CN103549411A - Synchronous production technology for preparing dendrobium officinale oral liquid and piece beverage - Google Patents
Synchronous production technology for preparing dendrobium officinale oral liquid and piece beverage Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention discloses a synchronous production technology for preparing a dendrobium officinale oral liquid and a piece beverage, which is a method for extracting polysaccharide by exploding dendrobium plant cells combined an electronic program control (UHP) technology and ultrasonic water jet, and completely releases and dissolves peptidoglycan which is difficult to be extracted from dendrobium, and synchronously prepares an oral liquid or a beverage decoction piece. Low temperature, superhigh pressure and continuous flow cell disruption enables the plant cells to be instantly exploded and released, and under action of energy shearing effect, pressure intensity cavity effect and instant explosion effect, the plant cell is disrupted. Especially, dispersion, emulsification and particle nanocrystallization of the dendrobium officinale peptidoglycan substances maintain activity of the original substances, solves heat radiation difficulty, and avoids heat sensitivity substances to be destroyed. The technology is mainly applied to batch production of the high-content dendrobium peptidoglycan, and enables the dendrobium polysaccharide to be rapidly absorbed by a human body for prolonging life span.
Description
Technical field
The present invention relates to a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage, belong to common technology scope Internet of Things bioengineering field, particularly relate to the synchronous production technique of utilizing electronic program to control (UHP) low temperature explosion plant cell.
Background technology
Dendrobium candidum rises establishing in large scale in the whole nation, the stem of noble dendrobium is the perennial herbaceous plant that grows nonparasitically upon another plant of the orchid family, there is unique medical value, be described as first of nine immortal grass and be used as medicine with stem, Chinese medicine is called the stem of noble dendrobium, belong to the yin tonics < < Chinese pharmacopoeia > > in tonic, according to the fast development of current growing dendrobium, the establishing in large scale of industrialization, the plantation casual household of surging forward, and exactly lack catching up with of scale deep processing industry, rest on maple and seek market on using stratagems, to there is vegetables valency in the stem of noble dendrobium price of going down for a long time, (2012 the end of the year stem of noble dendrobium price fresh goods per kilogram be 800-1500 unit, cost ratio with 2010, in 2 years, dropped 50%).
Owing at least containing 30% above heat-sensitive substance in plant, fear high temperature, and the old technique major part of dendrobium candidum finished product rests on tender stem is twisted into helical form or spring-like, dry, commodity are the storage of maple bucket, the reprocessing of maple bucket must not have new dendrobium candidum deep processed product, fine work exploitation by high temperature, and after the collection of the formation stem of noble dendrobium, price significantly drops.
The extracting method of plant polyose is generally extracting in boiling water, cycle is long, temperature is high, liquid ratio is large, be unfavorable for suitability for industrialized production, low-temperature ultrahigh-pressure (UHP) cell blasting technique, is according to the plant cell explosion between several pressure variations and one or more circulating pressure, recovery rate by explosion stem of noble dendrobium cell polysaccharide is the more than 95% of the stem of noble dendrobium self content, thereby draws the manufacturing technique method of the best active constituent content of oral liquid.
The extracting method of current existing Dendrobium officinale polysaccharide is: dendrobium candidum water is: 100ml/g; Extracting temperature is 100 ℃, extraction time is 3-5 hour, after extraction, have the waste of more than 70% WATER AS FLOW MEDIUM at least, more advanced have electromagnetic oscillation, enzyme digestion reaction, ultrasonic wave extract, all only complicated with, industrialization cost and high technology process as experiment because its energy is little.
Documents: 200810162493.3 dendrobium polysaccharide extracting method, 201210080911.0 response surface method dendrobium polysaccharide extraction processes, 201210291799.5 disposable dendrobium polysaccharide EN separating and extracting process, all be subject to the quantitative limitation of process conditions energy and can only be applied to laboratory, cannot realize industrialization volume production at all, technique is at least destroyed more than 30% heat-sensitive substance by high temperature at the temperature of 92.8 ℃, exists the defect of Dendrobium Plants serious waste.
Superelevation isostatic cool pressing continuous sterilization process and the device of the liquid food of documents 201110148468.1, it just carries out sterilizing to liquid food, although oral liquid belongs to liquid range, and (liquid food) belongs to conventional adopted name, especially because its technological requirement of difference of plant variety is also different, more specifically be that the difference, cell elite releasing effect of Chinese herbal medicine target plant is also just different, single pressure limit only plays sterilization functions, and its process time, utilization rate was lost greatly in long power consumption.
Dendrobium candidum contains abundant polysaccharose substance; there is the effect that strengthens immunologic function; if do not have, can realize the technique follow-up of scale deep processing; stem of noble dendrobium raw materials market will supply exceed demand; and static UHP common technology is combined with dynamic supersonic speed water jet technique; the preliminary experiment of technological process shows, low-temperature ultrahigh-pressure can impel the ripe explosion of dendrobium polysaccharide cell.
Under supersonic speed water jet operating mode, void effect explosion dendrobium candidum plant cell, dendrobium polysaccharide content discharges more than 95%, through looking into domestic and foreign literature, all be difficult electronic program control (UHP) general character pressure and be combined with spiral jet nozzle, produce supersonic jet and swash the relevant technological report that quick-fried stem of noble dendrobium plant cell extracts polysaccharide.
The invention discloses a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice, beverage, also belong to Chinese herbal medicine and extract innovation art field, it is the extension of industrial generic technology (UHP) innovation, this technique is with tunnel type accumulator, to be combined lower explosion plant cell with spiral jet nozzle technique, with the above ultra high pressure liquid of the following low temperature 500Mpa of 20 degree moment explosion dendrobium candidum plant cell, the process of peptidoglycan content and height, the synchronous batch production of many finished products.
Summary of the invention
The present invention has innovated the process conditions with above-mentioned diverse (UHP), it is the defect that overcomes above-mentioned technology, from enzyme digestion reaction, ultrasonic-leaching, film are separated, alcohol is analysed, sum up the reform of deficiency factor with the Technology Integration such as CO 2 supercritical, fluid extraction, industrialization volume production can maximize reduction operating cost, the overall economic efficiency of performance dendrobium candidum; Improve dendrobium polysaccharide purity (peptidoglycan) content, (UHP) be the abbreviation of plant cell blasting technique.
The greatest problem of comparing the more ultrasonic wave of current application, electromagnetic oscillation crush method is: in ultrasonic concussion process, sound wave is absorbed and produces large heat by solution, can not in time heat be shifted out, impel the temperature of cell suspending liquid sharply to raise, cause enzyme and other bioactivator deactivation, also because of the sound wave transmission of large-rolume container and heat radiation difficulty, energy consumption and large and limited the large-scale application of industrialization.
For solving the problems of the technologies described above, these affect first time, pressure and temp chain rate and solid-liquid ratio with plant cell circulation explosion in the factor of dendrobium polysaccharide recovery rate, carry out process conditions innovation, under the conversion of positive negative energy, in spiral jet nozzle, can produce 2 Mach of supersonic jets, thereby improve the yield of Dendrobium officinale polysaccharide, three kinds of finished products are synchronous output in a technological process, consumes energy low and has reduced the consumption of the energy.
Dendrobium officinale polysaccharide peptide content is difference by the difference of the stem of noble dendrobium place of production, kind, production management, due to dendrobium candidum Jing Gan tissue tight, the active ingredient condition of releasing needs the above high temperature of 130 degree, and high temperature has destroyed the heat-sensitive substance in plant cell, make poor stability and the cell wall structure of active substance of plant tightr, it is low and without the high-quality quantification finished product of dendrobium candidum deep processing that existing technique is extracted content.
The present invention is to provide a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage, with electronic program, control the combination of (UHP) common technology and supersonic speed water jet technique, under sensor information guiding, in spiral jet nozzle, carry out the conversion of positive negative energy, produce void effect and swash broken dendrobium candidum plant cell, discharge peptidoglycan content and much higher finished product synchronous production process.
Advanced common technology (UHP) system and device and the conditional combination of supersonic speed water jet technique, by the first section that is broken into 0.5-20mm of dry product dendrobium candidum (maple bucket), soak 24 hours at normal temperatures by the liquid ratio of clean water and dendrobium candidum.
Consider the remaining water of de-bubble, with clean water and dendrobium candidum, proportionally enter high speed beater again, release pressure after pressurize certain hour under the pressure of 450～550Mpa, decompression, pressurized circulation operation, spiral jet nozzle ejection filter and remove residue obtains Dendrobium officinale polysaccharide extract (oral liquid), is greater than the yield of existing any technique through the content of alcohol precipitation standard measure mensuration polysaccharide.
Dendrobium candidum as fresh goods cleans the rear section that is just broken into 20mm, enter high speed beater, with clean water, according to the slurries ratio of 50 to 1 dendrobium candidums, dilute again, pressurize 5-15 minute release pressure under the pressure of 450～550Mpa, pressurization, decompression cycles operate 3 partial nodes and are controlled by node sensor, and technique overall process is 0.65 hour 50L; Dendrobium candidum slurries after release pressure adopt 3 groups of apertures to be respectively 1.2 μ m, 0.8 μ m, 0.6 μ m ceramic membrane filter, Dendrobium officinale polysaccharide extract (oral liquid) removes slag to obtain, the purity super existing technique far away that quantitatively records polyoses content through alcohol precipitation, slag is pressed into medicine materical crude slice by pharmaceutical tabletting machine.
A kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage provided by the invention, following 3 variablees are set: the liquid ratio of dendrobium candidum dry product (maple bucket) and fresh goods and water, extract pressure and dwell time, corresponding according to eucaryotic cell structure demolition effect, utilize 3 pressurizations of circulation, reduce pressure into spiral jet nozzle, precipitation, concentrated, separation obtain dendrobium polysaccharide peptide, and the raffinate after separation is beverage.
Contrast drew with the process time; (UHP) variation of temperature and feed liquid chain rate, pressurized circulation number of times and pressure, is optimized the influence factor of dendrobium polysaccharide recovery rate, and conclusion is that the temperature of optimum optimizing condition is 18.5 ℃; The pressure that circulation pressurization is 3 times is respectively: 450Mpa10 minute, 500Mpa10 minute, 550Mpa10 minute, and the process time is 0.65 hour 5L, and chain rate is 1.25 o'clock, and the yield of polysaccharide can reach the more than 95% of stem of noble dendrobium content.
A kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice, beverage provided by the invention, the industry that is common technology (UHP) research and development intention is extended, can be used as the foundation stone of Industry Innovation, this dendrobium candidum special efficacy oral liquid process pressure can arrange arbitrarily below 620Mpa, under extra-high-speed superpressure condition, the non-total combinations such as the Hydrogenbond in oral liquid in high molecular weight steric structure, hydrophobic binding, ions binding change, and make medium 17
-Owater base hydrogen bond dialysis, forms trace element in 5-6 hydrone and dendrobium candidum and associates, and having produced a kind of Dendrobium officinale polysaccharide special efficacy oral liquid, filtrations recrement and be liquid more than medicine materical crude slice, precipitation is beverage, (UHP) is the abbreviation of ultra-high pressure blasting plant cell.
concrete technical scheme of the present invention is as follows
A kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage, adopt step 1: the section that is just broken into 0.5-20mm with dry product dendrobium candidum (maple bucket), with clean water, according to the dendrobium candidum liquid ratio of 10:1, soak at normal temperatures 24 hours again, consider except remaining water enters high speed beater with clean water according to 65:1 dendrobium candidum liquid ratio again and break into slurry, pressurize 5-15 minute release pressure under the pressure of 450～550Mpa, pressurization, decompression cycles operation 3 times; Step 2: the fresh goods stem of noble dendrobium enters high speed beater after cleaning the section that is just broken into afterwards 0.5-20mm, with clean water, according to the slurries ratio of 50:1 dendrobium candidum, dilute again, 15 minutes release pressures of pressurize under the pressure of 450～550Mpa, pressurization, decompression cycles operation 3 times; It is characterized in that: tunnel type accumulator is controlled pressure by electronic program and generated and discharge, and under sensor information guiding, by spiral jet nozzle, changes positive negative energy, makes to produce void effect in spiral jet nozzle chamber and swashs quick-fried dendrobium candidum cell.
Dendrobium candidum dry product (maple bucket) and fresh goods have two kinds of different liquid ratios, and circulating pressure and dwell time difference; According to eucaryotic cell structure demolition effect, be pressurised into successively: 450,500.550Mpa, dwell time is sequentially: 15 minutes, 10 minutes, 5 minutes, carrying out decompression cycles is controlled by node sensor, the concentrated dendrobium polysaccharide peptide that is optimized for of product precipitation, parting liquid is beverage, dendrobium candidum slurries after release of pressure adopt 3 groups of apertures to be respectively 1.2 μ m, 0.8 μ m, 0.6 μ m ceramic membrane filter removes slag, and by pharmaceutical tabletting machine, slag are pressed into medicine materical crude slice.
When entering the making beating of high speed beater by 65:1 liquid ratio after, dendrobium candidum dry product enters tunnel type accumulator, pressurize 5-15 minute release pressure under the pressure of 450～550Mpa, pressurization, decompression cycles operation 3 times, in release of pressure, enter spiral jet nozzle, the positive negative energy of spiral jet nozzle chamber internal conversion under sensor information guiding, make to produce void effect in spiral jet nozzle chamber and swash quick-fried stem of noble dendrobium cell, tunnel type accumulator is controlled pressure by electronic program and is generated and discharge.
When iron-sheet dendrobe fresh product enters tunnel type accumulator by 50:1 slurries after diluting, 15 minutes release pressures of pressurize under the pressure of 450～550Mpa, pressurization, decompression cycles operation 3 times; It is characterized in that: in the time of release of pressure, enter spiral jet nozzle, the positive negative energy of spiral jet nozzle chamber internal conversion under sensor information guiding, make to produce void effect in spiral jet nozzle chamber and swash quick-fried stem of noble dendrobium cell, above step is all controlled pressure by electronic program and is generated and discharge.
Be further characterized in that: stem of noble dendrobium dry product (maple bucket) and fresh goods have two kinds of different liquid ratios and circulating pressure and dwell time three kinds of different differences; According to eucaryotic cell structure demolition effect, be pressurised into successively: 450,500.550Mpa, dwell time is: the decompression that circulates in 15 minutes, 10 minutes, 5 minutes, time chain rate program is controlled by node sensor, and liquid material is optimized for dendrobium polysaccharide peptide under filtering, precipitate, concentrating, and parting liquid is beverage.
Be further characterized in that: the pressure-bearing device in process conditions must be stainless steel, can meet foodstuff sanitation-stage requirement, dendrobium candidum slurries after release of pressure adopt 3 groups of apertures to be respectively 1.2 μ m, 0.8 μ m again, 0.6 μ m ceramic membrane filter removes slag, and by conventional pharmaceutical tabletting machine, slag are pressed into medicine materical crude slice.Described pressure-bearing device is tunnel type accumulator.
Described electronic program is controlled and is connected to form by pressure sensor, the time relay, signal conversion receiver, node sensor line, according to arranging, require to send e-command, by the lead conversion of positive negative energy of signal conversion receiver, when pressure, dwell time are in order designing requirement, start, close, each security alarm control valve of release pressure.
When process conditions are the pressure-bearing device tunnel type accumulator below 500L, supporting connection spiral jet nozzle forms process system, maximum pressure is 620Mpa, temperature is lower than 20 ℃, classification is pressurised into: 450.500.550Mpa circulating pressure 3 times, as a kind of process conditions method of oral liquid process, above-described pressure-bearing device is applied on the same day: tunnel type accumulator is arranged by 3 pipe U-shaped door case types that connect into of stainless steel, the little intermediate drum circle in described spiral jet nozzle inner chamber two.
Technique (one), with dry product kind dendrobium candidum (maple bucket), be just broken into the section of 0.5-20mm, with clean water, according to the liquid ratio of 10 to 1 dendrobium candidums, soak at normal temperatures 24 hours, the remaining water of worry de-bubble enters high speed beater with clean water according to 65 to 1 dendrobium candidums again and breaks into slurry, then enter tunnel type accumulator, slurries 15 minutes release pressures of pressurize under the pressure of 450～550Mpa in accumulator, decompression, release of pressure after pressurized circulation operates 3 times, in release of pressure, enter spiral jet nozzle, under the conversion of pressure positive negative energy in spiral jet nozzle cavity, produce void effect, by the transmission of node sensor signal, open spiral jet nozzle spout, with 2 Mach of supersonic jets, swash quick-fried dendrobium candidum plant cell.
The slurries, the filter and remove residue that discharge in accumulator obtain Dendrobium officinale polysaccharide extract (oral stoste), and it is 0.65 hour 50L that node sensor is controlled technical process; Through alcohol precipitation, quantitatively record content >=95% of polysaccharide, filter the slag staying and be pressed into medicine materical crude slice by conventional pharmaceutical tabletting machine.
(2), use fresh goods dendrobium candidum: the section that is directly broken into 20mm after cleaning, enter high speed beater, with clean water, according to the slurries of 50 to 1 dendrobium candidums, after diluting, enter tunnel type accumulator again, pressurize 5-15 minute release pressure under the pressure of 450～550Mpa, pressurization, release of pressure after decompression cycles operates 3 times, in release of pressure, enter spiral jet nozzle, under the conversion of pressure positive negative energy in spiral jet nozzle cavity, produce void effect, by the transmission of node sensor signal, open spiral jet nozzle spout, with 2 Mach of supersonic jets, swash quick-fried dendrobium candidum plant cell.
Discharge the slurries filtration in accumulator, the Dendrobium officinale polysaccharide extract (oral stoste) that removes slag to obtain, technique overall process is 0.65 hour 50L; The content that quantitatively records polysaccharide through alcohol precipitation reaches 95% of stem of noble dendrobium content, and slag is pressed into medicine materical crude slice by conventional pharmaceutical tabletting machine.
By 3 groups respectively different pressure rings than explosion plant cell, to the polysaccharide release conditions of dendrobium candidum carry out the dwell time, pressure rings converts than classification, temperature stabilization exists
20 ℃below, when liquid material chain rate affects under the factor of polysaccharide yield, in spiral jet nozzle, void effect produces the sharp quick-fried dendrobium candidum plant cell of supersonic jet of 2 Mach.
Slurries obtain best optimization yield condition, and the comprehensive benefit, the added value efficiency that have improved product improve, the discharge of the basic contamination-free of technical process, and operation energy consumption reduces, and has the practical significance of suitability for industrialized production.
According to eucaryotic cell structure demolition effect, by 3 pressurizations, decompression cycles, carry out products perfection, the dendrobium candidum slurries after release pressure adopt 3 groups of apertures to be respectively 1.2 μ m, 0.8 μ m, 0.6 μ m ceramic membrane filter, and extract peptidoglycan purity is high.
Adopt new varieties dendrobium candidum to extract polysaccharide, dendrobium polysaccharide content >=58%, yield >=56.5%, dendrobine content >=0.2%, 95% of anthocyanidin purity >=content, oral stoste precipitates to concentrate again and is optimized for dendrobium polysaccharide peptide, and parting liquid is that beverage, slag compressing tablet are medicine materical crude slice, the stem of noble dendrobium oral liquid that synchronous process produces has the optimization of matter, the lifting of amount, has and high attached value.
Description of drawings 1 is production technological process.
below with the accompanying drawing detailed annotation specific embodiment
Embodiment 1, dendrobium candidum oral liquid are produced:
one, dry product processing
1, dry product soaks
By the disconnected section of dendrobium candidum dry product, be 0.5-20mm, be dipped to moisture content and be greater than 60% (weight content, general 24 hours), when soaking, there is cleaning action, after considering the remaining water of de-soak, with clean water, according to the liquid ratio of 65 to 1 dendrobium candidums, mix, with the making beating of high speed beater, enter storage tank and do pressurization preparation.
2, the slurries of dendrobium candidum suck 500L pressure-bearing device (tunnel type accumulator) with vavuum pump, pressure transmitter classification cycle is pressurised into 450,500,550Mpa each once, successively the dwell time be 15,10,5min, the 3rd time release pressure rear slurry swashs quick-fried stem of noble dendrobium plant cell with 2 Mach of supersonic jets in spiral jet nozzle, then membrane filtration removes slag, and cannedly under aseptic condition becomes a kind of dendrobium candidum special efficacy oral liquid.
two, fresh goods processing
1, clean making beating
Iron-sheet dendrobe fresh product is cleaned, shears section is 0.5-20mm, directly uses clean water according to high speed beater making beating for the liquid ratio of 50 to 1 dendrobium candidums, enters storage tank and does pressurization preparation.
2, the slurries of bright dendrobium candidum suck 500L pressure-bearing device (tunnel type accumulator) with vavuum pump, pressure transmitter classification cycle is pressurised into 450,500,550Mpa each once, each dwell time is 10min, the 3rd time release pressure rear slurry swashs quick-fried stem of noble dendrobium plant cell with 2 Mach of supersonic jets in spiral jet nozzle, then membrane filtration removes slag, and cannedly under aseptic condition becomes a kind of dendrobium candidum special efficacy oral liquid.
three, micro-polysaccharide drink
1, concentration extraction: iron-sheet dendrobe fresh product is cleaned, is cut into 0.5-20mm section, directly pull an oar with high speed beater according to the solid-liquid ratio of 50 to 1 dendrobium candidums with clean water, enter the pressurization of storage tank do and prepare.
Slurries suck 500L pressure-bearing device (tunnel type accumulator) with vavuum pump, by pressure transmitter classification cycle, be pressurised into 450.500.550Mpa respectively once, each dwell time 10min, the 3rd time release pressure rear slurry swashs quick-fried dendrobium candidum plant cell, then filter and remove residue with 2 Mach of supersonic jets in spiral jet nozzle.
Filtered fluid floats supernatant liquor with the alcohol precipitation method, then is respectively 1.2 μ m, 0.8 μ m, the concentrated polysaccharide underflow that to obtain of 0.6 μ m nano ceramics film dehydration with 3 groups of apertures, through the yield of the benzene phenol-sulfuric acid method quantitative assay polysaccharide of improvement, is the more than 95% of stem of noble dendrobium content.
2, rinsing liquid also contains polysaccharide and other element of 0.5-1.2% after measured, and rinsing liquid is canned under aseptic condition can become a kind of drinking water that contains micro-polysaccharide, and added value is considerably beyond the beverage of class mineral water.
four, Dendrobium officinale polysaccharide medicine materical crude slice
Due to the recrement after filtering, include at least multiple other elements such as Dendrobium officinale polysaccharide more than 0.5-1.2%, alkaloid, EN, when being less than 20%, mixes with the solid tablet 5% of (medicinal regulation permission to use) edible drying to moisture content, with pharmaceutical tabletting machine film-making, be a kind of healthcare decoction pieces of low content polysaccharide, finished product packing.
tool of the present invention has the following advantages and efficiency
Apply a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage, at electronic program, control (UHP) technical conditions and be combined explosion stem of noble dendrobium plant cell with supersonic speed spiral water jet technique, the peptidoglycan that is difficult to extraction in the stem of noble dendrobium discharge dissolving completely, refine into oral liquid, beverage medicine materical crude slice.
The fragmentation of low-temperature ultrahigh-pressure continuous flow cell discharges plant cell moment explosion, under the effect of energy shearing effect, pressure void effect, moment blasting effect, makes its plant cell broken; Especially the dispersion of Dendrobium officinale polysaccharide peptide material, emulsification, particle nanometer, kept original material active, large capacity pressure-bearing device has solved heat radiation difficulty in existing technique, has avoided the destroyed of heat-sensitive substance, and the dendrobium polysaccharide purity that is absorbed by the body is high and help to promote longevity.
By electronic program, control each safety alarm device and control valve, guarantee technical process handling safety, when process conditions are pressure-bearing device and the spiral jet nozzle (separately having Specialty Design) below 500L, adopt pressure-bearing device and the jet pipe inner chamber of stainless steel, reach foodstuff sanitation-stage requirement completely, maximum pressure is 6150Mpa, temperature is lower than 20 ℃, classification is pressurised into 450.500.550Mpa and circulates after 3 times, under the conversion of slurries positive negative energy in by spiral jet nozzle cavity, produce void effect, with 2 Mach of supersonic jets, swash quick-fried stem of noble dendrobium plant cell, polysaccharide discharges more than 95%, process time is that M hour 500L output can reach the above industrialization of middle rank, 95% of the rate of releasing >=stem of noble dendrobium content of polysaccharide, shortened the production time, production process temperature is low, operating cost is produced in the low saving of consuming energy, improved product efficiency, chain rate has reduced energy loss while being 1:25, water resource is without waste, and production technology overall process, without zero emission, meets the production standard of national environmental protection cleaned industry.
In sum, it is the innovation of oral liquid production method that (UHP) super-pressure circulation pressurization that the present invention adopts designs a model, belong to a kind of extension of common technology, can be applicable to various oral liquid beverages, with existing technique electromagnetic oscillation, enzyme digestion reaction, supercritical ultrasonics technology is compared, its industrialization production scale is large, polysaccharide yield maximizes (different by the polyoses content of the different cultivars stem of noble dendrobium), and resulting optimum condition is not the value of setting, but within the scope imposing a condition, pressure-bearing device takes (UHP) super-pressure circulation pressurization to be combined with spiral jet nozzle, what obtain is best quantification process conditions.
With micro-filtration (MF), ultrafiltration (UF), compare with techniques such as counter-infiltration (RO) or nanofiltrations (NF), energy consumption and operating cost reduce greatly, amplified industrialization production capacity, can effectively improve the quality of products and reduce production costs, utilize low temperature extra-high-speed superpressure moment explosion plant cell, dendrobium polysaccharide is released in solution completely, medium is clean water, can utilize water resource abundant, at (UHP) low-temperature ultrahigh-pressure (below 20 ℃), avoided in plant the destroyed of effective heat-sensitive substance, improved the quality of stem of noble dendrobium oral liquid, the overall economic efficiency of investment, technique is simple, electronic program control operation is convenient, safety, operating cost is cheap, being suitable for automatic industrial produces, product color is good, and dissolubility is good, and active component purity is high.
Finally; it is also to be noted that; a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice, beverage; because its low temperature liquid super-pressure technique is that common technology can range of application and wide; what more than enumerate is only several specific embodiments of the present invention; obviously; the invention is not restricted to above embodiment; can also there be many retrofits, products innovation, patent families; all distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention, all should think protection scope of the present invention.
Claims (3)
1. a synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage, adopt step 1: the section that is just broken into 0.5-20mm with dry product dendrobium candidum (maple bucket), with clean water, according to the dendrobium candidum liquid ratio of 10:1, soak at normal temperatures 24 hours again, consider except remaining water enters high speed beater with clean water according to 65:1 dendrobium candidum liquid ratio again and break into slurry, pressurize 5-15 minute release pressure under the pressure of 450～550Mpa, pressurization, decompression cycles operation 3 times; Step 2: the fresh goods stem of noble dendrobium enters high speed beater after cleaning the section that is just broken into afterwards 0.5-20mm, with clean water, according to the slurries ratio of 50:1 dendrobium candidum, dilute again, 15 minutes release pressures of pressurize under the pressure of 450～550Mpa, pressurization, decompression cycles operation 3 times; It is characterized in that: tunnel type accumulator is controlled pressure by electronic program and generated and discharge, and under sensor information guiding, by spiral jet nozzle, changes positive negative energy, makes to produce void effect in spiral jet nozzle chamber and swashs quick-fried dendrobium candidum cell.
2. according to a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage of claim 1, it is characterized in that: dendrobium candidum dry product (maple bucket) and fresh goods have two kinds of different liquid ratios, and circulating pressure and dwell time difference; According to eucaryotic cell structure demolition effect, be pressurised into successively: 450,500.550Mpa, the dwell time is sequentially: 15 minutes, 10 minutes, 5 minutes, to carry out decompression cycles and controlled by node sensor, product precipitation is concentrated is optimized for dendrobium polysaccharide peptide, and parting liquid is beverage.
3. a kind of synchronous production technique of making dendrobium candidum oral liquid, medicine materical crude slice beverage according to claim 1, it is characterized in that: the dendrobium candidum slurries after release of pressure adopt 3 groups of apertures to be respectively 1.2 μ m, 0.8 μ m, 0.6 μ m ceramic membrane filter removes slag, and by pharmaceutical tabletting machine, slag are pressed into medicine materical crude slice.
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| CN109998007A (en) * | 2018-01-05 | 2019-07-12 | 黑龙江省宏达大健康产业有限公司 | A kind of formula and preparation method thereof of blueberry small-molecular peptides solid beverage |
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