CN103556462A - Antistatic finishing method for wool textiles - Google Patents
Antistatic finishing method for wool textiles Download PDFInfo
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- CN103556462A CN103556462A CN201310500269.1A CN201310500269A CN103556462A CN 103556462 A CN103556462 A CN 103556462A CN 201310500269 A CN201310500269 A CN 201310500269A CN 103556462 A CN103556462 A CN 103556462A
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Abstract
The invention relates to an antistatic finishing method for wool textiles and belongs to the field of textile processing. The antistatic finishing method for the wool textiles comprises the following steps: carrying out pre-treatment on wool textiles to be subjected to antistatic finishing by using gamma-mercaptopropyl triethoxy silane and carrying out the antistatic finishing after the pre-treatment. The pre-treatment process of the gamma-mercaptopropyl triethoxy silane changes a direct bonding manner of an antistatic agent and the surfaces of the wool textiles in a traditional process; wool fibers and the antistatic agent are connected to the two ends of the gamma-mercaptopropyl triethoxy silane which serves as a molecular bridge by a chemical condensation reaction, so that the bonding force of the interface is enhanced, and the antistatic performance and the washing resistance of the wool textiles are improved.
Description
Technical field
The method that the present invention relates to the antistatic finish of a kind of wool textile product, belongs to textile processing field.
Technical background
Wool textile product are clothes high-grade fabrics, because wool textile product have unique appearance style and good heat-preserving function is widely used it.Wool fibre is the fiber that hygroscopicity is very strong, but because wool surface scale layer has lipoid structure, hydrophobicity is large, easily produces static, has affected the use of wool textile product.The antistatic finish of wool textile product is the problem that wool industry is paid close attention to always, although there is in recent years certain progress, the wool textile product after arranging exist feel, hygroscopicity to change, and antistatic effect is subject to that ambient humidity affects greatly, the problem such as wash resistant not.
Open magazine < < textile science research > >, the 4th phase of calendar year 2001 publication date, name is called < < and improves in the theory of woolen anti-static function and Probe into effect > > and disclose the wool fabric of making blending with conductive fiber and fleece fibre blended spinning, the fabric antistatic effect of gained is remarkable, and good endurance.But its weak point is sneaking into of conductive fiber has changed the natural good hygroscopicity of wool textile product, soft premium properties.
Open magazine < < textile technology progress > >, the 2nd phase of 2006 publication dates, name is called in the processing method > > of < < antistatic spinning wool fabric and discloses in the soft process of rear arrangement and added appropriate nonionic surface active agent can reach certain antistatic effect, but less at the ambient humidity hydrone that hour fabric absorbs, the antistatic effect of non-ionic surface active agent declines very fast, and fabric is after repeatedly washing, antistatic property declines significantly, not lasting.
Open magazine < < textile journal > >, the 3rd phase of 2009 publication dates, name is called in the antistatic finish of < < wool fabric and influence factor > > thereof and discloses use both sexes antistatic agent treatment wool fabric, it is less that after processing, wool fabric antistatic effect is subject to the impact of humidity of environment, but because antistatic additive and fabric are directly bonding mode, do not form chemical bond, antistatic additive is combined insecure with fabric, after washing, antistatic property declines significantly, not lasting.
Open magazine < < wool spinning science and technology > >, at 2012 publication date o. 11th, name is called in < < wool fabric antistatic finish technique > > and discloses with shitosan cationic functional finishing agent wool fabric is carried out to antistatic finish, although wool fabric antistatic effect is remarkable after arranging by the method, but because shitosan and fabric be take the coated and Hydrogenbond of physics as main, fabric antistatic effect is wash resistant not.
Summary of the invention
For the problems referred to above, in order to increase the antistatic behaviour of wool textile product after antistatic finish and its washing resistance, the object of the present invention is to provide and a kind ofly can effectively to wool textile product, carry out the method for carrying out the pretreated antistatic finish of silane coupler with γ-mercapto propyl triethoxy before antistatic finish.
To achieve these goals, technical solution of the present invention is:
The method of a kind of wool textile product antistatic finish, comprise the immersion in the antistatic finish of wool textile product or the operation of padding antistatic additive, dry and baking, described method for sorting refers to that with gamma-mercaptopropyltriethoxysilane, treating the wool textile product of doing antistatic finish carries out preliminary treatment, after preliminary treatment is complete, carry out antistatic finish, pretreated method is to carry out according to the following steps again.
The preparation of a pretreatment fluid:
Gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 10-30g/L, wherein, the bath raio of pretreatment fluid is 1:10-1:50.
B treats the preliminary treatment of antistatic finish wool textile product:
To treat that antistatic finish wool textile product are placed in the pretreatment fluid of being prepared by a step and soak or pad, the liquid carrying rate for the treatment of antistatic finish wool textile product after soaking or padding is 80-100%.
C treats the oven dry of antistatic finish wool textile product:
To treat that antistatic finish wool textile product carry out drying and processing through b step is pretreated, wherein, bake out temperature is 80-100 ℃, and drying time is 3-6 min.
Described wool textile product are a kind of in loose wool fiber or wool top or wool yarn or wool fabric.
Described padding is to soak one roll or two soak two a kind of in rolling.
Owing to having adopted above technical scheme, technical characterstic of the present invention is: the present invention adopts and to treat the wool textile product of doing antistatic finish and carry out gamma-mercaptopropyltriethoxysilane preliminary treatment, mutually there is condensation reaction in gamma-mercaptopropyltriethoxysilane intermolecular meeting after hydrolysis, thereby at wool molecular surface, formed netted molecular film, the molecule fragment after each condensation contains sulfydryl and hydroxyl.Sulfydryl has the character of mercaptan or thiophenol, and Radical Addition easily occurs, can with the carboxyl reaction of wool fibre, simultaneously sulphur-hydrogen bond also can be combined by the sulfide linkage on wool fibre, so just on wool textile product surface, has formed one deck molecular film.When wool textile product are dried between the temperature of 80-100 ℃, sulphur-hydrogen bond can link together by chemical bond and wool textile product.Again by wool textile product after pretreatment through padding antistatic additive, dry and bake processing, this arrangement process just makes on gamma-mercaptopropyltriethoxysilane the hydroxyl after hydrolysis react with antistatic additive, with the mode combination of chemical bond.Whole chemical treating process process change the direct bonding mode of antistatic additive and wool in traditional handicraft, by the sulfydryl on the condensate of gamma-mercaptopropyltriethoxysilane condensation and hydroxyl respectively with wool and antistatic additive generation chemical reaction, the mode connecting by chemical bond has substituted the mode of traditional Hydrogenbond.The basic principle of the antistatic finish method of wool textile product of the present invention is by this molecular bridge of gamma-mercaptopropyltriethoxysilane, with chemical reaction, wool fibre and antistatic additive to be connected to its two ends, and the mode of connection is that chemical bond connects.The present invention has improved the adhesion at interface, has strengthened wool textile product antistatic effect and washing resistance thereof.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is specifically described.
The method of a kind of wool textile product antistatic finish, comprise the immersion in the antistatic finish of wool textile product or the operation of padding antistatic additive, dry and baking, described method for sorting refers to that with gamma-mercaptopropyltriethoxysilane, treating the wool textile product of doing antistatic finish carries out preliminary treatment, carries out antistatic finish again after preliminary treatment is complete.The method concrete steps of wool textile product antistatic finish are as follows:
The preparation of a pretreatment fluid:
Gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 10-30g/L, wherein, the bath raio of pretreatment fluid is 1:10-1:50.
B treats the preliminary treatment of antistatic finish wool textile product:
To treat that antistatic finish wool textile product are placed in the pretreatment fluid of being prepared by a step and soak or pad, the liquid carrying rate for the treatment of antistatic finish wool textile product after soaking or padding is 80-100%.Pad is to soak one roll or two soak two a kind of in rolling.Wool textile product are a kind of in loose wool fiber or wool top or wool yarn or wool fabric.
C treats the oven dry of antistatic finish wool textile product:
To treat that antistatic finish wool textile product carry out drying and processing through b step is pretreated, wherein bake out temperature is 80-100 ℃, and drying time is 3-6 min.
The preparation of d antistatic agent solution:
Antistatic additive is mixed with water, stir and be mixed with antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:10-1:50, and the concentration of antistatic agent solution is 20-40g/L.
The antistatic treatment of e wool textile product:
Wool textile product after c step process are placed in to the antistatic agent solution of being prepared by d step and soak or pad, the liquid carrying rate that soaks or pad rear wool textile product is 80-100%.Pad is to soak one roll or two soak two a kind of in rolling.
The oven dry of f wool textile product:
Wool textile product through e step process are carried out to drying and processing, and wherein, bake out temperature is 80-100 ℃, and drying time is 3-6 min.
Baking of g wool textile product:
Wool textile product through f step process are baked to processing, and wherein, baking temperature is 120-140 ℃, and the time of baking is 2-3 min.
Specific embodiment
Embodiment mono-:
By above-mentioned processing step: select wool fabric as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 10g/L, wherein, the bath raio of pretreatment fluid is 1:10.To treat that antistatic finish wool fabric is placed in pretreatment fluid two and soaks two and roll, two soak two treats that the liquid carrying rate of antistatic finish wool fabric is 80% after rolling.By pretreated, treat that antistatic finish wool fabric dries, bake out temperature is 80 ℃, and drying time is 6 min.Antistatic additive is mixed with water, stir and be mixed with 20g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:30.Pretreated wool fabric is placed in to antistatic agent solution two and soaks two and roll, two to soak two liquid carrying rates that roll rear wool fabric be 100%.By two, soak two wool fabrics that roll after processing and dry, bake out temperature is 80 ℃, and drying time is 6 min.Wool fabric after drying is baked, and baking temperature is 140 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.12 s, after washing, electrostatic half-life is 1.45 s.
Embodiment bis-:
By above-mentioned processing step: select wool fibre as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 30g/L, wherein, the bath raio of pretreatment fluid is 1:40.To treat that antistatic finish wool fibre is placed in pretreatment fluid and soaks 20 min, the liquid carrying rate for the treatment of antistatic finish wool fibre after immersion is 90%.By pretreated, treat that antistatic finish wool fibre dries, bake out temperature is 100 ℃, and drying time is 4 min.Antistatic additive is mixed with water, stir and be mixed with 30g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:30.Pretreated wool fibre is placed in to antistatic agent solution and soaks 20 min, after soaking, the liquid carrying rate of wool fibre is 80%.Wool fibre after immersion treatment is dried, and bake out temperature is 90 ℃, and drying time is 3 min.Wool fibre after drying is baked, and baking temperature is 140 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.02 s, after washing, electrostatic half-life is 1.12 s.
Embodiment tri-:
By above-mentioned processing step: select wool top as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 30g/L, wherein, the bath raio of pretreatment fluid is 1:20.To treat that antistatic finish wool top is placed in pretreatment fluid one and soaks one and roll, one soaks one treats that the liquid carrying rate of antistatic finish wool textile product is 80% after rolling.By pretreated, treat that antistatic finish wool top dries, bake out temperature is 100 ℃, and drying time is 6 min.Antistatic additive is mixed with water, stir and be mixed with 30g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:50.Pretreated wool top is placed in to antistatic agent solution one and soaks one and roll, one to soak a liquid carrying rate that rolls rear wool top be 80%.By one, soak a wool top rolling after processing and dry, bake out temperature is 100 ℃, and drying time is 6 min.Wool top after drying is baked, and baking temperature is 140 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.03 s, after washing, electrostatic half-life is 1.14 s
Embodiment tetra-:
By above-mentioned processing step: select wool yarn as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 30g/L, wherein, the bath raio of pretreatment fluid is 1:30.To treat that antistatic finish wool yarn is placed in pretreatment fluid and soaks 20 min, after soaking, the liquid carrying rate of wool yarn is 80%.By pretreated, treat that antistatic finish wool yarn dries, bake out temperature is 100 ℃, and drying time is 3 min.Antistatic additive is mixed with water, stir and be mixed with 40g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:20.Pretreated wool yarn is placed in to antistatic agent solution and soaks 20 min, after soaking, the liquid carrying rate of wool textile product is 80%.Wool yarn after immersion treatment is dried, and bake out temperature is 100 ℃, and drying time is 4 min.Wool yarn after drying is baked, and baking temperature is 140 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 0.98 s, after washing, electrostatic half-life is 1.04 s.
Embodiment five:
By above-mentioned processing step: select wool fabric as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 20g/L, wherein, the bath raio of pretreatment fluid is 1:10.To treat that antistatic finish wool fabric is placed in pretreatment fluid two and soaks two and roll, two soak two treats that the liquid carrying rate of antistatic finish wool fabric is 80% after rolling.By pretreated, treat that antistatic finish wool fabric dries, bake out temperature is 100 ℃, and drying time is 3 min.Antistatic additive is mixed with water, stir and be mixed with 20g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:50.Pretreated wool fabric is placed in to antistatic agent solution two and soaks two and roll, two to soak two liquid carrying rates that roll rear wool fabric be 100%.By two, soak two wool fabrics that roll after processing and dry, bake out temperature is 100 ℃, and drying time is 6 min.Wool fabric after drying is baked, and baking temperature is 140 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.04 s, after washing, electrostatic half-life is 1.13 s.
Embodiment six:
By above-mentioned processing step: select wool fibre as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 20g/L, wherein, the bath raio of pretreatment fluid is 1:40.To treat that antistatic finish wool fibre is placed in pretreatment fluid one and soaks one and roll, one soaks one treats that the liquid carrying rate of antistatic finish wool fibre is 80% after rolling.By pretreated, treat that antistatic finish wool fibre dries, bake out temperature is 80 ℃, and drying time is 5 min.Antistatic additive is mixed with water, stir and be mixed with 30g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:30.Pretreated wool fibre is placed in to antistatic agent solution one and soaks one and roll, one to soak a liquid carrying rate that rolls rear wool fibre be 100%.By two, soak two wool fibres that roll after processing and dry, bake out temperature is 80 ℃, and drying time is 5 min.Wool fibre after drying is baked, and baking temperature is 130 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.12, after washing, electrostatic half-life is 1.22 s.
Embodiment seven:
By above-mentioned processing step: select wool top as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 20g/L, wherein, the bath raio of pretreatment fluid is 1:20.To treat that antistatic finish wool top is placed in pretreatment fluid two and soaks two and roll, two soak two treats that the liquid carrying rate of antistatic finish wool top is 100% after rolling.By pretreated, treat that antistatic finish wool top dries, bake out temperature is 100 ℃, and drying time is 6 min.Antistatic additive is mixed with water, stir and be mixed with 40g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:30.Pretreated wool top is placed in to antistatic agent solution two and soaks two and roll, two to soak two liquid carrying rates that roll rear wool top be 80%.By two, soak two wool tops that roll after processing and dry, bake out temperature is 100 ℃, and drying time is 6 min.Wool top after drying is baked, and baking temperature is 140 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.15 s, after washing, the half-life is 1.23 s.
Embodiment eight:
By above-mentioned processing step: select wool yarn as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 30g/L, wherein, the bath raio of pretreatment fluid is 1:10.To treat that antistatic finish wool fabric is placed in pretreatment fluid and soaks 20 min, after soaking, the liquid carrying rate of wool yarn is 80%.The antistatic finish wool yarn for the treatment of after soaking is dried, and bake out temperature is 100 ℃, and drying time is 4 min.Antistatic additive is mixed with water, stir and be mixed with 20g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:20.Pretreated wool yarn is placed in to antistatic agent solution and soaks 20 min, after soaking, the liquid carrying rate of wool yarn is 80%.Wool yarn after immersion treatment is dried, and bake out temperature is 80 ℃, and drying time is 5 min.Wool yarn after drying is baked, and baking temperature is 120 ℃, and the time of baking is 2 min.
Result: wool textile product electrostatic half-life is 1.21 s, after washing, electrostatic half-life is 1.23 s.
Embodiment nine:
By above-mentioned processing step: select wool fabric as the wool textile product for the treatment of antistatic treatment, gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 20g/L, wherein, the bath raio of pretreatment fluid is 1:50.To treat that antistatic finish wool fabric is placed in pretreatment fluid two and soaks two and roll, two soak two treats that the liquid carrying rate of antistatic finish wool fabric is 100% after rolling.By pretreated, treat that antistatic finish wool fabric dries, bake out temperature is 90 ℃, and drying time is 6 min.Antistatic additive is mixed with water, stir and be mixed with 30g/L antistatic agent solution, wherein, the bath raio of antistatic agent solution is 1:50.Pretreated wool fabric is placed in to antistatic agent solution two and soaks two and roll, two to soak two liquid carrying rates that roll rear wool fabric be 90%.By two, soak two wool fabrics that roll after processing and dry, bake out temperature is 100 ℃, and drying time is 5 min.Wool fabric after drying is baked, and baking temperature is 120 ℃, and the time of baking is 3 min.
Result: wool textile product electrostatic half-life is 1.05 s, after washing, electrostatic half-life is 1.18 s.
Claims (3)
1. the method for wool textile product antistatic finish, comprise the immersion in the antistatic finish of wool textile product or the operation of padding antistatic additive, dry and baking, it is characterized in that: described method for sorting refers to that with gamma-mercaptopropyltriethoxysilane, treating the wool textile product of doing antistatic finish carries out preliminary treatment, after preliminary treatment, carry out antistatic finish, pretreated method is to carry out according to the following steps again;
The preparation of a pretreatment fluid:
Gamma-mercaptopropyltriethoxysilane is mixed with water, stir and be mixed with the pretreatment fluid that concentration is 10-30g/L, wherein, the bath raio of pretreatment fluid is 1:10-1:50;
B treats the preliminary treatment of antistatic finish wool textile product:
To treat that antistatic finish wool textile product are placed in the pretreatment fluid of being prepared by a step and soak or pad, the liquid carrying rate for the treatment of antistatic finish wool textile product after soaking or padding is 80-100%;
C treats the oven dry of antistatic finish wool textile product:
To treat that antistatic finish wool textile product carry out drying and processing through b step is pretreated, wherein, bake out temperature is 80-100 ℃, and drying time is 3-6 min.
2. the method for a kind of wool textile product as claimed in claim 1 antistatic finish, is characterized in that: described wool textile product are a kind of in loose wool fiber or wool top or wool yarn or wool fabric.
3. the method for a kind of wool textile product as claimed in claim 1 antistatic finish, is characterized in that: described padding is to soak one roll or two soak two a kind of in rolling.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103981722A (en) * | 2014-04-23 | 2014-08-13 | 桐乡市濮院毛针织技术服务中心 | Antistatic finishing method of wool blended fabric |
| CN106120200A (en) * | 2016-06-22 | 2016-11-16 | 武汉纺织大学 | Hydrophilic, the antistatic finish device of a kind of one side wool fabric and method for sorting |
| CN106637960A (en) * | 2016-12-30 | 2017-05-10 | 东华大学 | Durable flame-retardant finish method for cotton fabric based on ultraviolet light curing reaction |
| CN112482028A (en) * | 2020-11-28 | 2021-03-12 | 无锡市丹怡纺织品有限公司 | Preparation method of antistatic wool fabric |
| CN109537286B (en) * | 2018-12-14 | 2021-07-20 | 东华大学 | Durable hydrophilic finishing agent for wool fabric and preparation method and application thereof |
| CN115467163A (en) * | 2022-09-29 | 2022-12-13 | 淮阴工学院 | Preparation method of surface antistatic fiber fabric |
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| CN101660262A (en) * | 2009-09-27 | 2010-03-03 | 武汉科技学院 | Bridging type crease-resist finishing method for wool |
| CN102720053A (en) * | 2012-06-18 | 2012-10-10 | 太原理工大学 | Flame-retardant treatment method for wool fibers |
| CN103103753A (en) * | 2012-12-26 | 2013-05-15 | 北京市塑料研究所 | Method for surface treatment of fibers or fabric through coupling agent |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101660262A (en) * | 2009-09-27 | 2010-03-03 | 武汉科技学院 | Bridging type crease-resist finishing method for wool |
| CN102720053A (en) * | 2012-06-18 | 2012-10-10 | 太原理工大学 | Flame-retardant treatment method for wool fibers |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103981722A (en) * | 2014-04-23 | 2014-08-13 | 桐乡市濮院毛针织技术服务中心 | Antistatic finishing method of wool blended fabric |
| CN106120200A (en) * | 2016-06-22 | 2016-11-16 | 武汉纺织大学 | Hydrophilic, the antistatic finish device of a kind of one side wool fabric and method for sorting |
| CN106120200B (en) * | 2016-06-22 | 2018-10-19 | 武汉纺织大学 | A kind of the hydrophilic of single side wool fabric, antistatic finish device and method for sorting |
| CN106637960A (en) * | 2016-12-30 | 2017-05-10 | 东华大学 | Durable flame-retardant finish method for cotton fabric based on ultraviolet light curing reaction |
| CN109537286B (en) * | 2018-12-14 | 2021-07-20 | 东华大学 | Durable hydrophilic finishing agent for wool fabric and preparation method and application thereof |
| CN112482028A (en) * | 2020-11-28 | 2021-03-12 | 无锡市丹怡纺织品有限公司 | Preparation method of antistatic wool fabric |
| CN115467163A (en) * | 2022-09-29 | 2022-12-13 | 淮阴工学院 | Preparation method of surface antistatic fiber fabric |
| CN115467163B (en) * | 2022-09-29 | 2023-12-08 | 淮阴工学院 | Preparation method of surface antistatic fiber fabric |
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Application publication date: 20140205 |