CN103558317A - Balance gas equipressure transfer device and method applied to preparation process of transformer oil chromatographic analysis standard oil - Google Patents

Balance gas equipressure transfer device and method applied to preparation process of transformer oil chromatographic analysis standard oil Download PDF

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Publication number
CN103558317A
CN103558317A CN201310511599.0A CN201310511599A CN103558317A CN 103558317 A CN103558317 A CN 103558317A CN 201310511599 A CN201310511599 A CN 201310511599A CN 103558317 A CN103558317 A CN 103558317A
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China
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standard oil
preparation
cylinder
oil
solenoid valve
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CN201310511599.0A
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CN103558317B (en
Inventor
朱洪斌
余翔
张建国
陈大兵
刘建军
李成钢
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State Grid Corp of China SGCC
State Grid Jiangsu Electric Power Co Ltd
Electric Power Research Institute of State Grid Jiangsu Electric Power Co Ltd
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State Grid Corp of China SGCC
State Grid Jiangsu Electric Power Co Ltd
Electric Power Research Institute of State Grid Jiangsu Electric Power Co Ltd
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Abstract

The invention discloses a balance gas equipressure transfer device and method applied to a preparation process of transformer oil chromatographic analysis standard oil. The balance gas equipressure transfer device comprises a standard oil preparation tank, a first air cylinder and a second air cylinder, wherein the two air cylinders are both provided with linear motors; control circuits of the air cylinders are provided with a plurality of electromagnetic valves which can be switched on and off randomly; the first air cylinder is used for preparing the standard oil; the second air cylinder is used for transferring a balance gas; the bottom in the standard oil preparation tank is provided with an air bag; the standard oil is arranged above the air bag; the balance gas is arranged above the standard oil. The balance gas equipressure transfer method applied to the preparation process of transformer oil chromatographic analysis standard oil solves the difficulty of concentration change of prepared standard oil, which is caused by the fact that oil and gas balance is easily damaged by balance gas transfer during the preparation process of transformer oil chromatographic analysis standard oil. The standard oil prepared by the method has the characteristics of accurate target concentration, high stability and the like.

Description

The isobaric transfer device of Balance Air and method thereof in Chromatographic Analysis of Transformer oil standard oil process for preparation
Technical field
The present invention relates to the isobaric transfer device of Balance Air and method thereof in a kind of Chromatographic Analysis of Transformer oil standard oil process for preparation.Belong to electric system field of mechanical technique.
Background technology
When the Balance Air in Chromatographic Analysis of Transformer oil standard oil process for preparation shifts at present, because easily causing gas back dissolving, Balance Air, various factors shifts the phenomenons such as incomplete, the standard oil making is like this concentration meeting distortion not only, and stability is relatively poor, cannot be for a long time for Chromatographic Analysis of Transformer oil.In power industry nowadays, in the more and more important situation of Chromatographic Analysis of Transformer oil, prepare true, accurate, believable Chromatographic Analysis of Transformer oil standard oil necessary.
Summary of the invention
Technical matters to be solved by this invention is to provide the isobaric transfer device of Balance Air and method thereof in a kind of Chromatographic Analysis of Transformer oil standard oil process for preparation.
For solving the problems of the technologies described above, the invention provides the isobaric transfer device of Balance Air in a kind of Chromatographic Analysis of Transformer oil standard oil process for preparation, comprise standard oil preparation fuel tank, the first cylinder, the second cylinder, described two cylinders are all with linear electric motors, arrange somely can carry out arbitrarily the solenoid valve of opening and closing operations on the operation circuit of described two cylinders; Described the first cylinder is for standard oil preparation, and described the second cylinder shifts for balanced gas; Described standard oil preparation fuel tank inner bottom part is installed air bag, and described air bag top is standard oil, and standard oil top is Balance Air.
Above-mentioned standard oil preparation top of oil-tank setting pressure sensor.
Above-mentioned solenoid valve has four, is respectively solenoid valve one, solenoid valve two, solenoid valve three, solenoid valve four; Described solenoid valve two one end connect Balance Air, and solenoid valve three one end connect the first cylinder, after the other end of solenoid valve two and solenoid valve three collects, are connected to the second cylinder; Described solenoid valve four one end connect air bag, and the other end connects the second cylinder; Two operation circuits that described the second cylinder connects are a solenoid valve one in parallel in its port.
The volume of above-mentioned the second cylinder equals the volume of standard oil preparation fuel tank inner equilibrium gas.
In standard oil process for preparation, the isobaric transfer method of Balance Air, utilizes said apparatus, comprises the following steps:
1) preparation of standard oil: device carries out the preparation of Chromatographic Analysis of Transformer oil standard oil according to the pressure of setting by the first cylinder in standard oil preparation fuel tank, pressure transducer can show actual preparation pressure, and air bag can be used to carry out preparation pressure adjusting in standard oil process for preparation;
2) Balance Air shifts: under preparation pressure state, carry out balanced gas transfer after oil gas dissolution equilibrium, during transfer, first only open solenoid valve one, piston nose in the second cylinder is close to cylinder wall, then shut electromagnetic valve one, open solenoid valve two, solenoid valve four, the Balance Air that pulls piston that standard oil is prepared in fuel tank is slowly transferred to the second cylinder, in transfer process, piston gas below supplements the air bag in fuel tank simultaneously, because the volume of the second cylinder equals the volume of standard oil preparation fuel tank inner equilibrium gas, when piston moves to the second cylinder end, Balance Air in standard oil preparation fuel tank is also transferred in the second cylinder completely, Balance Air shifts complete, whole process is all carried out under isopiestic state.
The beneficial effect that the present invention reaches:
In Chromatographic Analysis of Transformer oil standard oil process for preparation of the present invention, Balance Air isobaric transfer method has changed the transfer method of Balance Air in standard oil process for preparation in the past, has adopted isobaric transfer.In Chromatographic Analysis of Transformer oil standard oil process for preparation of the present invention, the isobaric transfer method of Balance Air has solved in Chromatographic Analysis of Transformer oil standard oil process for preparation the difficult point of easily destroying gas and oil equilibration when Balance Air shifts and causing joined standard oil concentration to change.Avoid the gas back dissolving, the Balance Air that in Balance Air transfer process, occur to shift the phenomenons such as incomplete, guaranteed the Stability and veracity of standard oil concentration, for Chromatographic Analysis of Transformer oil provides reliable foundation.When Chromatographic Analysis of Transformer oil is important all the more, make chromatographic data have rule to follow, also further for the safe operation of electrical equipment provides sound assurance.
Accompanying drawing explanation
Fig. 1 is the structural representation of device of the present invention.
Embodiment
Below in conjunction with accompanying drawing, the present invention is further illustrated.
As shown in Figure 1, the isobaric transfer device of Balance Air in a kind of Chromatographic Analysis of Transformer oil standard oil process for preparation, comprise standard oil preparation fuel tank 1, the first cylinder 8, the second cylinder 9, two cylinders are all with linear electric motors, arrange somely can carry out arbitrarily the solenoid valve of opening and closing operations on the operation circuit of two cylinders; The first cylinder 8 is for standard oil preparation, and the second cylinder 9 shifts for balanced gas; Standard oil preparation fuel tank 1 inner bottom part is installed air bag 2, and air bag 2 tops are standard oils, and standard oil top is Balance Air.
Standard oil preparation fuel tank 1 top setting pressure sensor 3.
Solenoid valve has four, is respectively solenoid valve 1, solenoid valve 25, solenoid valve 36, solenoid valve 47; Solenoid valve 25 one end connect Balance Air, and solenoid valve 36 one end connect the first cylinder 8, after the other end of solenoid valve 25 and solenoid valve 36 collects, are connected to the second cylinder 9; Solenoid valve 47 one end connect air bag 2, and the other end connects the second cylinder 9; Two operation circuits that the second cylinder 9 connects are a solenoid valve 1 in parallel in its port.
The volume of the second cylinder 9 equals the volume of standard oil preparation fuel tank 1 inner equilibrium gas.
In a kind of Chromatographic Analysis of Transformer oil standard oil process for preparation provided by the invention, the isobaric transfer method of Balance Air, utilizes said apparatus, comprises the following steps:
1) preparation of standard oil: device carries out the preparation of Chromatographic Analysis of Transformer oil standard oil according to the pressure (pressure-fired or micro-negative pressure) of setting by the first cylinder 8 in standard oil preparation fuel tank 1, pressure transducer 3 can show actual preparation pressure, and air bag 2 can be used to carry out preparation pressure adjusting in standard oil process for preparation;
2) Balance Air shifts: under preparation pressure state, carry out balanced gas transfer after oil gas dissolution equilibrium, during transfer, first only open solenoid valve 1, piston nose in the second cylinder 9 is close to cylinder wall, then shut electromagnetic valve 1, open solenoid valve 25, solenoid valve 47, the Balance Air that pulls piston that standard oil is prepared in fuel tank is slowly transferred to the second cylinder 9, in transfer process, piston gas below supplements the air bag 2 in fuel tank simultaneously, because the volume of the second cylinder 9 equals the volume of standard oil preparation fuel tank 1 inner equilibrium gas, when piston moves to the second cylinder 9 end, Balance Air in standard oil preparation fuel tank 1 is also transferred in the second cylinder 9 completely, Balance Air shifts complete, whole process is all carried out under isopiestic state.
Below with preferred embodiment, disclose the present invention, so it is not intended to limiting the invention, all take to be equal to replace or technical scheme that the scheme of equivalent transformation obtains, all drop in protection scope of the present invention.

Claims (5)

1. the isobaric transfer device of Balance Air in a Chromatographic Analysis of Transformer oil standard oil process for preparation, it is characterized in that: comprise standard oil preparation fuel tank, the first cylinder, the second cylinder, described two cylinders are all with linear electric motors, arrange somely can carry out arbitrarily the solenoid valve of opening and closing operations on the operation circuit of described two cylinders; Described the first cylinder is for standard oil preparation, and described the second cylinder shifts for balanced gas; Described standard oil preparation fuel tank inner bottom part is installed air bag, and described air bag top is standard oil, and standard oil top is Balance Air.
2. the isobaric transfer device of Balance Air in Chromatographic Analysis of Transformer oil standard oil process for preparation according to claim 1, is characterized in that: described standard oil preparation top of oil-tank setting pressure sensor.
3. the isobaric transfer device of Balance Air in Chromatographic Analysis of Transformer oil standard oil process for preparation according to claim 1, is characterized in that: described solenoid valve has four, is respectively solenoid valve one, solenoid valve two, solenoid valve three, solenoid valve four; Described solenoid valve two one end connect Balance Air, and solenoid valve three one end connect the first cylinder, after the other end of solenoid valve two and solenoid valve three collects, are connected to the second cylinder; Described solenoid valve four one end connect air bag, and the other end connects the second cylinder; Two operation circuits that described the second cylinder connects are a solenoid valve one in parallel in its port.
4. the isobaric transfer device of Balance Air in Chromatographic Analysis of Transformer oil standard oil process for preparation according to claim 1, is characterized in that: the volume of described the second cylinder equals the volume of standard oil preparation fuel tank inner equilibrium gas.
5. the isobaric transfer method of Balance Air in Chromatographic Analysis of Transformer oil standard oil process for preparation, is characterized in that utilizing the device described in claim 1-4, comprises the following steps:
1) preparation of standard oil: device carries out the preparation of Chromatographic Analysis of Transformer oil standard oil according to the pressure of setting by the first cylinder in standard oil preparation fuel tank, pressure transducer can show actual preparation pressure, and air bag can be used to carry out preparation pressure adjusting in standard oil process for preparation;
2) Balance Air shifts: under preparation pressure state, carry out balanced gas transfer after oil gas dissolution equilibrium, during transfer, first only open solenoid valve one, piston nose in the second cylinder is close to cylinder wall, then shut electromagnetic valve one, open solenoid valve two, solenoid valve four, the Balance Air that pulls piston that standard oil is prepared in fuel tank is slowly transferred to the second cylinder, in transfer process, piston gas below supplements the air bag in fuel tank simultaneously, because the volume of the second cylinder equals the volume of standard oil preparation fuel tank inner equilibrium gas, when piston moves to the second cylinder end, Balance Air in standard oil preparation fuel tank is also transferred in the second cylinder completely, Balance Air shifts complete, whole process is all carried out under isopiestic state.
CN201310511599.0A 2013-10-25 2013-10-25 Balance gas equipressure transfer device and method applied to preparation process of transformer oil chromatographic analysis standard oil Active CN103558317B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108014665A (en) * 2017-12-28 2018-05-11 国网安徽省电力公司电力科学研究院 Gas-liquid mixed distributing device
CN111453217A (en) * 2019-09-04 2020-07-28 国网四川省电力公司电力科学研究院 On-site inspection or calibration oil storage device and method for oil chromatography on-line monitoring device in high-altitude area

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003098165A (en) * 2001-09-27 2003-04-03 Hitachi Ltd Apparatus for producing standard oil for gas analyzing apparatus in transformer oil
CN1654952A (en) * 2004-02-13 2005-08-17 中国科学院大连化学物理研究所 Apparatus and method for measuring distribution constant of dissolved gas in transformer oil
CN101762641A (en) * 2010-01-08 2010-06-30 山东中惠仪器有限公司 Automatic volume displaced type vacuum degasser for transformer oil
CN201965045U (en) * 2010-12-16 2011-09-07 河南省中分仪器有限公司 Preparation device for standard oil sample of dissolved gas in transformer oil

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003098165A (en) * 2001-09-27 2003-04-03 Hitachi Ltd Apparatus for producing standard oil for gas analyzing apparatus in transformer oil
CN1654952A (en) * 2004-02-13 2005-08-17 中国科学院大连化学物理研究所 Apparatus and method for measuring distribution constant of dissolved gas in transformer oil
CN101762641A (en) * 2010-01-08 2010-06-30 山东中惠仪器有限公司 Automatic volume displaced type vacuum degasser for transformer oil
CN201965045U (en) * 2010-12-16 2011-09-07 河南省中分仪器有限公司 Preparation device for standard oil sample of dissolved gas in transformer oil

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108014665A (en) * 2017-12-28 2018-05-11 国网安徽省电力公司电力科学研究院 Gas-liquid mixed distributing device
CN108014665B (en) * 2017-12-28 2023-11-07 国网安徽省电力公司电力科学研究院 Gas-liquid mixed oil distributing device
CN111453217A (en) * 2019-09-04 2020-07-28 国网四川省电力公司电力科学研究院 On-site inspection or calibration oil storage device and method for oil chromatography on-line monitoring device in high-altitude area
CN111453217B (en) * 2019-09-04 2024-05-14 国网四川省电力公司电力科学研究院 Device and method for on-site inspection or calibration of oil storage device of oil chromatograph in high-altitude area

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Effective date of registration: 20151123

Address after: PA Weier road Jiangning District of Nanjing City, Jiangsu Province, No. 1 211103

Patentee after: Jiangou Provincial Power Test Inst Co., Ltd.

Patentee after: State Grid Corporation of China

Patentee after: Jiangsu Electric Power Company

Patentee after: Electric Power Research Institute of Jiangsu Electric Power Company

Address before: 100031 Xicheng District West Chang'an Avenue, No. 86, Beijing

Patentee before: State Grid Corporation of China

Patentee before: Jiangsu Electric Power Company

Patentee before: Electric Power Research Institute of Jiangsu Electric Power Company