CN103622120A - Corn stalk beverage and preparation method thereof - Google Patents

Corn stalk beverage and preparation method thereof Download PDF

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Publication number
CN103622120A
CN103622120A CN201310536447.6A CN201310536447A CN103622120A CN 103622120 A CN103622120 A CN 103622120A CN 201310536447 A CN201310536447 A CN 201310536447A CN 103622120 A CN103622120 A CN 103622120A
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juice
cornstalk
beverage
preparation
maize stem
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CN201310536447.6A
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CN103622120B (en
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黄聪亮
郑佳俐
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

The invention discloses a corn stalk beverage and a preparation method thereof. The corn stalk beverage is prepared from the following raw materials in percentage by weight: 18%-22% of raw corn stalk juice, 3%-5% of raw clear corn juice, 0.12%-0.17% of a sour agent, 2.5%-3.5% of a sweetening agent, 0.01%-0.04% of food additives and the balance being water. The preparation method comprises the following steps: checking and accepting the raw materials, removing leaves and washing, squeezing to obtain juice, protecting the color, coarsely filtering, blending, carrying out micro-filtering through a ceramic membrane, instantly sterilizing at ultrahigh temperature, canning and sealing, cooling to room temperature to obtain the corn stalk beverage, airing, inspecting, performing label trapping, label shrinking and code spraying, and packaging and storing the sealed and cooled corn stalk beverage. The corn stalk beverage produced by using the method is high in light transmittance and good in storage stability, sensory quality and stability, and completely retains the aroma.

Description

A kind of maize stem beverage and preparation method thereof
Technical field
The present invention relates to technical field of beverage processing, specifically refer to a kind of maize stem beverage and preparation method thereof.
Background technology
Corn is annual gramineae herbaceous plant, is important cereal crops and important feed resource, is also the highest cereal crops of whole world total output.Corn is economized in the plantation of China Da Shiyu, as Jilin, Henan, Shandong, Zhejiang, Fujian, Yunnan, Guangdong, Guangxi, Guizhou, Sichuan, Shaanxi, Gansu, Hebei, Anhui, Xinjiang and other places.The ripening fruits of gathering in summer, autumn.Cornstalk amount after corn is gathered is very large, and all the time, cornstalk does not all obtain making full use of of people, and its feed, fertilizer and fuel that is often used as animal is used, and value is very low.For improving the value of cornstalk, people are used as raw-food material by research by cornstalk, as patent No. CN200610054545.6 cornstalk beverage and processing method thereof, by cornstalk being cleaned, squeezes, filtration, sterilization, be compressed to after the concentration of 5-50%, then blend and be diluted to maize stem beverage according to mouthfeel.
Summary of the invention
The invention reside in a kind of raising light transmittance is provided, storage-stable is good, and organoleptic quality and stability are high, fragrance retains complete maize stem beverage and processing method thereof.
Concrete technical scheme of the present invention is as follows:
A kind of maize stem beverage and preparation method thereof, described maize stem beverage is that the raw material being configured by following ratio is by weight prepared from:
Cornstalk Normal juice 18-22%, the clear juice Normal juice of corn 3-5%, acid 0.12-0.17%, sweetener 2.5-3.5%, food additives 0.01-0.04%, surplus is water;
The manufacturing process of described maize stem beverage is as follows:
(1) raw material is checked and accepted: select fresh, complete, without disease and pest, the cornstalk raw material that has no mechanical damage;
(2) defoliation cleans: by cornstalk raw material defoliation, soak 28-35min in clear water, and repeatedly rinse, wash silt and the impurity on cornstalk surface;
(3) press extracting juice: the cornstalk cleaning is pressed to extracting juice;
(4) protect look: after cornstalk Normal juice squeezes out, add immediately the ascorbic acid of 0.02-0.04% and stir and protect look, prevent brown stain;
(5) coarse filtration: cornstalk Normal juice is carried out to centrifugal filtration with centrifuge, and the nylon cloth in described centrifuge more than pad 80 orders, removes the impurity in Normal juice, flux during raising later stage membrane filtration also reduces film pollution;
(6) allotment: add after food additives toward cornstalk Normal juice, then add in proportion the clear juice of corn, sweetener, acid and water and stir;
(7) microfiltration of ceramic membrane: adopt 0.05 μ m-0.5 μ m ceramic membrane to filter, cause the macromolecular substances of later stage precipitation to remove the overwhelming majority;
(8) ultra high temperature short time sterilization: adopt 135 ℃ of above high temperature sterilization 7-9s;
(9) filling and sealing: after container filling is cleaned with automatic bottle cleaning machine, the product after sterilization filling and sealing the bottle that falls 85 ℃-95 ℃ time;
(10) cooling: the product after filling is cooled to room temperature and obtains described maize stem beverage;
Described maize stem beverage filling and sealing, cooling after, by being packaged into storehouse after air-dry, check, cover mark, contracting mark, coding.
Described pressure extracting juice comprises twice squeezing, and the cornstalk cleaning is pressed to extracting juice for the first time, then with 100 ℃ of hot water, carries out carrying out twice pressing after high temperature spray, improves cornstalk juice crushing juice rate.
Described sweetener is sucrose.
Described acid is citric acid.
Described food additives are potassium sorbate.
Advantage of the present invention:
Corn is the highest cereal crops of whole world total output, the data that national food information centre provides show, China's Chinese maize output in 2012 is estimated to reach 2.01 hundred million tons, and the quantity of the maize straw that its plant development produces is extremely huge, but people did not have to be made full use of in recent years.And modern scientific research report, the main carbohydrate-wood sugar in maize straw, due to its unique chemical property and physiological function, has the health care of the rich man's diseases such as prevention diabetes, hypertension, obesity.The a series of cornstalk Normal juice of being processed into of maize straw process, as the raw material of preparation of drinks, is not only had to the utilization rate that certain health care can also largely improve maize straw.
The present invention is primary raw material by cornstalk Normal juice, the clear juice Normal juice of corn, by interpolation citric acid and sucrose allotment, is made, and by repeatedly allocating, has determined the optimum formula of maize stem beverage beverage; The present invention first carries out centrifugal filtration to cornstalk Normal juice, remove the impurity in Normal juice, and then the cornstalk beverage after adopting 0.05 μ m-0.5 μ m ceramic membrane to allotment filters, to remove the overwhelming majority, cause the macromolecular substances of later stage precipitation, so, the cornstalk Normal juice making there will not be any muddiness and deposited phenomenon, thereby guarantees that the clarification of cornstalk Normal juice has good stability and fragrance retains, improve light transmittance, storage-stable, organoleptic quality and the stability of maize stem beverage.
Accompanying drawing explanation
Fig. 1 is the comparison diagram of the light transmittance of microfiltration of ceramic membrane and the clarification of traditional enzymolysis.
The specific embodiment
For the ease of it will be appreciated by those skilled in the art that by the following examples, the present invention is described in further detail, but the present invention is not limited only to this.
A kind of maize stem beverage and preparation method thereof, described maize stem beverage is that the raw material being configured by following ratio is by weight prepared from: cornstalk Normal juice 20%, the clear juice Normal juice 4% of corn, citric acid 0.15%, sucrose 3%, potassium sorbate 0.02%, water 72.83%,
The manufacturing process of described maize stem beverage is as follows:
(1) raw material is checked and accepted: select fresh, complete, without disease and pest, the cornstalk raw material that has no mechanical damage;
(2) defoliation cleans: by cornstalk raw material defoliation, soak 30min in clear water, and repeatedly rinse, wash silt and the impurity on cornstalk surface;
(3) press extracting juice: described pressure extracting juice comprises twice squeezing, and the cornstalk cleaning is pressed to extracting juice for the first time, then with 100 ℃ of hot water, carry out carrying out twice pressing after high temperature spray, improve cornstalk juice crushing juice rate.
(4) protect look: after cornstalk Normal juice squeezes out, add immediately 0.03% ascorbic acid and stir and protect look, prevent brown stain;
(5) coarse filtration: cornstalk Normal juice is carried out to centrifugal filtration with centrifuge, and the nylon cloth in described centrifuge more than pad 80 orders, removes the impurity in Normal juice, flux during raising later stage membrane filtration also reduces film pollution;
(6) allotment: add toward cornstalk Normal juice after 0.02% potassium sorbate, then add in proportion the clear juice of corn, sucrose, citric acid and water and stir;
(7) microfiltration of ceramic membrane: adopt 0.20 μ m ceramic membrane to filter, cause the macromolecular substances of later stage precipitation to remove the overwhelming majority;
Determining of ceramic membrane aperture:
Light transmittance, clear juice yield and the fragrance loss variation of cornstalk Normal juice after 0.05 μ m, 0.20 μ m, tri-kinds of aperture ceramic membrane clarifications of 0.50 μ m sees the following form.
The impact of 3 kinds of aperture inorganic ceramic membranes of table 1 on indexs such as cornstalk juice physics and chemistry
Index Normal juice 0.05μm 0.20μm 0.50μm
Light transmittance (%) 70.5 98.7 97.2 91.3
Clear juice yield (%) 100 65.3 80.1 87.5
Fragrance ?+++++ +++ ++++ +++++
Stability (10 months) Precipitate Without precipitation Without precipitation Precipitate
Note: "+" is the grading system of cornstalk juice fragrance ,+more multilist shows that fragrance is better, best result is " 5+ "
By test data, can be found out that the ceramic membrane in three kinds of apertures can more effectively hold back the macromolecular substances that easily causes turbidity sediment in cornstalk juice.But fragrance reservation aspect, the clear juice fragrance loss of 0.05 μ m membrane filtration is larger, and after 0.20 μ m membrane microfiltration, cornstalk juice fragrance is slightly lost but loses littlely, and the clear juice fragrance that 0.5 μ m makes is compared and is not almost had loss with Normal juice.Aspect bin stability, preserve at normal temperatures after 10 months, there is precipitation in the subsider juice that 0.50 μ m film makes, and 0.05 μ m, all there is not any muddiness and deposited phenomenon in the subsider juice that 0.20 μ m film makes, clarification has good stability.By comprehensive comparison, aspect storage-stable, 0.05 μ m, 0.20 μ m can reach satisfied effect, but consider that 0.05 μ m membrane filtration fragrance loss is large and clear juice yield is on the low side.Therefore determine that 0.20 μ m is for the best film aperture of clarification cornstalk juice.
(8) ultra high temperature short time sterilization: adopt 135 ℃ of above high temperature sterilization 8s;
(9) filling and sealing: after container filling is cleaned with automatic bottle cleaning machine, the product after sterilization 90 ℃ of filling and sealings the bottle that falls while hot;
(10) cooling: the product after filling is cooled to room temperature and obtains described maize stem beverage;
Described maize stem beverage filling and sealing, cooling after, by being packaged into storehouse after air-dry, check, cover mark, contracting mark, coding.
The present invention is made by cornstalk Normal juice, the clear juice Normal juice of corn, citric acid and sucrose allotment, by repeatedly allocating, to determine the optimum formula of maize stem beverage beverage;
the formulation selection experiment of cornstalk juice beverage
With cornstalk Normal juice (A), the clear juice Normal juice of corn (B), citric acid (C) and 4 factors of sucrose (D), carry out L 9(3 4) orthogonal test (table 3), to determine the optimum formula of maize stem beverage beverage.
Table 3 maize stem beverage formula factors water-glass
Organoleptic indicator's scoring and standard:
Invite 10 and be engaged in Majors of Food personnel, according to product standards of grading (in Table 4) to the product of different formulations according to color and luster, smell, mouthfeel, mark, according to appraisal result, determine the optimization formula of corn juice beverage.
Table 4 sensory evaluation scores standard
Normative reference (100 minutes) Color and luster (30 minutes) Fragrance (30 minutes) Mouthfeel (40 minutes)
Excellent Faint yellow, non-variegation, color and luster is (26 ~ 30) evenly Fragrance is pure and fresh, free from extraneous odour (27 ~ 30) Sour-sweet moderate flavor coordination tasty and refreshing lubricious (36 ~ 40)
Good Color and luster slightly dark or slightly shallow (20 ~ 25) Fragrance is lighter, slightly taste (22 ~ 26) Sour-sweet degree is better, and mouthfeel is slightly coarse, tasty and refreshing not (30 ~ 35)
Poor Color is too shallow or too dark, has variegated (0 ~ 19) Without fragrance, there are denseer boiling taste or peculiar smell (0 ~ 21) Peracid is excessively sweet, and sour-sweet taste is excessively light, or has other strange taste (0 ~ 29)
Table 5 orthogonal experiments table
As can be seen from Table 5, optimum formula technique is A 2b 1c 2d 1, cornstalk Normal juice 20%, the clear juice Normal juice 4% of corn, citric acid 1.5g/L (0.15%), sucrose 3%.
The present invention first to cornstalk Normal juice by centrifugal filtration, remove the impurity in Normal juice, and then the cornstalk beverage after adopting 0.05 μ m-0.5 μ m ceramic membrane to allotment filters, to remove the overwhelming majority, cause the macromolecular substances of later stage precipitation, so the cornstalk Normal juice, making there will not be any muddiness and deposited phenomenon.
the Contrast on effect experiment of microfiltration of ceramic membrane and the clarification of traditional enzymolysis
In order to inquire into the superiority of membrane filter method, itself and traditional enzymatic isolation method are contrasted, relatively light transmittance, sense organ and the stability after the two clarification.
1. microfiltration of ceramic membrane clarification: Normal juice → 200 order filtration → microfiltration of ceramic membrane → clear juice → sterilizing bottling
2. traditional enzymolysis clarification: the Normal juice → enzymolysis → enzyme → centrifugal filtration of going out → sterilizing bottling
(ceramic membrane is selected 0.20 μ m film, and operating pressure is 0.2MPa, and temperature is 30 ℃, and flow velocity is 2m/s; Enzymolysis process: pectase 1500U/100g; Protease 5000U/100g; PH=4.5; T=50 ℃; Time 2h.)
The contrast of the light transmittance of microfiltration of ceramic membrane and the clarification of traditional enzymolysis as shown in Figure 1.
The contrast of table 2 organoleptic quality and stability
Sample Outward appearance Local flavor Stability
Cornstalk Normal juice Yellow, muddy, opaque Local flavor is obvious, free from extraneous odour After 10 months, precipitate
Enzyme process subsider juice Faint yellow, clarification, transparent Local flavor is slightly light, and micro-have a peculiar smell After 10 months, precipitate
Ceramic membrane subsider juice Faint yellow, limpid, bright Local flavor is obvious, free from extraneous odour After 10 months, have no precipitation
From above analysis, can find out, with ceramic membrane, clarify cornstalk juice beverage and in light transmittance, sense organ or storage stability, be all obviously better than traditional enzymatic isolation method.
The foregoing is only preferred embodiment of the present invention, all equalizations of doing according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.

Claims (5)

1. maize stem beverage and preparation method thereof, is characterized in that: described maize stem beverage is that the raw material by the following configuration of ratio is by weight prepared from:
Cornstalk Normal juice 18-22%, the clear juice Normal juice of corn 3-5%, acid 0.12-0.17%, sweetener 2.5-3.5%, food additives 0.01-0.04%, surplus is water;
The manufacturing process of described maize stem beverage is as follows:
(1) raw material is checked and accepted: select fresh, complete, without disease and pest, the cornstalk raw material that has no mechanical damage;
(2) defoliation cleans: by cornstalk raw material defoliation, soak 28-35min in clear water, and repeatedly rinse, wash silt and the impurity on cornstalk surface;
(3) press extracting juice: the cornstalk cleaning is pressed to extracting juice;
(4) protect look: after cornstalk Normal juice squeezes out, add immediately the ascorbic acid of 0.02-0.04% and stir and protect look, prevent brown stain;
(5) coarse filtration: cornstalk Normal juice is carried out to centrifugal filtration with centrifuge, and the nylon cloth in described centrifuge more than pad 80 orders, removes the impurity in Normal juice, flux during raising later stage membrane filtration also reduces film pollution;
(6) allotment: add after food additives toward cornstalk Normal juice, then add in proportion the clear juice of corn, sweetener, acid and water and stir;
(7) microfiltration of ceramic membrane: adopt 0.05 μ m-0.5 μ m ceramic membrane to filter, cause the macromolecular substances of later stage precipitation to remove the overwhelming majority;
(8) ultra high temperature short time sterilization: adopt 135 ℃ of above high temperature sterilization 7-9s;
(9) filling and sealing: after container filling is cleaned with automatic bottle cleaning machine, the product after sterilization filling and sealing the bottle that falls 85 ℃-95 ℃ time;
(10) cooling: the product after filling is cooled to room temperature and obtains described maize stem beverage;
Described maize stem beverage filling and sealing, cooling after, by being packaged into storehouse after air-dry, check, cover mark, contracting mark, coding.
2. a kind of maize stem beverage according to claim 1 and preparation method thereof, it is characterized in that: described pressure extracting juice comprises twice squeezing, the cornstalk cleaning is pressed to extracting juice for the first time, then with 100 ℃ of hot water, carry out carrying out twice pressing after high temperature spray, improve cornstalk juice crushing juice rate.
3. a kind of maize stem beverage according to claim 1 and preparation method thereof, is characterized in that: described sweetener is sucrose.
4. a kind of maize stem beverage according to claim 1 and preparation method thereof, is characterized in that: described acid is citric acid.
5. a kind of maize stem beverage according to claim 1 and preparation method thereof, is characterized in that: described food additives are potassium sorbate.
CN201310536447.6A 2013-11-04 2013-11-04 A kind of manufacture method of maize stem beverage Expired - Fee Related CN103622120B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107549565A (en) * 2017-10-19 2018-01-09 陈春安 A kind of agricultural crop straw beverage and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1078615A (en) * 1993-04-15 1993-11-24 刘绍之 Drink made from corn juice
CN1943446A (en) * 2006-10-30 2007-04-11 李来凤 Corn stalk drink and its processing method
CN102771850A (en) * 2012-08-13 2012-11-14 安徽农业大学 Method for preparing cooling drink by use of chrysanthemum straw

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1078615A (en) * 1993-04-15 1993-11-24 刘绍之 Drink made from corn juice
CN1943446A (en) * 2006-10-30 2007-04-11 李来凤 Corn stalk drink and its processing method
CN102771850A (en) * 2012-08-13 2012-11-14 安徽农业大学 Method for preparing cooling drink by use of chrysanthemum straw

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
范娟等: "玉米秸秆汁营养效价及其原生态秸秆汁饮料生产新工艺研发", 《2010全国农作物秸秆综合利用研讨会暨新技术新产品交流会》, 20 June 2011 (2011-06-20) *
范娟等: "玉米秸秆饮料营养成分与生产工艺流程研究", 《江苏农业科学》, no. 01 *
阮美娟等: "《饮料工艺学》", 31 January 2013, article "膜分离技术" *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107549565A (en) * 2017-10-19 2018-01-09 陈春安 A kind of agricultural crop straw beverage and preparation method thereof

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