger, and the distance that alloy melt flows through floamed ceramics filtrating piece is longer, and filter effect is also better, but alloy melt stream to overcome the kinetic energy that resistance consumes also larger.Use the ceramic foam filter that aperture is little, thickness is large, need very high molten metal statical head to overcome resistance to flow.In continuous casting or large discharge casting technique, utilize centrifugal force, be to provide high-head a kind of easy way.At present, Copper and its alloy composite purification technology, is particularly useful for melt composite purification technology in Copper and its alloy continuous casting and rolling production, is not yet developed.
Summary of the invention
The object of the present invention is to provide a kind of Copper and its alloy melt spun field of force combined filtration method that efficiency is high, effective, environmental pollution is little.
For achieving the above object, the technical solution adopted in the present invention is for comprising following method steps:
1. prefabricated a kind of iron and steel or ceramic running channel, it is made up of sprue and cross gate, cross gate top circle hole centreline overlaps with sprue medullary ray, in running channel, brushing refractory paint, fully dries, placement of multiple layers ceramic filter (device) in cross gate, stack by the descending order in aperture of ceramic filter (device) from the inside to the outside, place charcoal particle or charcoal lump in the middle of ceramic filter (device), composition compound filter, this compound filter total thickness is 20 ~ 200mm;
2. compound filter is fixed on the turning axle of centrifugal device;
3. before cast, compound filter is preheated to more than 500 DEG C;
4. start centrifugal device, compound filter is rotated, rotating speed is in 10 ~ 2000r/min simultaneously, and then inject copper melts or copper alloy melt, copper melts or copper alloy melt carry out combined filtration through compound filter under centrifugal action.
Described porcelain filter can be block foam porcelain filter, tubular ceramic foam filter, honeycomb ceramic filter sheet device, or the combination between them.Wherein, the pore size of described block foam porcelain filter is 10 ~ 40ppi, and thickness is 20 ~ 50mm; The pore size of described tubular ceramic foam filter is 10 ~ 40ppi, and barrel bore size is 20 ~ 400mm, and thickness is 20 ~ 50mm; The pore size of described ceramic honeycomb filter is 1 ~ 10mm, and thickness is 20 ~ 50mm.
Described charcoal particle is of a size of 1 × 10 × 10 ~ 2 × 20 × 50mm, and the thickness of the charcoal layer of formation is 20 ~ 100mm; Described charcoal lump is of a size of 2 × 15 × 15 ~ 2 × 25 × 30mm, and the thickness of the charcoal layer of formation is 20 ~ 100mm.
The invention has the beneficial effects as follows: 1. can removal of impurities, simultaneously again can deoxidation, more than 5 μm inclusion particle rejection rates can reach more than 90%, copper melts oxygen level≤5ppm, and Melt parity is high, can significantly put forward heavy alloyed over-all properties; 2. simple to operate, be easy to control; 3. environmental pollution is little, meets environment protection requirement; 4. apparatus structure is simple, and cost is lower.
Accompanying drawing explanation
Fig. 1 is the embodiment of the present invention 1 compound filter structural representation;
Fig. 2 is the embodiment of the present invention 2 compound filter structural representation;
Fig. 3 is the embodiment of the present invention 2 compound filter structure schematic top plan view.
In the drawings, 1, sprue 2, ceramic filter (device) 3, charcoal layer 4, cross gate.
Embodiment
Below by way of specific embodiment, technical scheme of the present invention is further described.
Embodiment 1:
Compound filter structural representation as shown in Figure 1, the method step is:
1. prefabricated a kind of iron and steel or ceramic running channel, it is made up of with cross gate 4 vertical with it sprue 1, and cross gate 4 two ends are equipped with exit passageway;
in running channel, brushing refractory paint, fully dries;
3. three layer filtration medium is stacked in the porcelain filter 2 in cross gate 4, order is as follows: the first layer near center is gross porosity ceramic foam filter, the size in its aperture is 10ppi, thickness is 20mm, the second layer places charcoal particle, charcoal particle is of a size of 2 × 20 × 20mm, the thickness of the charcoal layer 3 formed is 60mm, outermost third layer places pore foam porcelain filter, its aperture is 40ppi's, thickness is 20mm, wherein the gross porosity ceramic foam filter of the first layer can large-sized inclusions particle in filtering medium, the charcoal layer that the charcoal particle of the second layer is formed can carry out filtration deoxidation to medium, the pore foam porcelain filter of third layer can size is tiny in filtering medium inclusion particle,
4. compound filter is fixed on the turning axle of centrifugal device;
5. before cast, compound filter is preheated to 600 DEG C;
6. start centrifugal device, running channel is rotated, rotating speed is 600r/min, and then inject copper alloy melt, copper alloy melt carries out combined filtration through compound filter under centrifugal action, and alloy melt can obtain very high cleanliness factor.
Embodiment 2:
Compound filter structural representation as shown in Figures 2 and 3, the method step is:
1. prefabricated a kind of iron and steel running channel, it is made up of sprue 1 and tubular cross gate 4 concentric with it;
in running channel, brushing refractory paint, fully dries;
3. three layer filtration medium is stacked in the porcelain filter 2 in cross gate 4, order is as follows: the first layer near center is gross porosity tubular ceramic foam filter, the size in its aperture is 10ppi, the internal diameter size of cylinder is 100mm, thickness is 20mm, the second layer is placed and is of a size of 2 × 25 × 25mm charcoal lump, charcoal layer 3 thickness formed is 80mm, third layer places pore tubular ceramic foam filter, the size in its aperture is 40ppi, barrel bore is 300mm, thickness is 20mm, wherein the pore tubular ceramic foam filter of the first layer can large-sized inclusions particle in filtering medium, the charcoal layer that the charcoal lump of the second layer is formed can carry out filtration deoxidation to medium, the pore tubular ceramic foam filter of third layer can size is tiny in filtering medium inclusion particle,
4. compound filter is fixed on the turning axle of centrifugal device;
5. before cast, compound filter is preheated to 700 DEG C;
6. start centrifugal device, running channel is rotated, rotating speed is 500r/min, and then inject copper alloy melt, copper alloy melt carries out combined filtration through compound filter under centrifugal action.

Claims (1)

1. a Copper and its alloy melt spun field of force combined filtration method, is characterized in that comprising following method steps:
1. prefabricated a kind of iron and steel or ceramic running channel, it is made up of sprue and cross gate, cross gate top circle hole centreline overlaps with sprue medullary ray, in running channel, brushing refractory paint, fully dries, placement of multiple layers porcelain filter in cross gate, stack by the descending order in the aperture of porcelain filter from the inside to the outside, place charcoal particle or charcoal lump in the middle of porcelain filter, composition compound filter, this compound filter total thickness is 20 ~ 200mm;
2. compound filter is fixed on the turning axle of centrifugal device;
3. before cast, compound filter is preheated to more than 500 DEG C;
4. start centrifugal device, compound filter is rotated, make rotating speed simultaneously in 10 ~ 2000r/min, then pour into a mould copper melts or copper alloy melt, copper melts or copper alloy melt carry out combined filtration through compound filter under centrifugal action;
Described porcelain filter is block foam porcelain filter, tubular ceramic foam filter, ceramic honeycomb filter, or the combination between them;
The pore size of described block foam porcelain filter is 10 ~ 40ppi, and thickness is 20 ~ 50mm;
The pore size of described tubular ceramic foam filter is 10 ~ 40ppi, and barrel bore size is 20 ~ 400mm, and thickness is 20 ~ 50mm;
The pore size of described ceramic honeycomb filter is 1 ~ 10mm, and thickness is 20 ~ 50mm;
Described charcoal particle is of a size of 1 × 10 × 10 ~ 2 × 20 × 50mm, and the thickness of the charcoal layer of formation is 20 ~ 100mm; Described charcoal lump is of a size of 2 × 15 × 15 ~ 2 × 25 × 30mm, and the thickness of the charcoal layer of formation is 20 ~ 100mm.
CN201310659022.4A 2013-12-10 2013-12-10 Copper and its alloy melt spun field of force combined filtration method Expired - Fee Related CN103627909B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310659022.4A CN103627909B (en) 2013-12-10 2013-12-10 Copper and its alloy melt spun field of force combined filtration method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310659022.4A CN103627909B (en) 2013-12-10 2013-12-10 Copper and its alloy melt spun field of force combined filtration method

Publications (2)

Publication Number Publication Date
CN103627909A CN103627909A (en) 2014-03-12
CN103627909B true CN103627909B (en) 2015-10-21

Family

ID=50209354

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310659022.4A Expired - Fee Related CN103627909B (en) 2013-12-10 2013-12-10 Copper and its alloy melt spun field of force combined filtration method

Country Status (1)

Country Link
CN (1) CN103627909B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2727478C1 (en) * 2020-01-24 2020-07-21 Олег Владимирович Анисимов Method of cleaning aluminum and its alloys from intermetallides and other non-metallic inclusions

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0347108A1 (en) * 1988-06-14 1989-12-20 Alcan International Limited Treatment of molten light metals
CN1379116A (en) * 2002-01-22 2002-11-13 上海交通大学 Molten metals mixer
CN1386871A (en) * 2002-04-30 2002-12-25 上海交通大学 Deep-bed apparatus of industrial centrifugal machine for filtering out entrainments from molten aluminium
CN1389583A (en) * 2002-04-30 2003-01-08 上海交通大学 Filtering method of non-metallic inclusion in aluminium melt
CN1555944A (en) * 2003-12-30 2004-12-22 上海交通大学 Copper fused mass filtering deoxygen technology
CN1556232A (en) * 2003-12-30 2004-12-22 上海交通大学 Device for producing oxygen less copper utilizing waste red copper
CN101884956A (en) * 2009-05-16 2010-11-17 史志铭 High-temperature fusant filtering equipment
CN102069147A (en) * 2011-01-30 2011-05-25 南昌航空大学 Method for composite-filtering multiple filter media in aluminum-alloy-melt centrifuge field
CN102139348A (en) * 2011-03-16 2011-08-03 南昌航空大学 Composite filtering method of a plurality of filter media in centrifugal force field of steel melt
CN102888517A (en) * 2012-11-05 2013-01-23 南昌航空大学 Zinc and zinc alloy melt foamed ceramic centrifugal compound purification device

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0347108A1 (en) * 1988-06-14 1989-12-20 Alcan International Limited Treatment of molten light metals
CN1379116A (en) * 2002-01-22 2002-11-13 上海交通大学 Molten metals mixer
CN1386871A (en) * 2002-04-30 2002-12-25 上海交通大学 Deep-bed apparatus of industrial centrifugal machine for filtering out entrainments from molten aluminium
CN1389583A (en) * 2002-04-30 2003-01-08 上海交通大学 Filtering method of non-metallic inclusion in aluminium melt
CN1555944A (en) * 2003-12-30 2004-12-22 上海交通大学 Copper fused mass filtering deoxygen technology
CN1556232A (en) * 2003-12-30 2004-12-22 上海交通大学 Device for producing oxygen less copper utilizing waste red copper
CN101884956A (en) * 2009-05-16 2010-11-17 史志铭 High-temperature fusant filtering equipment
CN102069147A (en) * 2011-01-30 2011-05-25 南昌航空大学 Method for composite-filtering multiple filter media in aluminum-alloy-melt centrifuge field
CN102139348A (en) * 2011-03-16 2011-08-03 南昌航空大学 Composite filtering method of a plurality of filter media in centrifugal force field of steel melt
CN102888517A (en) * 2012-11-05 2013-01-23 南昌航空大学 Zinc and zinc alloy melt foamed ceramic centrifugal compound purification device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2727478C1 (en) * 2020-01-24 2020-07-21 Олег Владимирович Анисимов Method of cleaning aluminum and its alloys from intermetallides and other non-metallic inclusions

Also Published As

Publication number Publication date
CN103627909A (en) 2014-03-12

Similar Documents

Publication Publication Date Title
CN101781712B (en) Runner type online degassing device
CN103990786B (en) A kind of for removing the device and method of molten steel field trash in double flow tray billet continuous casting machine tundish
CN103990787A (en) Device and method for removing molten steel slag inclusion in continuous casting tundish
CN107119192A (en) The method and device of electromagnetism vortex driving force purifying molten metal
CN104550805A (en) Device and method for preparing magnesium alloy ingot blank for deformation
CN103990772B (en) A kind of metallurgical plant removing double flow tray billet continuous casting machine tundish inclusion
CN201880881U (en) Aluminum melt filtering device
CN102069147B (en) Method for composite-filtering multiple filter media in aluminum-alloy-melt centrifuge field
CN104212985A (en) Preparation method of low-H content aerospace aluminum alloy melt
CN103627909B (en) Copper and its alloy melt spun field of force combined filtration method
CN202963405U (en) Liquid aluminum casting filter device
CN207887873U (en) The anti-dross device of double zigzags for continuous casting production exit
CN104624995B (en) The device of liquid level fluctuation of crystallizer is suppressed under a kind of high pulling rate
CN206392813U (en) Liquid copper and its alloy Continuous Up casting filter
CN102139348B (en) Composite filtering method of a plurality of filter media in centrifugal force field of steel melt
CN207695615U (en) A kind of bilayer dual control aluminium slag filter device
CN202139280U (en) Aluminum liquid online filtering device
CN110227814B (en) Rotary centrifugal filtering tundish for continuous casting and rolling production of clean steel
CN2889442Y (en) Filtering device for alloy solution
CN106825485B (en) A kind of aluminium alloy purification siphon transfer pipe
CN203209685U (en) Quasi-four-hole immersed nozzle for FTSC thin slab continuous casting crystallizer
CN105234360B (en) Molten steel inclusion catcher and inclusion removing method
CN110744012A (en) Spiral hole type ceramic filter for metal casting
CN101791693B (en) Tundish with quick-replaceable inclusion removing device and operation method thereof
CN111496242A (en) Turbulent flow type aluminum alloy melt deslagging and filtering device and using method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151021

Termination date: 20171210

CF01 Termination of patent right due to non-payment of annual fee