CN103599022A - Plumeria rubra toothpaste - Google Patents

Plumeria rubra toothpaste Download PDF

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Publication number
CN103599022A
CN103599022A CN201310588272.3A CN201310588272A CN103599022A CN 103599022 A CN103599022 A CN 103599022A CN 201310588272 A CN201310588272 A CN 201310588272A CN 103599022 A CN103599022 A CN 103599022A
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CN
China
Prior art keywords
toothpaste
flos plumeriae
plumeriae acutifoliae
plumeria rubra
stem
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Granted
Application number
CN201310588272.3A
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Chinese (zh)
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CN103599022B (en
Inventor
高诚伟
段柄荣
邱会昆
伍治平
龚云一
杜光明
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YUNNAN PULAMEI BIOLOGICAL SCIENCE & TECHNOLOGY DEVELOPMENT Co Ltd
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YUNNAN PULAMEI BIOLOGICAL SCIENCE & TECHNOLOGY DEVELOPMENT Co Ltd
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Priority to CN201310588272.3A priority Critical patent/CN103599022B/en
Publication of CN103599022A publication Critical patent/CN103599022A/en
Application granted granted Critical
Publication of CN103599022B publication Critical patent/CN103599022B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention relates to plumeria rubra toothpaste. The toothpaste comprises a toothpaste body, and is characterized by being prepared by the following steps: adding 0.2-5 mass percent of plumeria rubra stem extract and 0.05-1 mass percent of plumeria rubra essential oil into the toothpaste body; crushing and drying the plumeria rubra stems and leaves, and extracting with ethanol, recycling the ethanol, and degreasing, decolorizing and drying the extracting liquid to obtain plumeria rubra stem and leaf extract; distilling plumeria rubra petals with vapor to extract plumeria rubra essential oil, or extracting with a low-boiling-point hydrocarbon solvent, volatilizing the solvent at a temperature of 10-60 DEG C to obtain the plumeria rubra essential oil. The toothpaste is wide in raw material source, safe without side effect, has the effects of resisting inflammation, bacteria and allergy, plays effects of preventing and treating oral diseases and oral hygiene, and has good taste due to the unique fragrance of the plumeria rubra essential oil.

Description

Flos Plumeriae Acutifoliae toothpaste
Technical field
The present invention relates to toothpaste technical field, specifically a kind of Flos Plumeriae Acutifoliae toothpaste.
Background technology
Toothpaste variety and effect are in the market various, and the articles for daily use in the cleaning teeth oral cavity that toothpaste is each family daily life must be used, must brush teeth 1-2 time for each person every day, be long-term consumable products, be widely used in each family, hotel, school, armies etc., the place that every people of having lives, just needs toothpaste.Adopt different raw materials make or had much with the toothpaste of additive, various medicated toothpaste are different for the effect of human body and oral disease.But the application there is not yet the medicated toothpaste that adds natural plants Flos Plumeriae Acutifoliae before proposing.
Summary of the invention
In order to widen the raw material of making toothpaste, improve prevention and treatment oral disease and mouthfeel, the invention provides a kind of Flos Plumeriae Acutifoliae toothpaste, it is characterized in that adding stem and leaf ethanol extraction and the Flos Plumeriae Acutifoliae quintessence oil of Flos Plumeriae Acutifoliae in the mastic of toothpaste.Technical scheme of the present invention is as follows:
A Flos Plumeriae Acutifoliae toothpaste, comprises lotion of toothpaste, it is characterized in that, in the mastic of toothpaste, by mass percent, adds 0.2-5% Flos Plumeriae Acutifoliae stem and leaf extract and 0.05-1% Flos Plumeriae Acutifoliae quintessence oil; By Flos Plumeriae Acutifoliae stem and leaf pulverize, dry after with ethanol extraction, reclaim extracting solution after ethanol through defat, except color, dry, obtain described Flos Plumeriae Acutifoliae stem and leaf extract; Flos Plumeriae Acutifoliae petal is obtained to Flos Plumeriae Acutifoliae quintessence oil with vapor distillation, or with low boiling point hydrocarbon solvent extraction and after solvent evaporates at 10-60 ℃ of temperature, obtain described Flos Plumeriae Acutifoliae quintessence oil.
As further preferred technical scheme: add Flos Plumeriae Acutifoliae stem and leaf extract 3% and 0.5% Flos Plumeriae Acutifoliae quintessence oil by mass percent in the mastic of toothpaste.
Flos Plumeriae Acutifoliae, calls remote Fructus Gardeniae, egg yolk flower, Daji Hua, India jasmine, and the end of the branch of remote Cape jasmine is blunt round end, and one to winter, and leaf falls after light, the bare apperance just as Cornu Cervi, and therefore remote Cape jasmine is called again " Cornu Cervi tree ".Mainly be distributed in the ground such as Guangdong, Guangxi, Yunnan, Fujian of South America, Mexico, subtropical zone, Tropical Asian and China's Mainland, at present by artificial introducing and planting.The Flos Plumeriae Acutifoliae raw material sources of making toothpaste are extensive.
In the spending of Flos Plumeriae Acutifoliae containing plumieric acid, glycoside and volatile oil; In peel of stem, contain plumieride (C 21h 26o 12); In Flos Plumeriae Acutifoliae root, contain plumericin, isoplumericin, brown plumericin, β-dihydroplumericin, β-dihydroplumericinic acid; In its leaf, contain flavonoid glycoside, kaempferol glycoside, quercetin glucoside; And in milk containing lupeol.
The extract of Flos Plumeriae Acutifoliae has antiinflammatory, antibacterial and antiallergic, bring down a fever and the effect of paroxysmal pain, and oral disease and oral hygiene are had to preventive and therapeutic action; Flos Plumeriae Acutifoliae quintessence oil has distinctive fragrance, in prevention and treatment oral disease, also can improve toothpaste mouthfeel.
The product that adopts the present invention to make, safety has no side effect, and has antiinflammatory, antibacterial and antianaphylactic effect, oral disease and oral hygiene are had to preventive and therapeutic action, and the peculiar odor type of Flos Plumeriae Acutifoliae quintessence oil can allow toothpaste mouthfeel better.
The specific embodiment
Embodiment 1
Moisture content is pulverized, is dried to Flos Plumeriae Acutifoliae stem and leaf and lower than 10% rear use 60% concentration ethanol, extract 40-60 minute, extracting solution reclaim ethanol by defat, except color, after dry Flos Plumeriae Acutifoliae stem and leaf extract.
Flos Plumeriae Acutifoliae petal adopts steam distillation directly to obtain Flos Plumeriae Acutifoliae quintessence oil, or uses low boiling hydrocarbon kind solvent as extractions such as pentane or hexanes on Flos Plumeriae Acutifoliae flower petal, and through obtaining Flos Plumeriae Acutifoliae quintessence oil after solvent evaporates at 10-60 ℃ of temperature.
By the mastic mass percent of toothpaste, the consumption of Flos Plumeriae Acutifoliae stem and leaf extract is 3%, Flos Plumeriae Acutifoliae quintessence oil consumption is 0.5%, add appropriate surfactant, wetting agent, abrasivus, binding agent, sweeting agent and other composition and be prepared into lotion of toothpaste, vacuum filling in dentifrice tube, quality inspection, packing.
Embodiment 2
Processing technology, according to embodiment 1, is only adjusted into 0.5% by the consumption of Flos Plumeriae Acutifoliae stem and leaf extract, and Flos Plumeriae Acutifoliae quintessence oil consumption is 0.35%.
Embodiment 3
Processing technology, according to embodiment 1, is only adjusted into 0.2% by the consumption of Flos Plumeriae Acutifoliae stem and leaf extract, and Flos Plumeriae Acutifoliae quintessence oil consumption is 0.1%.
Embodiment 4
Processing technology, according to embodiment 1, is only adjusted into 95% concentration ethanol by the extraction solvent of Flos Plumeriae Acutifoliae stem and leaf extract, and other is constant.

Claims (2)

1. a Flos Plumeriae Acutifoliae toothpaste, comprises lotion of toothpaste, it is characterized in that, in the mastic of toothpaste, by mass percent, adds 0.2-5% Flos Plumeriae Acutifoliae stem and leaf extract and 0.05-1% Flos Plumeriae Acutifoliae quintessence oil; By Flos Plumeriae Acutifoliae stem and leaf pulverize, dry after with ethanol extraction, reclaim extracting solution after ethanol through defat, except color, dry, obtain described Flos Plumeriae Acutifoliae stem and leaf extract; Flos Plumeriae Acutifoliae petal is obtained to Flos Plumeriae Acutifoliae quintessence oil with vapor distillation, or with low boiling point hydrocarbon solvent extraction and after solvent evaporates at 10-60 ℃ of temperature, obtain described Flos Plumeriae Acutifoliae quintessence oil.
2. a kind of Flos Plumeriae Acutifoliae toothpaste according to claim 1, is characterized in that, in the mastic of toothpaste, by mass percent, adds Flos Plumeriae Acutifoliae stem and leaf extract 3% and 0.5% Flos Plumeriae Acutifoliae quintessence oil.
CN201310588272.3A 2013-11-21 2013-11-21 Plumeria rubra toothpaste Expired - Fee Related CN103599022B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310588272.3A CN103599022B (en) 2013-11-21 2013-11-21 Plumeria rubra toothpaste

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Application Number Priority Date Filing Date Title
CN201310588272.3A CN103599022B (en) 2013-11-21 2013-11-21 Plumeria rubra toothpaste

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CN103599022A true CN103599022A (en) 2014-02-26
CN103599022B CN103599022B (en) 2015-11-25

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104622739A (en) * 2015-01-12 2015-05-20 德利宝(广州)香料有限公司 Toothpaste containing plumeria rubra extract essence and preparation method of toothpaste
CN105476938A (en) * 2016-02-01 2016-04-13 东莞品派实业投资有限公司 Chinese medicinal toothpaste and preparation method thereof
CN107467177A (en) * 2017-09-25 2017-12-15 广西壮族自治区农业科学院农产品加工研究所 A kind of longan seed essential oil fresh applied to dragon fruit and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102961414A (en) * 2012-12-17 2013-03-13 重庆市中药研究院 Chinese herbal medicine raw stock and application thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102961414A (en) * 2012-12-17 2013-03-13 重庆市中药研究院 Chinese herbal medicine raw stock and application thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
芳香园AROMA GARDEN: "稀有精油作用简介", 《HTTP://BLOG.SINA.COM.CN/S/BLOG_499283010101F8H3.HTML》, 16 December 2012 (2012-12-16), pages 1 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104622739A (en) * 2015-01-12 2015-05-20 德利宝(广州)香料有限公司 Toothpaste containing plumeria rubra extract essence and preparation method of toothpaste
CN105476938A (en) * 2016-02-01 2016-04-13 东莞品派实业投资有限公司 Chinese medicinal toothpaste and preparation method thereof
CN107467177A (en) * 2017-09-25 2017-12-15 广西壮族自治区农业科学院农产品加工研究所 A kind of longan seed essential oil fresh applied to dragon fruit and preparation method thereof
CN107467177B (en) * 2017-09-25 2020-10-27 广西壮族自治区农业科学院农产品加工研究所 Longan seed essential oil preservative applied to dragon fruits and preparation method thereof

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