CN103589345B - A kind of fire prevention bonded adhesives and production technique thereof - Google Patents
A kind of fire prevention bonded adhesives and production technique thereof Download PDFInfo
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- CN103589345B CN103589345B CN201210289899.4A CN201210289899A CN103589345B CN 103589345 B CN103589345 B CN 103589345B CN 201210289899 A CN201210289899 A CN 201210289899A CN 103589345 B CN103589345 B CN 103589345B
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- degrees celsius
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Abstract
The present invention relates to a kind of production technique of prevent fires bonded adhesives and fire prevention bonded adhesives, comprise water glass, borax, Xylo-Mucine, aluminum oxide powder, silica powder, it is characterized in that: also comprise tripoly phosphate sodium STPP and white sugar and rare earth, its quality proportioning is: water glass 73%, white sugar 10%, tripoly phosphate sodium STPP 0.5%, borax 1%, Xylo-Mucine 0.5%, aluminum oxide powder 12%, rare earth 2%, silica powder 1%.The invention has the advantages that: (1) combustionproperty reaches national fire safety standard, burning-point 1200 degrees Celsius and more than.(2) cost is low, profitable, greatly reduces than other fire prevention bonded adhesives material costs.(3) in production process without the need to coal combustion, three-waste free discharge, energy-saving and water-saving.
Description
Technical field
The invention belongs to chemical field, is exactly a kind of fire prevention bonded adhesives and production technique thereof specifically.
Background technology
Containing organic materials in the raw materials for production of fireproof bonding glue in the market, in use can produce black smoke, can damage the health of people; Such as, be in the patent of CN101195735A at notification number, it makes fire prevention bonded adhesives and contains the organic materialss such as resol, epoxy resin, phenylenediamine, and its burning-point is only at 500 degrees Celsius.Some organic materialss itself have boiling characteristics, all can affect the health of human body, cause detrimentally affect, in addition, also do not meet the regulation of fire service law to surrounding environment in production and use procedure afterwards.General interpolation inorganic materials can affect the adhesive property of assembly glue, and duration of service, length easily came off; Also can affect fireproof bonding glue and obtain curing speed, and the characteristic of acidproof alkali salt.
Summary of the invention
The present invention in order to solve existing Waterproof gum not environmentally, the problem of adhesiveproperties difference, provide a kind of smokeless, nontoxic, nonflammable fire prevention bonded adhesives, the technical scheme of employing is:
A kind of fire prevention bonded adhesives, comprise water glass, borax, Xylo-Mucine, aluminum oxide powder, silica powder, it is characterized in that: also comprise tripoly phosphate sodium STPP and white sugar and rare earth, its quality proportioning is: water glass 73%, white sugar 10%, tripoly phosphate sodium STPP 0.5%, borax 1%, Xylo-Mucine 0.5%, aluminum oxide powder 12%, rare earth 2%, silica powder 1%.
To prevent fires the production technique of caking agent glue, first used by Xylo-Mucine 90 degrees Celsius of hot-water soaks 24 hours stand-by in advance.Water glass, white sugar, tripoly phosphate sodium STPP, borax, rare earth, silica powder being added in proportion band stirs in heating in water bath for reaction device, and heat up and stir, temperature controls at 100 degrees Celsius, and constant temperature starts to be cooled to 80 degrees Celsius for 2 hours.Add carboxymethylcellulose sodium solution, constant temperature stirs 30 minutes, is cooled to 40 degrees Celsius and adds aluminum oxide powder, stirs 30 minutes, discharging, sieves, packs.
The invention has the advantages that: (1) combustionproperty reaches national fire safety standard, burning-point 1200 degrees Celsius and more than.(2) cost is low, profitable, greatly reduces than other fire prevention bonded adhesives material costs.(3) in production process without the need to coal combustion, three-waste free discharge, energy-saving and water-saving.(4) nontoxic, smokeless, tasteless, belong to " environmental protection bonded adhesives ".(5) white sugar can help water glass to dewater after heating, and improves concentration and the degree of adhesion of Waterproof gum.(6) tripoly phosphate sodium STPP adding trace here plays the effect of dispersion, strengthens homogeneity and the mobility of gluing.
Specific embodiment
A kind of fire prevention bonded adhesives, comprise water glass, borax, Xylo-Mucine, aluminum oxide powder, it is characterized in that: also comprise tripoly phosphate sodium STPP, white sugar and rare earth, its quality proportioning is: water glass 73%, white sugar 10%, tripoly phosphate sodium STPP 0.5%, borax 1%, Xylo-Mucine 0.5%, aluminum oxide powder 12%, rare earth 2%, silica powder 1%.
To prevent fires the production technique of caking agent glue, first used by Xylo-Mucine 90 degrees Celsius of hot-water soaks 24 hours stand-by in advance.Water glass, white sugar, tripoly phosphate sodium STPP, borax, rare earth, silica powder being added in proportion band stirs in heating in water bath for reaction device, and heat up and stir, temperature controls at 100 degrees Celsius, and constant temperature starts to be cooled to 80 degrees Celsius for 2 hours.Add carboxymethylcellulose sodium solution, constant temperature stirs 30 minutes, is cooled to 40 degrees Celsius and adds aluminum oxide powder, stirs 30 minutes, discharging, sieves, packs.
The above; it is only the specific embodiment of the present invention; but the protection domain of invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with claims limited range.
Claims (2)
1. a fire prevention bonded adhesives, comprise water glass, borax, Xylo-Mucine, aluminum oxide powder, silica powder, it is characterized in that: also comprise tripoly phosphate sodium STPP, white sugar and rare earth, its quality proportioning is: water glass 73%, white sugar 10%, tripoly phosphate sodium STPP 0.5%, borax 1%, Xylo-Mucine 0.5%, aluminum oxide powder 12%, rare earth 2%, silica powder 1%.
2. utilize claim 1 to prepare a production technique for fire prevention caking agent glue, it is characterized in that: first used by Xylo-Mucine 90 degrees Celsius of hot-water soaks 24 hours stand-by in advance; Water glass, white sugar, tripoly phosphate sodium STPP, borax, rare earth, silica powder being added in proportion band stirs in heating in water bath for reaction device, and heat up and stir, temperature controls at 100 degrees Celsius, and constant temperature starts to be cooled to 80 degrees Celsius for 2 hours; Add carboxymethylcellulose sodium solution, constant temperature stirs 30 minutes, is cooled to 40 degrees Celsius and adds aluminum oxide powder, stirs 30 minutes, discharging, sieves, packs.
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CN201210289899.4A CN103589345B (en) | 2012-08-15 | 2012-08-15 | A kind of fire prevention bonded adhesives and production technique thereof |
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CN201210289899.4A CN103589345B (en) | 2012-08-15 | 2012-08-15 | A kind of fire prevention bonded adhesives and production technique thereof |
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CN103589345A CN103589345A (en) | 2014-02-19 |
CN103589345B true CN103589345B (en) | 2015-08-19 |
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CN201210289899.4A Expired - Fee Related CN103589345B (en) | 2012-08-15 | 2012-08-15 | A kind of fire prevention bonded adhesives and production technique thereof |
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2646969A1 (en) * | 1976-10-18 | 1978-04-20 | Woellner Werke | Water glass adhesive for bonding paper - contg. sugar for more rapid wetting without fraying |
CN1464015A (en) * | 2002-06-04 | 2003-12-31 | 沈忠善 | Multifunctional composite granule high temperature glue and method for making same |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0832111A (en) * | 1994-07-14 | 1996-02-02 | Omron Corp | Semiconductor light emitting element as well as light emitting device, photodetector, optical information processor, and photocoupler utilizing the element |
CN101426872B (en) * | 2007-02-15 | 2011-08-31 | 中国科学院过程工程研究所 | High temperature resistant inorganic composite adhesive |
-
2012
- 2012-08-15 CN CN201210289899.4A patent/CN103589345B/en not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2646969A1 (en) * | 1976-10-18 | 1978-04-20 | Woellner Werke | Water glass adhesive for bonding paper - contg. sugar for more rapid wetting without fraying |
CN1464015A (en) * | 2002-06-04 | 2003-12-31 | 沈忠善 | Multifunctional composite granule high temperature glue and method for making same |
Non-Patent Citations (1)
Title |
---|
丁志平."无机胶黏剂".《精细化工概论》.化学工业出版社,2011,第125-126页. * |
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