CN103555103A - Novel environment-friendly thermal insulation anti-corrosive coating - Google Patents
Novel environment-friendly thermal insulation anti-corrosive coating Download PDFInfo
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Abstract
The invention discloses novel environment-friendly thermal insulation anti-corrosive coating. The novel environment-friendly thermal insulation anti-corrosive coating comprises a component A, a component B and a component C, wherein the weight ratio of the component A to the component B to the component C is (500-1000): (50-80): 2, the component A comprises the following materials in parts by weight: 40-50 parts of acrylic emulsion, 140-180 parts of titanium dioxide, 35-45 parts of lithopone, 5-8 parts of expanded perlite, 3-5 parts of hollow glass beads, 3-5 parts of vermiculite, 3-5 parts of sericite powder, 8-12 parts of epoxy resin, 12-18 parts of acetone, 3-8 parts of ethylene glycol monobutyl ether, 1-3 parts of commercially available OP-10 type emulsifier, 0.1-0.3 part of sodium hydroxide, 30-50 parts of ethanol and 70-100 parts of deionized water; the component B comprises the following materials in parts by weight: 3-5 parts of coating curing agent, 2-4 parts of tetrachloroisophthalonitrile, 1-2 parts of antifreeze agent, 0.3-0.8 part of defoaming agent, 0.1-0.15 parts of sterilizing agent, 0.1-0.4 part of dispersant, 1-1.5 parts of alkali swelling thickening agent, 0.1-0.2 part of cellulose thickener, 0.1-0.15 part of wetting agent and 0.5-1 part of film-forming agent; and the component C is ultramarine or phthalocyanine blue or phthalocyanine green or phthalocyanine red or bright red.
Description
Technical field
The present invention relates to a kind of new anti-corrosion coating and preparation method thereof, more particularly, relate to a kind of novel environment friendly heat-insulating anti-corrosive coating.
Background technology
In prior art, conventional skin coating is to be mostly coating prepared by base-material with vinylbenzene-ACRYLIC EMULSION, pure acrylic latex or elastomeric propylene yogurt liquid.Its shortcoming is to produce fine cracks after being applied to body of wall, puts forth effort poor, anti-pollution characteristic and poor performance at low temperatures etc.; In addition, owing to there is vinylbenzene in coating, be material, smell is quite dense; When exterior wall applies, smell distributes in a large number in atmosphere, has caused pollution; And the set time of such coating is relatively long, therefore, during coating, should be noted that Changes in weather, in the rainfall connecting, can not construct, therefore, there is larger limitation.Traditional solvent-borne type protective system can discharge a large amount of VOC, and living environment and people healthy had to potential threat.Enhancing gradually along with people's environmental consciousness, Environmental Protection in China general bureau has just promulgated < < water-borne coatings environmental labelling product technical requirements > > in 2002, the quantity discharged of restriction VOC, to reduce the pollution of coating to environment, thereby water-based anticorrosive paint becomes the focus of falling over each other research.Water-based anticorrosive paint is mainly to take water as solvent and dispersion agent, compares production and transportation safer with solvent-borne type protective system, does not contain or contains a small amount of solvent, and VOC burst size is extremely low, is applicable to indoor and outdoor environment.At present, water-based anticorrosive paint has almost reached the performance of solvent-borne type protective system.Water-based anticorrosive paint kind is a lot, mainly contains epoxy, vinylformic acid, inorganic zinc silicate and polyurethane coating etc., wherein industrialized aqueous epoxy coating and aqueous inorganic zinc-enriched coating, the water soluble acrylic acid coating of mainly containing of success.
Water soluble acrylic acid protective system membrane formation mechanism is complicated, and sticking power is slightly short of compared with water-base epoxy; Aqueous inorganic zinc silicate anti-corrosive paint requires too high to processing base level, and easily forms high density zinc salt while not using finish paint; Property of Waterborne Polyurethane is fine, but cost is higher.
Polystyrene (PS) is a kind of unformed simple linear polymer, having the characteristics such as heat insulation, sound insulation, shockproof, waterproof, acid and alkali-resistance, have the advantages such as light weight is attractive in appearance concurrently, is one of most widely used plastics in the world, and mostly be disposable use, with the rear waste product that becomes.And useless PS chemical property is more stable, has the features such as anticorrosive, ageing-resistant, at occurring in nature, be difficult for aging rotting, be difficult to natural degradation and be degraded by microorganisms, not affine by physical environment.Landfill and burning are that people process two kinds of conventional methods of discarded PS now.Yet these two kinds of methods can cause the wasting of resources and serious environmental problem, consequent a large amount of " white garbage " become a great problem of current environment protection.Therefore using discarded PS to produce water-based anticorrosive paint, is a kind of mode of production that has environmental benefit.
Consider above-mentioned practical situation, those skilled in the art is being devoted to study a kind of novel water corrosion-resistant epoxy paint always, replace existing solvent-borne type protective system, and simultaneously need have good sticking power, lower cost and better simply preparation method.
Summary of the invention
For the deficiency existing in prior art, the invention provides a kind of novel environment friendly heat-insulating anti-corrosive coating.
To achieve these goals, technical scheme of the present invention is as follows:
A heat-insulating anti-corrosive coating, consists of A component, B component and component C, in parts by weight, meets: component A: component B: component C=(500～1000): (50～80): 2; Wherein, component A counts by weight, includes following material and content: ACRYLIC EMULSION 40-50 part; Titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Component B, by by weight, includes following material and content: coating curing agent: 3～5 parts, daconil M: 2～4 parts; Antifreezing agent 1-2 part; Defoamer 0.3-0.8 part; Sterilant 0.1-0.15 part; Dispersion agent 0.1-0.4 part; Alkali swelling thickening material 1-1.5 part, cellulose thickener 0.1-0.2 part; Wetting agent 0.1-0.15 part; Film coalescence aid 0.5-1 part; Component C is that ultramarine or phthalocyanine blue or phthalein viridescent or the blue or green parts by weight red or bright red each raw material of phthalein are.
Described dispersion agent is that EFKA-5065 dispersion agent and EFKA-4050 dispersion agent are according to the mixture of 4:6; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 1:1.
Described defoamer and select respectively EFKA-2722 and EFKA-3239.
Described dispersion agent can be the polyphosphoric acid salt dispersant solution of 10% mass percent, and wherein poly refers to the compound of dimerization or trimerization or dimerization and trimerization; Described phosphoric acid salt refers to phosphide sodium or phosphide potassium or phosphide ammonium.
Described mould inhibitor is Sodium Fluoride or 10, the two phenoxazine arsenic of 10 '-oxo.
Described defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.
A method for described exterior wall water-borne protective system, it prepares by the following method:
The first step: make component A: first ratio takes ACRYLIC EMULSION 40-50 part by weight; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Mixture is heated to 75～85 ℃; Insulation is also stirred 1 hour simultaneously, obtains initial latex; Again by titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts add initial latex to stir to obtain A component emulsion together; Pack A component emulsion into the component A that gets product in packaging vessel;
Second step: make component B: ratio takes the various raw materials of component B mixing and stirring and packs container into and obtain finished product component B by weight;
The 3rd step: according to component A: component B: component C=(500～1000): (50～80): 2 weight ratio takes component C and inserts the component C that gets product in container; And rationally take in proportion component A and component B;
The 4th step: by the 3rd step, claim finished product component C insert in finished product component B, fully stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin coating.
The present invention compares with the skin coating of prior art, has following main beneficial effect:
Raw material variety is few, pollution-free, and making method is simple, and required equipment is few: without benzene, aldehydes matter, therefore pollution-free in the present invention, and basic odorlessness; Starting material in the present invention easily purchase and cost relatively low; In the present invention, only need once to heat, and carry out under normal pressure, therefore do not need complicated reactor, security improves greatly.
Set time is short, low for the requirement for environmental conditions applying: the present invention, through test, applies normally, when coating thickness is 1-3mm, within 12 hours, just reaches 95% degree of cure at 25 ℃; And existing coating needs just can reach for 36 hours 95% degree of cure; Be that existing coating is unsuitable for exterior wall coating in rainy season.
Fungicidal properties is excellent: product of the present invention is coated on the exterior wall that does not get sunlight of buildings, under the natural condition of 20-40 ℃ of outside air temperatures, for metope of the same area, spray identical tap water continuous every day, in 60 days, use and on skin of the present invention, do not see any mildew, and in prior art, used at random the exterior coating of 20 brands, there is mildew in various degree.
Therefore, the present invention has the beneficial effects such as pollution-free, making method is simple, required equipment is few, set time is short, low for the requirement for environmental conditions applying, fungicidal properties is excellent.
Embodiment
For more detailed elaboration the present invention, this one embodiment of the invention is as follows:
Embodiment 1
A heat-insulating anti-corrosive coating, consists of A component, B component and component C, in parts by weight, meets: component A: component B: component C=(500～1000): (50～80): 2; Wherein, component A counts by weight, includes following material and content: ACRYLIC EMULSION 40-50 part; Titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Component B, by by weight, includes following material and content: coating curing agent: 3～5 parts, daconil M: 2～4 parts; Antifreezing agent 1-2 part; Defoamer 0.3-0.8 part; Sterilant 0.1-0.15 part; Dispersion agent 0.1-0.4 part; Alkali swelling thickening material 1-1.5 part, cellulose thickener 0.1-0.2 part; Wetting agent 0.1-0.15 part; Film coalescence aid 0.5-1 part; Component C is that ultramarine or phthalocyanine blue or phthalein viridescent or the blue or green parts by weight red or bright red each raw material of phthalein are.
Described dispersion agent is that EFKA-5065 dispersion agent and EFKA-4050 dispersion agent are according to the mixture of 4:6; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 1:1.
Described defoamer and select respectively EFKA-2722 and EFKA-3239.
Described dispersion agent can be the polyphosphoric acid salt dispersant solution of 10% mass percent, and wherein poly refers to the compound of dimerization or trimerization or dimerization and trimerization; Described phosphoric acid salt refers to phosphide sodium or phosphide potassium or phosphide ammonium.
Described mould inhibitor is Sodium Fluoride or 10, the two phenoxazine arsenic of 10 '-oxo.
Described defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.
A method for described exterior wall water-borne protective system, it prepares by the following method:
The first step: make component A: first ratio takes ACRYLIC EMULSION 40-50 part by weight; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Mixture is heated to 75～85 ℃; Insulation is also stirred 1 hour simultaneously, obtains initial latex; Again by titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts add initial latex to stir to obtain A component emulsion together; Pack A component emulsion into the component A that gets product in packaging vessel;
Second step: make component B: ratio takes the various raw materials of component B mixing and stirring and packs container into and obtain finished product component B by weight;
The 3rd step: according to component A: component B: component C=(500～1000): (50～80): 2 weight ratio takes component C and inserts the component C that gets product in container; And rationally take in proportion component A and component B;
The 4th step: by the 3rd step, claim finished product component C insert in finished product component B, fully stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin coating.
The water corrosion-resistant epoxy paint that has adopted preparation method of the present invention to obtain, one of its key technical indexes, i.e. the Corrosion Protection of coating, as shown in the table:
| Sequence number | Interventions Requested | Technical requirements | Assay | Conclusion |
| 1 | Condition in container | Without lump, after stirring, be uniform state | Meet the requirements | Qualified |
| 2 | Smell | Tasteless | Meet the requirements | Qualified |
| 3 | Application property | Brush two roads accessible | Meet the requirements | Qualified |
| 4 | Low-temperature stability (20 ℃) | Never degenerate | Meet the requirements | Qualified |
| 5 | 25 ℃ of set times | ≤24h | 12h | Qualified |
| 6 | Appearance of film | Normally | Meet the requirements | Qualified |
| 7 | Water-fastness | 96h is without extremely | Meet the requirements | Qualified |
| 8 | Acid resistance | 48h is without extremely | Meet the requirements | Qualified |
| 9 | Abrasion resistance (inferior) | ≥500 | 2500 | Qualified |
| 10 | Midew proof | During humidity 40%, continuous 60 days without mildew | Without mildew | Qualified |
As can be seen from the above table, the coating preparing by method of the present invention, comparing other water-based anticorrosive paint has following advantage:
1. higher to the sticking power of base material;
2. the chemical-resistant of filming is better;
3. can mix use with other waterborne polymeric, complementary in performance;
Embodiment 2
A heat-insulating anti-corrosive coating, consists of A component, B component and component C, in parts by weight, meets: component A: component B: component C=(500～1000): (50～80): 2; Wherein, component A counts by weight, includes following material and content: ACRYLIC EMULSION 40-50 part; Titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Component B, by by weight, includes following material and content: coating curing agent: 3～5 parts, daconil M: 2～4 parts; Antifreezing agent 1-2 part; Defoamer 0.3-0.8 part; Sterilant 0.1-0.15 part; Dispersion agent 0.1-0.4 part; Alkali swelling thickening material 1-1.5 part, cellulose thickener 0.1-0.2 part; Wetting agent 0.1-0.15 part; Film coalescence aid 0.5-1 part; Component C is that ultramarine or phthalocyanine blue or phthalein viridescent or the blue or green parts by weight red or bright red each raw material of phthalein are.
Described dispersion agent is that EFKA-5065 dispersion agent and EFKA-4050 dispersion agent are according to the mixture of 4:6; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 1:1.
Described defoamer and select respectively EFKA-2722 and EFKA-3239.
Described dispersion agent can be the polyphosphoric acid salt dispersant solution of 10% mass percent, and wherein poly refers to the compound of dimerization or trimerization or dimerization and trimerization; Described phosphoric acid salt refers to phosphide sodium or phosphide potassium or phosphide ammonium.
Described mould inhibitor is Sodium Fluoride or 10, the two phenoxazine arsenic of 10 '-oxo.
Described defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.
A method for described exterior wall water-borne protective system, it prepares by the following method:
The first step: make component A: first ratio takes ACRYLIC EMULSION 40-50 part by weight; Pearlstone 5-8 part; 5 parts of hollow glass micropearls; 5 parts of vermiculite powers; 5 parts of sericites in powder; Epoxy resin: 12 parts, acetone: 18 parts, ethylene glycol monobutyl ether: 8 parts, commercially available OP-10 type emulsifying agent: 3 parts, sodium hydroxide: 0.3 part, ethanol: 50 parts, deionized water: 100 parts; Mixture is heated to 75～85 ℃; Insulation is also stirred 1 hour simultaneously, obtains initial latex; Again by titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts add initial latex to stir to obtain A component emulsion together; Pack A component emulsion into the component A that gets product in packaging vessel;
Second step: make component B: ratio takes the various raw materials of component B mixing and stirring and packs container into and obtain finished product component B by weight;
The 3rd step: according to component A: component B: component C=(500～1000): (50～80): 2 weight ratio takes component C and inserts the component C that gets product in container; And rationally take in proportion component A and component B;
The 4th step: by the 3rd step, claim finished product component C insert in finished product component B, fully stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin coating.
The water corrosion-resistant epoxy paint that has adopted preparation method of the present invention to obtain, one of its key technical indexes, i.e. the Corrosion Protection of coating, as shown in the table:
| Sequence number | Interventions Requested | Technical requirements | Assay | Conclusion |
| 1 | Condition in container | Without lump, after stirring, be uniform state | Meet the requirements | Qualified |
| 2 | Smell | Tasteless | Meet the requirements | Qualified |
| 3 | Application property | Brush two roads accessible | Meet the requirements | Qualified |
| 4 | Low-temperature stability (20 ℃) | Never degenerate | Meet the requirements | Qualified |
| 5 | 25 ℃ of set times | ≤24h | 12h | Qualified |
| 6 | Appearance of film | Normally | Meet the requirements | Qualified |
| 7 | Water-fastness | 96h is without extremely | Meet the requirements | Qualified |
| 8 | Acid resistance | 48h is without extremely | Meet the requirements | Qualified |
| 9 | Abrasion resistance (inferior) | ≥500 | 2500 | Qualified |
| 10 | Midew proof | During humidity 40%, continuous 60 days without mildew | Without mildew | Qualified |
More than show and described ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and specification sheets, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (8)
1. a novel environment friendly heat-insulating anti-corrosive coating, consists of A component, B component and component C, in parts by weight, meets: component A: component B: component C=(500～1000): (50～80): 2; Wherein, component A counts by weight, includes following material and content: ACRYLIC EMULSION 40-50 part; Titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Component B, by by weight, includes following material and content: coating curing agent: 3～5 parts, daconil M: 2～4 parts; Antifreezing agent 1-2 part; Defoamer 0.3-0.8 part; Sterilant 0.1-0.15 part; Dispersion agent 0.1-0.4 part; Alkali swelling thickening material 1-1.5 part, cellulose thickener 0.1-0.2 part; Wetting agent 0.1-0.15 part; Film coalescence aid 0.5-1 part; Component C is that ultramarine or phthalocyanine blue or phthalein viridescent or the blue or green parts by weight red or bright red each raw material of phthalein are.
2. novel environment friendly heat-insulating anti-corrosive coating according to claim 1, is characterized in that: described dispersion agent is that EFKA-5065 dispersion agent and EFKA-4050 dispersion agent are according to the mixture of 4:6; The EFKA-3777 flow agent that described flow agent is and EFKA-3239 flow agent are according to the mixture of 1:1.
3. novel environment friendly heat-insulating anti-corrosive coating according to claim 1, is characterized in that: described defoamer and select respectively EFKA-2722 and EFKA-3239.
4. according to claim 1 or novel environment friendly heat-insulating anti-corrosive coating claimed in claim 2, it is characterized in that: dispersion agent can be the polyphosphoric acid salt dispersant solution of 10% mass percent, and wherein poly refers to the compound of dimerization or trimerization or dimerization and trimerization; Described phosphoric acid salt refers to phosphide sodium or phosphide potassium or phosphide ammonium.
5. according to claim 1 or novel environment friendly skin water-based anticorrosive paint claimed in claim 2, it is characterized in that: described mould inhibitor is Sodium Fluoride or 10 the two phenoxazine arsenic of 10 '-oxo.
6. according to claim 1 or novel environment friendly heat-insulating anti-corrosive coating claimed in claim 2, it is characterized in that: described defoamer is polydimethylsiloxane or silicone emulsion or the fatty acid ester compounded thing of higher alcohols or polyoxyethylene polyoxypropylene tetramethylolmethane ether or polyoxyethylene polyoxy propyl alcohol amidogen ether or polypropylene glycerol aether and polyoxypropylene.
7. a method of preparing exterior wall water-borne protective system claimed in claim 1, it prepares by the following method:
The first step: make component A: first ratio takes ACRYLIC EMULSION 40-50 part by weight; Pearlstone 5-8 part; Hollow glass micropearl 3-5 part; Vermiculite power 2-5 part; Sericite in powder 3-5 part; Epoxy resin: 8～12 parts, acetone: 12～18 parts, ethylene glycol monobutyl ether: 3～8 parts, commercially available OP-10 type emulsifying agent: 1～3 part, sodium hydroxide: 0.1～0.3 part, ethanol: 30～50 parts, deionized water: 70～100 parts; Mixture is heated to 75～85 ℃; Insulation is also stirred 1 hour simultaneously, obtains initial latex; Again by titanium dioxide: 140～180 parts, zinc sulfide white: 35～45 parts add initial latex to stir to obtain A component emulsion together; Pack A component emulsion into the component A that gets product in packaging vessel;
Second step: make component B: ratio takes the various raw materials of component B mixing and stirring and packs container into and obtain finished product component B by weight;
The 3rd step: according to component A: component B: component C=(500～1000): (50～80): 2 weight ratio takes component C and inserts the component C that gets product in container; And rationally take in proportion component A and component B;
The 4th step: by the 3rd step, claim finished product component C insert in finished product component B, fully stirring and dissolving, obtains lysate; Lysate is joined in finished product component A, stir and obtain skin coating.
8. novel environment friendly heat-insulating anti-corrosive coating according to claim 1, its using method is the coating of choosing as described in aforementioned any one claim; External Wall is brushed, more than wherein disposable film thickness reaches 2mm; Dry coating under field conditions (factors) or in baking oven.
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Application publication date: 20140205 |