CN1036235A - The weaving techniques of pre-oxidized polyacrylonitrile fiber - Google Patents

The weaving techniques of pre-oxidized polyacrylonitrile fiber Download PDF

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Publication number
CN1036235A
CN1036235A CN 88101770 CN88101770A CN1036235A CN 1036235 A CN1036235 A CN 1036235A CN 88101770 CN88101770 CN 88101770 CN 88101770 A CN88101770 A CN 88101770A CN 1036235 A CN1036235 A CN 1036235A
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China
Prior art keywords
fabric
oxidized
bar
fibre
polyacrylonitrile
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Pending
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CN 88101770
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Chinese (zh)
Inventor
赵宇辉
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RESEARCH INST OF TEXTILE SCIENCE SHANXI PROV
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RESEARCH INST OF TEXTILE SCIENCE SHANXI PROV
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Priority to CN 88101770 priority Critical patent/CN1036235A/en
Publication of CN1036235A publication Critical patent/CN1036235A/en
Pending legal-status Critical Current

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  • Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
  • Woven Fabrics (AREA)

Abstract

A kind of method with the pure fabric of plain polypropylene nitrile fibrous woven device fabrication pre-oxidized polyacrylonitrile fiber, be with water-soluble fibre and pre-oxidized polyacrylonitrile fiber blending, be woven into the molten again soluble fiber that anhydrates behind the fabric, obtain virgin pp nitrile pre-oxidized fibers fabric at last.This method technology is simple, and the fabric cost is low, and yarn strength and weaving efficiency are higher, and the fabric flame resistance is good, and not on fire in naked light, fire endurance oxygen index (OI) can reach 48~60.This fabric can be used for the dustcoat of military equipments such as tank, artillery; Also can make the special fireproof clothes.It is the ideal fireproof textile material.

Description

The weaving techniques of pre-oxidized polyacrylonitrile fiber
The present invention relates to a kind of weaving techniques of the polyacrylonitrile fibre of anti-the combustion.Belong to the method for giving oxidized fiber fabric with the method processing virgin pp nitrile of blending.Being meant specifically that the fiber that adds in the blending process can dissolve after being made into fabric removes, and finally obtains the method that the virgin pp nitrile gives oxidized fiber fabric.
The weaving method of the known polyacrylonitrile fibre of anti-the combustion has: (1) adds chemical fire retardant, and this fabric can burn in naked light, only leaves just to have oneself behind the naked light and put out effect; The fire endurance oxygen index (OI) of this fabric is up to 28~30 simultaneously.(2) the virgin pp nitrile gives oxidized fibre phosphorus content height, property is crisp, need with 15~30% wool blendedly just have a spinnability, and wool need carry out flame treatment, the fire endurance oxygen index (OI) of the wool-blend fabric after the processing, compares with the fire endurance oxygen index (OI) that the virgin pp nitrile gives the oxidation fabric and to still have gap.
The objective of the invention is: a kind of method of giving oxidized fiber fabric with plain polypropylene nitrile fibrous woven device fabrication virgin pp nitrile is provided.
Realize that the technical scheme that the object of the invention adopted is: with polyacrylonitrile give oxidized fibre and water-soluble fibre bar by 60 to 40 to 85 than 15(weight ratio) mix, in relative humidity 50~70%, under the condition that temperature is 20~25 ℃ after the crush cutting slivering, through operations such as doubling, rove, spun yarn spinnings resultant yarn, again through winder, warping, weave, operation such as dissolving and be made into fabric; Drafting after-ripening bar weight can be 4.8~9.5g/m; The roving-drafting multiple can be 5~7 times, and the spinning-drafting multiple can be 15~17 times, and the twist can be controlled in 390~450 sth. made by twisting/rice, 8~55 public of scopes of can spinning, and fabric can be 260~310g/m 2
Advantage of the present invention and good effect are: textile technology is simple, need not to change existing acrylic Weaving device, and the fabric cost is low, and yarn strength is higher by 25~35% than wool blended; Higher more than 30% than the pure oxidized fibre that gives.Weaving efficiency is higher by 40~50% than wool blended, and is higher by 30~35% than the pure oxidized fibre that gives.The fabric flame resistance is good, and not on fire in naked light, the fire endurance oxygen index (OI) can reach 48~60.This fabric can be used for the dustcoat of military equipments such as tank, artillery, also can do the special fireproof clothes of military project, forest, public security.
Most preferred embodiment of the present invention is: with fibre fineness 1.5
Figure 881017701_IMG1
(D) heavy 16g/m(of the hydrolysis vinylon fiber bar of the heavy 10g/m of bar, fibre length 90mm, regain 2.9% and bar or 8.8g/m), the polyacrylonitrile of regain 6.5% gives the oxidized fibre bar, giving the oxidized fibre bar by polyacrylonitrile is 75: 25 than hydrolysis vinylon fiber bar, under the condition of 20~25 ℃ of relative humidity 60~70%, temperature through B 412Gilling machine crush cutting slivering is after B 423And B 432Gill box, B 465ASpeed frames, B 583AFine spining machine is spun into 24 public left and right sides yarns, is made into the 310g/m fabric through 1332MD bobbin winder etc. again, and the hydrolysis vinylon fiber is removed in dissolving in boiling water, obtains about 285g/m at last 2The virgin pp nitrile give oxidized fiber fabric.Its concrete technological parameter can be:
1, B 412Gilling machine:
The drafting number is 6 also, and drafting multiple gets 7.27, spaces to be 55mm needle plate 10#, pressurization 8kg/cm 2, shaping quantitatively is 9.5g/m.
2, B 423Gill box:
The drafting number is 8 also, drafting multiple 6.42, and spacing is 60mm, needle plate 13#, pressurization 10kg/cm 2, the quantitative 8.4g/m of shaping.
3, B 432Gill box:
The drafting number is 2 also, drafting multiple 6.86, the 45mm that spaces, needle plate 16#, pressurization 10kg/cm 2, the quantitative 2.4g/m of shaping.
4, B 465ASpeed frames:
The drafting number is 2 also, 7 times of drafting multiples, the 100 * 105mm that spaces, the twist 15.11 sth. made by twisting/rice, 505.43 rev/mins of ingot speed, the heavy 0.65g/m of bar.
5, B 583AFine spining machine:
Drafting multiple 15.48, the 110 * 100mm that spaces, the twist 405.5 sth. made by twisting/rice, 8432 rev/mins of ingot speed, steel wire (volume) 23#, strip quantitatively are 0.042g/m.
6,1332MD bobbin winder:
Tension pulley weight 26g, the yarn clearer 0.6mm that spaces.

Claims (3)

1, a kind of Weaving device with plain polypropylene nitrile fiber is produced the method that polyacrylonitrile gives the pure fabric of oxidized fibre, it is characterized in that: polyacrylonitrile is given oxidized fibre mix by 60 to 40 to 85 to 15 (weight ratios) with the water-soluble fibre bar, after the crush cutting slivering, through operations such as doubling, rove, spun yarn spinnings resultant yarn, again through winder, warping, weave, operation such as dissolving forms fabric.
2, by the described method of claim 1, it is characterized in that: spinning humidity can be 50~70%(relative humidity), temperature can be 20~25 ℃; Drafting after-ripening bar weight can be 4.8~9.5g/m; The roving-drafting multiple can be 5~7 times, and the spinning-drafting multiple can be 15~17 times; The twist can be 390~450 sth. made by twisting/rice; 8~55 public of scopes of can spinning; Fabric can be 260~310g/m 2
3, by claim 1,2 described methods, it is characterized in that: water-soluble fibre can be a hydrolysis vinylon; The ratio that polyacrylonitrile gives oxidized fibre bar and hydrolysis vinylon fiber bar can be 75 to 25.
CN 88101770 1988-03-29 1988-03-29 The weaving techniques of pre-oxidized polyacrylonitrile fiber Pending CN1036235A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 88101770 CN1036235A (en) 1988-03-29 1988-03-29 The weaving techniques of pre-oxidized polyacrylonitrile fiber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 88101770 CN1036235A (en) 1988-03-29 1988-03-29 The weaving techniques of pre-oxidized polyacrylonitrile fiber

Publications (1)

Publication Number Publication Date
CN1036235A true CN1036235A (en) 1989-10-11

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CN 88101770 Pending CN1036235A (en) 1988-03-29 1988-03-29 The weaving techniques of pre-oxidized polyacrylonitrile fiber

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CN (1) CN1036235A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103374788A (en) * 2013-05-16 2013-10-30 江南大学 Quasi-all-carbon multi-axial warp kitted fabric stitched with pre-oxidized fibers
CN105040222A (en) * 2015-07-10 2015-11-11 上海兰邦工业纤维有限公司 Fireproof yarn high in limit oxygen index, preparation method of fireproof yarn and fabric of fireproof yarn
CN106149135A (en) * 2016-09-23 2016-11-23 仇晓丰 Temperature-sensitive biological fiber fabric
CN106435952A (en) * 2016-10-13 2017-02-22 余燕平 Novel light inflaming-resisting heat-insulating heat preservation protection fabric and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103374788A (en) * 2013-05-16 2013-10-30 江南大学 Quasi-all-carbon multi-axial warp kitted fabric stitched with pre-oxidized fibers
CN105040222A (en) * 2015-07-10 2015-11-11 上海兰邦工业纤维有限公司 Fireproof yarn high in limit oxygen index, preparation method of fireproof yarn and fabric of fireproof yarn
CN106149135A (en) * 2016-09-23 2016-11-23 仇晓丰 Temperature-sensitive biological fiber fabric
CN106435952A (en) * 2016-10-13 2017-02-22 余燕平 Novel light inflaming-resisting heat-insulating heat preservation protection fabric and preparation method thereof

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