CN103602902A - Powder metallurgy pressure-resistant composite metal material and preparation method thereof - Google Patents

Powder metallurgy pressure-resistant composite metal material and preparation method thereof Download PDF

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Publication number
CN103602902A
CN103602902A CN201310469328.3A CN201310469328A CN103602902A CN 103602902 A CN103602902 A CN 103602902A CN 201310469328 A CN201310469328 A CN 201310469328A CN 103602902 A CN103602902 A CN 103602902A
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powder
metal material
composite metal
hour
sintering
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CN201310469328.3A
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CN103602902B (en
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胡光荣
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Guangxi Shenglong Metallurgical Co Ltd
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TONGLING XINCHUANG FLUID TECHNOLOGY Co Ltd
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Abstract

The invention discloses a powder metallurgy pressure-resistant composite metal material. The composite metal material is characterized in that: the composite metal material is prepared from following raw materials in parts by weight: 45-47 of 316 stainless steel powder, 50-74 of iron powder, 1-2 of graphite fiber, 1-2 of molybdenum disulfide, 7-8.5 of aluminum, 4.5-5.5 of vanadium, 11-13 of molybdenum, 4-5 of chromium and 2-3 of an additive; the graphite is added in the raw materials, thus enhancing the wear resistance and lubricating property of an axle sleeve; the axle sleeve prepared from the composite metal material has compact structure, good microstructure, small porosity, and excellent structural stiffness, hardness, antifatigue performance and tensile strength; the composite metal material can be used for preparing automotive EFI pumps; and the composite metal material can be used for products having requirements on corrosion resistance, small residual magnetism, gas tightness and surface hardness, such as motorcycles, gasoline engines, diesel engines, and the like.

Description

Withstand voltage composite material of a kind of powder metallurgy and preparation method thereof
Technical field
The present invention relates to field of powder metallurgy, particularly withstand voltage composite material of a kind of powder metallurgy and preparation method thereof.
Background technology
Powder metallurgy be produce metal-powder or with metal-powder (or mixture of metal-powder and non-metal powder) as raw material, through being shaped and sintering, produce the industrial technology of metallic substance, matrix material and all kinds goods.At present, powder metallurgy technology has been widely used in the fields such as traffic, machinery, electronics, aerospace, weapons, biology, new forms of energy, information and nuclear industry, becomes one of branch of tool development vitality in novel material science.That powder metallurgy technology possesses is significantly energy-conservation, economize material, excellent performance, Product Precision is high and the series of advantages such as good stability, is very suitable for producing in enormous quantities.In addition, part material and the also available powder metallurgy technology manufacture of complicated shape that with conventional cast method and machining process, cannot prepare, thereby enjoy the attention of industry member.Powder metallurgy structural part product material composition is not limited by melting, both can add alloying constituent, can add other structural constituent yet, and adjusts as requested in sizable scope, and then can reach the effect of mating with steel part in mechanical property.
Powder metallurgy mechanization degree is high, can reduce personnel, can raise the efficiency again, so that cost-saving.Powder metallurgy technology can replace traditional manufacturing process, for the vast traditional forms of enterprises cost-saving.
The stainless steel of manufacturing with powder metallurgy process, it is a kind of mmaterial, can be made into steel or part.Its advantage is to reduce segregation, and refinement microstructure, improves performance, saves material, and energy efficient, reduces costs.
So study the formula of the powder metallurgy of various components of machine, adapt to different needs, have great importance.
Summary of the invention
The object of this invention is to provide withstand voltage composite material of a kind of powder metallurgy and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
Powder metallurgy is a withstand voltage composite material, is made by the raw material of following weight part: 316 Stainless Steel Powder 45-47, iron powder 50-54, graphite fibre 1-2, molybdenumdisulphide 1-2, aluminium 7-8.5, vanadium 4.5-5.5, molybdenum 11-13, chromium 4-5, auxiliary agent 2-3;
Described auxiliary agent is made by the raw material of following weight part: iron powder 30-34, bamboo charcoal 3-5, citric acid 2-3, nano titanium oxide 1-2, Silane coupling agent KH550 1-2, Z 250 3-4, potassium primary phosphate 1-2, Zinc Stearate 2-3, N220 carbon black 1-2, methyltrimethoxy silane 1-2; Preparation method mixes iron powder, bamboo charcoal, Z 250, potassium primary phosphate, N220 carbon black, grind to form 200-300 order powder, then add methyltrimethoxy silane to mix, under 10-15Mpa, be pressed into blank, then, send at 920-950 ℃ and calcine 3-4 hour, cooling after, be ground into 300-400 order powder, mix with other remaining component, be heated to 60-70 ℃, under 1200-1500 rev/min, stir 1-2 hour, obtain.
Powder metallurgy of the present invention is withstand voltage composite material, by following concrete steps, made:
(1) 316 Stainless Steel Powders, iron powder, aluminium, vanadium, molybdenum, chromium are mixed, add in suitable quantity of water, send into ball milling in ball mill, obtain 250-400 order powder, then, spraying is dry, oven dry, under 9-13Mpa pressure, is pressed into bulk, then under nitrogen protection atmosphere 650-750 ℃ carry out sintering 8-10 hour, will be after the crushing material after sintering cross 200-400 mesh sieve;
(2) other remaining component is mixed;
(3) at 60-65 ℃, after mixing and stirring 70-90 minute, pack step (1), (2) material into mould, be pressed into base;
(4) pressed compact is placed in sintering oven, with 6-8 ℃/min of speed, is warming up to sintering 2-3 hour under 800-850 ℃ of condition; Then with 5-7 ℃/min of speed, be warming up to sintering 2-3 hour under 1050-1150 ℃ of condition; To be cooled to 425-455 ℃ with 8-10 ℃/min of speed again, be incubated after 1.5-2 hour, in air, slow cooling is to room temperature again.
In raw material of the present invention, increase graphite, increased wear resistance and the oilness of axle sleeve, the axle sleeve dense structure of manufacture, microtexture is good, and seldom, structural rigidity, hardness, fatigue performance, tensile strength properties are good for hole; For the preparation of automobile electronic fuel oil jet pump, adjust cushion block, material of the present invention also can be used for motorcycle, petrol motor, diesel engine etc., and other have the product of requirement to corrosion-resistant, few remanent magnetism, resistance to air loss and surface hardness.
Specific embodiments
Below by specific examples, the present invention is described in detail.
Powder metallurgy is a withstand voltage composite material, by following weight part (kilogram) raw material make: 316 Stainless Steel Powders 45, iron powder 50, graphite fibre 1, molybdenumdisulphide 1, aluminium 7, vanadium 4.5, molybdenum 11, chromium 4, auxiliary agent 2;
Described auxiliary agent by following weight part (kilogram) raw material make: iron powder 30, bamboo charcoal 3, citric acid 2, nano titanium oxide 1, Silane coupling agent KH550 1, Z 250 3, potassium primary phosphate 1, Zinc Stearate 2, N220 carbon black 1, methyltrimethoxy silane 1; Preparation method mixes iron powder, bamboo charcoal, Z 250, potassium primary phosphate, N220 carbon black, grind to form 200-300 order powder, then add methyltrimethoxy silane to mix, under 10-15Mpa, be pressed into blank, then, send at 920-950 ℃ and calcine 3-4 hour, cooling after, be ground into 300-400 order powder, mix with other remaining component, be heated to 60-70 ℃, under 1200-1500 rev/min, stir 1-2 hour, obtain.
Powder metallurgy of the present invention is withstand voltage composite material, by following concrete steps, made:
(1) 316 Stainless Steel Powders, iron powder, aluminium, vanadium, molybdenum, chromium are mixed, add in suitable quantity of water, send into ball milling in ball mill, obtain 250-400 order powder, then, spraying is dry, oven dry, under 9-13Mpa pressure, is pressed into bulk, then under nitrogen protection atmosphere 650-750 ℃ carry out sintering 8-10 hour, will be after the crushing material after sintering cross 200-400 mesh sieve;
(2) other remaining component is mixed;
(3) at 60-65 ℃, after mixing and stirring 70-90 minute, pack step (1), (2) material into mould, be pressed into base;
(4) pressed compact is placed in sintering oven, with 6-8 ℃/min of speed, is warming up to sintering 2-3 hour under 800-850 ℃ of condition; Then with 5-7 ℃/min of speed, be warming up to sintering 2-3 hour under 1050-1150 ℃ of condition; To be cooled to 425-455 ℃ with 8-10 ℃/min of speed again, be incubated after 1.5-2 hour, in air, slow cooling is to room temperature again.
Through detection, hardness of the present invention: HRC89; Tensile strength: 830MPa.

Claims (2)

1. the withstand voltage composite material of powder metallurgy, it is characterized in that, by the raw material of following weight part, made: 316 Stainless Steel Powder 45-47, iron powder 50-54, graphite fibre 1-2, molybdenumdisulphide 1-2, aluminium 7-8.5, vanadium 4.5-5.5, molybdenum 11-13, chromium 4-5, auxiliary agent 2-3;
Described auxiliary agent is made by the raw material of following weight part: iron powder 30-34, bamboo charcoal 3-5, citric acid 2-3, nano titanium oxide 1-2, Silane coupling agent KH550 1-2, Z 250 3-4, potassium primary phosphate 1-2, Zinc Stearate 2-3, N220 carbon black 1-2, methyltrimethoxy silane 1-2; Preparation method mixes iron powder, bamboo charcoal, Z 250, potassium primary phosphate, N220 carbon black, grind to form 200-300 order powder, then add methyltrimethoxy silane to mix, under 10-15Mpa, be pressed into blank, then, send at 920-950 ℃ and calcine 3-4 hour, cooling after, be ground into 300-400 order powder, mix with other remaining component, be heated to 60-70 ℃, under 1200-1500 rev/min, stir 1-2 hour, obtain.
2. the withstand voltage composite material of powder metallurgy according to claim 1, is characterized in that, by following concrete steps, is made:
(1) 316 Stainless Steel Powders, iron powder, aluminium, vanadium, molybdenum, chromium are mixed, add in suitable quantity of water, send into ball milling in ball mill, obtain 250-400 order powder, then, spraying is dry, oven dry, under 9-13Mpa pressure, is pressed into bulk, then under nitrogen protection atmosphere 650-750 ℃ carry out sintering 8-10 hour, will be after the crushing material after sintering cross 200-400 mesh sieve;
(2) other remaining component is mixed;
(3) at 60-65 ℃, after mixing and stirring 70-90 minute, pack step (1), (2) material into mould, be pressed into base;
(4) pressed compact is placed in sintering oven, with 6-8 ℃/min of speed, is warming up to sintering 2-3 hour under 800-850 ℃ of condition; Then with 5-7 ℃/min of speed, be warming up to sintering 2-3 hour under 1050-1150 ℃ of condition; To be cooled to 425-455 ℃ with 8-10 ℃/min of speed again, be incubated after 1.5-2 hour, in air, slow cooling is to room temperature again.
CN201310469328.3A 2013-10-10 2013-10-10 A kind of Powder metallurgy pressure-resistant composite metal material and preparation method thereof Active CN103602902B (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105790481A (en) * 2016-05-17 2016-07-20 安徽旋利达电机有限公司 Pressure-resistant motor housing
CN105821280A (en) * 2016-04-28 2016-08-03 昌利锻造有限公司 Powder metallurgy tool steel for automobile gear shift fork
CN105970123A (en) * 2016-05-17 2016-09-28 安徽旋利达电机有限公司 Pressure resistant electric machinery rotor
CN107338384A (en) * 2017-06-16 2017-11-10 苏州莱特复合材料有限公司 A kind of preparation method of powder metallurgy automobile piston
CN107900325A (en) * 2017-11-23 2018-04-13 日照职业技术学院 A kind of Powder metallurgy pressure-resistant composite metal material and preparation method thereof
CN109930093A (en) * 2017-12-17 2019-06-25 宜兴安纳西智能机械设备有限公司 A kind of pole plate cleaning brush mill apparatus bowl-type brush material
CN114231854A (en) * 2021-11-22 2022-03-25 深圳市波尔顿科技有限公司 High-strength high-corrosion-resistance stainless steel for antibacterial cutter

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1947896A (en) * 2005-10-12 2007-04-18 日立粉末冶金株式会社 Method of manufacturing the anti-wear sintered member, sintered valve seat, and method of manufacturing the same
CN101107376A (en) * 2005-01-31 2008-01-16 株式会社小松制作所 Sintered material, iron-based sintered sliding material and process for producing the same, sliding member and process for producing the same, and connecting apparatus
CN102172775A (en) * 2005-10-12 2011-09-07 日立粉末冶金株式会社 Method of manufacturing sintered valve seat
CN103231061A (en) * 2013-03-30 2013-08-07 安徽省恒宇粉末冶金有限公司 Powder metallurgy synchronous wheel and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101107376A (en) * 2005-01-31 2008-01-16 株式会社小松制作所 Sintered material, iron-based sintered sliding material and process for producing the same, sliding member and process for producing the same, and connecting apparatus
CN1947896A (en) * 2005-10-12 2007-04-18 日立粉末冶金株式会社 Method of manufacturing the anti-wear sintered member, sintered valve seat, and method of manufacturing the same
CN102172775A (en) * 2005-10-12 2011-09-07 日立粉末冶金株式会社 Method of manufacturing sintered valve seat
CN103231061A (en) * 2013-03-30 2013-08-07 安徽省恒宇粉末冶金有限公司 Powder metallurgy synchronous wheel and preparation method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105821280A (en) * 2016-04-28 2016-08-03 昌利锻造有限公司 Powder metallurgy tool steel for automobile gear shift fork
CN105790481A (en) * 2016-05-17 2016-07-20 安徽旋利达电机有限公司 Pressure-resistant motor housing
CN105970123A (en) * 2016-05-17 2016-09-28 安徽旋利达电机有限公司 Pressure resistant electric machinery rotor
CN107338384A (en) * 2017-06-16 2017-11-10 苏州莱特复合材料有限公司 A kind of preparation method of powder metallurgy automobile piston
CN107900325A (en) * 2017-11-23 2018-04-13 日照职业技术学院 A kind of Powder metallurgy pressure-resistant composite metal material and preparation method thereof
CN109930093A (en) * 2017-12-17 2019-06-25 宜兴安纳西智能机械设备有限公司 A kind of pole plate cleaning brush mill apparatus bowl-type brush material
CN114231854A (en) * 2021-11-22 2022-03-25 深圳市波尔顿科技有限公司 High-strength high-corrosion-resistance stainless steel for antibacterial cutter

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Address before: 244131 Jinqiao Industrial Park, Tongling County, Tongling, Anhui

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