CN103540409B - A kind of production method of lemon quintessence oil - Google Patents
A kind of production method of lemon quintessence oil Download PDFInfo
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Abstract
The present invention discloses a kind of production method of lemon quintessence oil, comprise cleaning and sterilizing, get essential oil, oily water separation, the steps such as encapsulation preservation, getting essential oil step adopts wiping skin mode to get oil, Lemon fruit is sent into vertical mill oil machine top quantitative storage feed bin, Lemon fruit enters from the top of oil grinding machine, go out from the side after falling into middle part mill mill fruit, due to the twirl of mill, Lemon fruit is constantly rolled on mill, simultaneously, due to the effect of centrifugal force, Lemon fruit also constantly collides with surrounding machine wall, it is broken fuel-displaced that Lemon fruit epidermis is made pericarp oil vacuole fully rupture by the mill shock rotated.The present invention adopts novel appts vertical mill oil machine to get oil, lemon oil extraction yield is up to 0.5%, inlet amount, mill fruit time, grind oily rotating speed aspect and all can do corresponding adjustment according to lemon characteristic, realize consecutive production, and produce after lemon profile complete, squeeze the juice except slag processed except tradition and also can be processed into the goods such as lemonade tablet, fruit fourth, rear end processing and utilization channel is more wide.
Description
Technical field
The present invention relates to the technical field that Pure natural plant essential oil is produced, particularly relate to a kind of production method of lemon quintessence oil.
Background technology
Plants essential oil is the distinctive aromatoising substance of extraction plant, is taken from herbal flower, leaf, root, bark, fruit, seed, resin etc. and extract with lixiviate, distillation, squeezing mode.Because essential oil-fumigation volatility is high, and molecule is little, be easy to be absorbed by the body, and energy rapid permeability people intracorporeal organ, unnecessary composition is excreted, whole process only needs several minutes, and the fragrance of plant itself, the also secretion of direct Stimulation of The Brain pendant, ferment and hormone secretion etc., function in balanced body, plays the effect of beauty and skin care.Well imagine that the secret of essential oil to human body is incomparable broad.Essential oil is the high enrichment extract of scented plants.
The manufacture method of plants essential oil mainly contains milling process, extraction, distillation etc.Wherein the essential oil of the autocratic oranges and tangerines generic of milling process is as lemon, orange, Fructus Citri Sarcodactylis, grape sleeve and red mandarin orange.Before nineteen thirty, this kind of essential oil still refines with sponge process, is namely extruded on sponge by essential oil by hand, then sponge impregnating grease to inhale its essential oil.Skilled workman understands the pressure that applying is suitable, and essential oil is extruded from pericarp, but this refinement method is because labor intensive, so with high costs, method of squeezing now gives machine handling all.Plants essential oil is from plantation to refinement, very complicated, takes time and effort, and requires consummate rigorous, so cost is quite high, is worth also certainly expensive.Lemon is rich in the nutritive ingredient of the multiple needed by human body such as citric acid, VC, limonene, essential oil, lemon yellow letones, pectin, be a kind of food of hyperkalemia hyponatremia, there is clearing away summer heat, cough-relieving is eaten in Appetizing spleen-tonifying, change, strengthen intestines peristalsis, prevent that cardiovascular and cerebrovascular is brittle, the function of skin maintenance; Normal food lemon has certain prevention and auxiliary therapeutic action to hypertension, heart trouble, cardiovascula arteriosclerosis, obesity, cutaneous pigmentation of improving.
In lemon, lemon quintessence oil content is up to 0.6-0.7%, lemon quintessence oil is containing the aroma-producing substance such as citral, limonene, be not only a kind of food flavor(ing) raw material of high-quality, be also widely used in the clean liquor of daily use chemicals and precision electronic element, extracting method is generally acupuncture and gets oil, squeezing and lixiviate.But acupuncture and milling process oil quality is high but extraction yield only has 0.3-0.4% usually, usually also need further distillation in extraction oil product, cause the of poor quality of essential oil.
Summary of the invention
In view of this, the invention provides a kind of production method of lemon quintessence oil, extraction yield high, quality better when producing lemon quintessence oil, the lemon profile after production is complete, does not affect the use of lemon.
For solving above technical problem, technical scheme of the present invention is, a kind of production method of lemon quintessence oil is provided, the lemon fresh fruit selected is carried out cleaning and sterilizing, get essential oil, oily water separation, encapsulation is preserved, described essential oil step of getting adopts wiping skin mode to get oil, concrete operations are: Lemon fruit is sent into vertical mill oil machine top storage bin, Lemon fruit enters from the top of oil grinding machine, go out from the side after falling into middle part mill mill fruit, due to the twirl of mill, Lemon fruit is constantly rolled on mill, simultaneously, due to the effect of centrifugal force, Lemon fruit also constantly collides with surrounding machine wall, it is broken fuel-displaced that Lemon fruit epidermis is made pericarp oil vacuole fully rupture by the mill shock rotated, and by HP shower, essential oil is rushed to oil grinding machine bottom recovery unit, spray water speed be 1.2-1.5 ton/hour, hydraulic pressure control is at 0.5-0.6MPa, the mill speed rotated is that 100-200 revs/min of frequency conversions are adjustable.
Preferably, described vertical mill oil machine comprises housing, storage bin is provided with in described housing, rotating grinding board, spray water system, retrieving arrangement, described storage bin is positioned at the top of housing, each charging 40-60 kilogram, Lemon fruit after charging is admitted to rotating grinding board, it is that the quartz sand of 3mm makes the equipment surface contacted with lemon be uneven that described rotating grinding board wall and machine surrounding inwall all scribble diameter, clash into lemon pericarp, the diameter 800-1200mm of rotating grinding board, mill bunker height 500-700mm, housing central section is provided with process fruit discharge port, the upper end of rotating grinding board connects storage bin, lower end connects oil-water residue retrieving arrangement.
Preferably, described get essential oil step before insert stage treatment step, Lemon fruit after cleaning and sterilizing is carried out classification by three kinds of specifications, then load grading machine, transverse diameter is respectively the fruitlet of 40-50mm, the middle fruit of 50-65mm, be greater than the large fruit of 65mm, wherein fruitlet enters a passage oil grinding machine, and middle fruit enters the second to the 7th passage oil grinding machine, and the fruit of large fruit 65mm enters the 8th passage oil grinding machine.
Preferably, described fruitlet, middle fruit, large fruit enter in the vertical mill oil machine that rotating grinding board diameter is 800mm, 1000mm, 1200mm respectively, fruitlet revolution 100-140 rev/min, mill oil time 60-65 second, middle fruit 140-160 rev/min, mill oil time 65-70 second, large fruit 160-200 rev/min, mill oil time 70-75 second.
Preferably, the mixture that described oil grinding machine bottom retrieving arrangement is collected, first filter through vibratory screening apparatus and remove thick slag, again through twin-stage separating treatment, first refinement treatment is carried out by spiral finishing machine, after the oil-water residue mixture obtained filters, oil refining is carried out with being pumped into butterfly separating machine, also lemon oil can be made to produce producing microbial containing moisture content by the lemon oil of butterfly separating machine gained to ruin and be oxidized, lemon oil sealing is temporary in bottom to be had in the cone-shaped stainless steel bucket of discharge outlet, in the storehouse of 0-10 DEG C, leave standstill 48 hours, discharge the moisture being deposited on bottom.
Preferably, the rotating speed of described butterfly separating machine 7000 revs/min, oil-water residue mixture feed rate controls identical with mill fruit spray water, maintenance 1.2-1.5 ton/hour.
Preferably, described in the lemon fresh fruit selected pluck for tree is upper after remove rot to go mouldy, disease and pest fruit, transverse diameter >=40mm, from the Lemon fruit plucking to the shelf-time of processing and be no more than the Lemon fruit of 48 hours.
Compared with prior art, tool of the present invention has the following advantages:
One, the extraction yield of present invention process is high: adopt novel appts vertical mill oil machine to get oil, carries out stage treatment simultaneously and selects the mill of suitable diameter to ensure the evenly abundant of Lemon fruit shock according to lemon size, make lemon oil extraction yield up to 0.5%.Inlet amount, mill fruit time, grind oily rotating speed aspect and all can do corresponding adjustment according to lemon characteristic, consecutive production can be realized, present invention process reaches 10 tons/hour to lemon fresh fruit treatment capacity, process 20,000 tons of lemon fresh fruit meters per year, lemon oil 20-40 ton can be increased, by lemon oil ready market price 300,000 yuan/ton, can be enterprise increases pure profit 600-1200 ten thousand yuan.
Two, present invention process products obtained therefrom product are of fine quality: utilize the method for physical shock to extract the lemon quintessence oil of pure natural, without any substance, pollution-free, and the technology adopting twin-stage to be separated, profit is fully separated, improves the quality of lemon quintessence oil further.
Three, present invention process is simple, easy to operate, and whole Production Flow Chart can not destroy Lemon fruit outward appearance, and the lemon external form after mill oil is complete, except carrying out traditional pressure extracting juice, also can be used for section or dices, and the comprehensive processing and utilization having widened lemon is worth.
Embodiment
In order to make those skilled in the art understand technical scheme of the present invention better, below in conjunction with specific embodiment, the present invention is described in further detail.
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
A production method for lemon quintessence oil, its concrete steps are as follows:
Select raw material fruit: the lemon fresh fruit selecting 7-8 maturation, lemon plucks the time 24-48 hour to delivering to source mill and carrying out processing from tree, remove rot to go mouldy, disease and pest really, Lemon fruit transverse diameter requirement >=40mm.
Pressure pulse cleaning: former fruit carries out bubbling flushing in Xi Guochi, remove silt and the foreign material of its surface attachment, Xi Guo pond, underground length, width and height are of a size of 3mx2mx3m, wash fruit pond median water level and remain on 3/4ths high places of pond, the thickness of lemon in Chi Guochi keeps 20 centimetres high, add before lemon and open surfing water pump, allow water rolling in pond.
Cleaning showers is sterilized: Lemon fruit in fruit pond is sent into ozone pond by the board-like lift with three sections of sprays, synchronous spray irrigation removes fruit telogenesis sewage, spray hydraulic pressure keeps 0.2-0.3MPa, water surface distance 40-60cm in lift outlet distance tank, consistency of ozone water 2-3mg/L, PH:5.0-5.5,2-3 minute during ozone water process, reduce fruit face heavy metal and agriculture residual, and by rolling bar lift send into grading machine.
Size classification process: carry out classification by three kinds of specifications, be respectively the fruitlet of 40-50mm, the middle fruit of 50-65mm, be greater than the large fruit of 65mm, wherein fruitlet enters the little oil grinding machine of a passage, and middle fruit enters oil grinding machine in the second to the 7th passage, and the fruit of large fruit 65mm enters the and enters the large oil grinding machine of eight passages.
Wipe skin centrifuging and taking oil: enter by the fruitlet of size classifier, middle fruit, large fruit lemon the oil grinding machine that diameter is 800mm, 1000mm, 1200mm respectively, grind oily controling parameters: every each inlet amount 50-60 kilogram of platform, spray water flow 1.2-1.5 ton/hour, hydraulic pressure keeps 0.5-0.6MPa, and spray water recycles; Fruitlet mill fruit machine revolution 100-140 rev/min, mill oil time 60-65 second, middle fruit mill fruit machine rotating speed 140-160 rev/min, mill oil time 65-70 second, large fruit mill fruit machine rotating speed 160-200 rev/min, mill oil time 70-75 second.Due to the twirl of mill, Lemon fruit is constantly rolled on mill, simultaneously, due to the effect of centrifugal force, Lemon fruit also constantly collides with surrounding machine wall, Lemon fruit epidermis is clashed into by the mill that rotates that pericarp oil vacuole is fully ruptured is broken fuel-displaced, and essential oil punching to oil grinding machine bottom recovery unit is formed oil-water emulsion by HP shower and enter next process and filter, and puies forward the Lemon fruit external form after oil complete.
Refinement treatment: first filtered by vibratory screening apparatus from oil grinding machine oil-water residue mixture out and remove thick slag, mesh size 200 order, amplitude 5-9mm, the dregs of fat of gained carry out refinement treatment through spiral finishing machine, contained oil grain slag in pomace is separated further, and after twice initial filter, the oil-water residue mixture of gained carries out oil refining by being pumped into butterfly separating machine.
Butterfly centrifugal is refined: when lemon oil grain slag mixture flows through the gap between video disc, solid particulate is deposited on video disc and forms sediment under whizzer effect.Sediment slides along disc surface and departs from video disc and accumulate in the maximum position of rotary drum interior diameter, because lemon oil proportion is lighter than water, in whizzer high-speed rotation, under centrifugal action, be collected at upper strata flow out from light liquid relief outlet, the water after separation enters cyclic water tank from the discharge of bottom heavy-fluid and makes spray water by being pumped into oil grinding machine.Butterfly separating machine rotating speed 7000 revs/min, profit feed rate control 1.2-1.5 ton/hour.
Low temperature stores sedimentation in advance: by the moisture content of lemon oil also containing minute quantity of butterfly separating machine gained, lemon oil can be made to produce producing microbial ruin and be oxidized, lemon oil sealing is temporary in bottom to be had in the cone-shaped stainless steel bucket of discharge outlet, in the storehouse of 0-10 DEG C, leave standstill 48 hours, discharge a small amount of moisture and micro-slag that are deposited on bottom.
Temperature control stores: be sub-packed in 100 liters of stainless steel casks by the sealing of the lemon oil of gained, store in the storehouse of 0-10 DEG C.Product uncap use before need to move to outdoor exercise use again after temperature return to room temperature, prevent the moisture in air from meeting and coldly condense in lemon oil surface.Packaging vessel can not use metal bucket and plastic tank, Liquid level bung 2-3cm place, avoids the oxygen in bucket in residual air to cause oil oxidation.
Get compared with oil process with horizontal oil grinding machine with cup type squeezing the juice, the extraction yield of vertical mill oil machine of the present invention is the highest, because first carried out Lemon fruit classification before mill oil, according to the oil grinding machine that Lemon fruit transverse diameter selects diameter different, be that the quartz sand of 3mm makes the equipment surface contacted with lemon be uneven by all scribbling diameter at rotating grinding board wall and machine surrounding inwall, due to the twirl of mill, Lemon fruit is constantly rolled on mill, simultaneously, due to the effect of centrifugal force, Lemon fruit also constantly collides with surrounding machine wall, operation scheme is irregular operation shape, include rolling, collision, the modes such as friction, achieve comprehensive without dead angle mill oil, Lemon fruit epidermis is clashed into by the mill that rotates and inwall that pericarp oil vacuole is fully ruptured is broken fuel-displaced, and extracted under the top-down flushing of HP shower, enter next process in oil-water residue mixture to filter.Mill fruit time arrival trailing flank door is automatically knocked at the door and is opened, and the lemon after mill oil throws away at the reactive force of mill centrifugal force and enters lower step operation.Grind speed of grinding plate and mill oil time in oily process simultaneously and all can do corresponding adjustment according to the characteristic of lemon fresh fruit.Its another principal feature is that single short run is concentrated and got oil (unit single enters lemon 40-60 kilogram), and simultaneously quartz sand quality is hard, wear-resisting acidproof, can not by lemon acid damage.
Horizontal oil grinding machine is (as Wuxi section peace, Jiangsu section prestige etc.) be by installing friction plane or screw rod in casing additional, rubbing in plane or screw rod is arranging jagged thorniness metal strip or draw point formation friction plane, friction integral plane is undertaken rhythmically rocking and vibrating or under the propelling of screw rod by the device that mounting spring device principal oscillation motor forms similar shaking table, Lemon fruit is in upper surface jitter and rolling, the oil vacuole of exocarp is punctured by draw point and gets oil, it is one of foot point not: due to lemon fruit be in the middle part of ellipse circular large two little, it is beated and concentrates on middle part with the primary friction face in roll procedure and cause the oil vacuole at lemon two ends place to be not easily punctured, not foot point two: because thick and comparatively hard and by lemon the peracidity of lemonade pericarp affects, the draw point easy passivation of needle point in use for some time, lemon oil vacuole is caused to puncture not thorough, not foot point three: Lemon fruit is in the oily process of mill, lemon leans on the promotion naturally of rocking of grinding machine or screw rod to move ahead, and adopt and enter fruit continuously, the mode of mill oil, the fruit after the fruit that newly enters and mill is easily made to mix, there is the phenomenon that part fruit excessively grinds oil and part fruit mill shortage of oil, because lemon is continuous advance, grinding machine length is fixing, then lemon mill fruit residence time in a device and the fltting speed of shaking table or screw rod are inverse relation, corresponding adjustment can not be done according to the size of Lemon fruit and fresh new degree, thus cause lemon oil extraction yield not enough, slow down speed, although the mill fruit time lengthens, but grind oily intensity to reduce, the not broken oil vacuole of thorn, tune up speed, though intensity increases, the mill oil time reduces, and does not reach the object of fully mill fruit.
Another kind is cup type (bowl formula) juice extractor (as U.S. JBT, poplar state Fu Er like), this machine is lemon is got to oil, squeezes the juice, the lower cup of single lemon access arrangement one by one, and oil obtains when being cup and lower cutter under fruit is placed, upper cup is anti-to come, and after extruding, fruit juice enters recycling machine.Meanwhile, pericarp shreds, and passes through at upper strata cup, and oil vacuole fracture is fuel-displaced.Though achieve get oil, squeeze the juice synchronously carry out and be separated, but its central principle of getting oily mode still extrudes, the middle part mainly concentrating on fruit of main stress point, the oil vacuole at base of fruit two ends place is not easily extruded to, from causing, oily extraction yield is on the low side, simultaneously because the cup size of every platform machine is fixing, lemon can only carry out classification by relative dimension scope, and therefore lemon can not coordinate completely with the size of cup and affect squeezing effect; In addition due to through cup type squeezing machine out after lemon peel shredded, the following process form of skin is single, after drying, obtained lemon peel slag is sold, and the lemon external form after this law processing remains unchanged substantially, except squeezing skin slag processed, also can be processed into the goods such as carbohydrate freeze-dried lemon slices, fruit fourth, following process utilizes channel more wide.
Below be only the preferred embodiment of the present invention, it should be pointed out that above-mentioned preferred implementation should not be considered as limitation of the present invention, protection scope of the present invention should be as the criterion with claim limited range.For those skilled in the art, without departing from the spirit and scope of the present invention, some improvements and modifications can also be made and also should be considered as protection scope of the present invention.
Claims (4)
1. a production method for lemon quintessence oil, the lemon fresh fruit selected is carried out cleaning and sterilizing, gets essential oil, oily water separation, encapsulation preserve, it is characterized in that:
Described essential oil step of getting adopts wiping skin mode to get oil, concrete operations are: Lemon fruit is sent into vertical mill oil machine top storage bin, Lemon fruit enters from the top of oil grinding machine, go out from the side after falling into middle part mill mill fruit, due to the twirl of mill, Lemon fruit is constantly rolled on mill, simultaneously, due to the effect of centrifugal force, Lemon fruit also constantly collides with surrounding machine wall, it is broken fuel-displaced that Lemon fruit epidermis is made pericarp oil vacuole fully rupture by the mill shock rotated, and by HP shower, essential oil is rushed to oil grinding machine bottom recovery unit, spray water speed be 1.2-1.5 ton/hour, hydraulic pressure control is at 0.5-0.6MPa, the mill speed rotated is that 100-200 revs/min of frequency conversions are adjustable,
Described vertical mill oil machine comprises housing, storage bin is provided with in described housing, rotating grinding board, spray water system, retrieving arrangement, described storage bin is positioned at the top of housing, each charging 40-60 kilogram, Lemon fruit after charging is admitted to rotating grinding board, it is that the quartz sand of 3mm makes the equipment surface contacted with lemon be uneven that described rotating grinding board wall and machine surrounding inwall all scribble diameter, clash into lemon pericarp, the diameter of rotating grinding board is 800-1200mm, housing central section is provided with process fruit discharge port, the upper end of rotating grinding board connects storage bin, lower end connects oil-water residue retrieving arrangement,
Described get essential oil step before insert stage treatment step, Lemon fruit after cleaning and sterilizing is carried out classification by three kinds of specifications, be respectively transverse diameter and be greater than 40mm and the fruitlet being less than 50mm, transverse diameter is not less than 50mm and is not more than the middle fruit of 65mm, transverse diameter is greater than the large fruit of 65mm, wherein fruitlet enters the little oil grinding machine of first channel, and middle fruit enters oil grinding machine in the second to the 7th passage, and large fruit enters the large oil grinding machine of the 8th passage;
Described fruitlet, middle fruit, large fruit enter in the vertical mill oil machine that rotating grinding board diameter is 800mm, 1000mm, 1200mm respectively, fruitlet revolution 100-140 rev/min, mill oil time 60-65 second, middle fruit 140-160 rev/min, mill oil time 65-70 second, large fruit 160-200 rev/min, mill oil time 70-75 second.
2. the production method of lemon quintessence oil as claimed in claim 1, it is characterized in that, the mixture that described oil grinding machine bottom retrieving arrangement is collected, first filter through vibratory screening apparatus and remove thick slag, again through twin-stage separating treatment, first refinement treatment is carried out by spiral finishing machine, after the oil-water residue mixture obtained filters, oil refining is carried out with being pumped into butterfly separating machine, also lemon oil can be made to produce microorganism containing moisture by the lemon oil of butterfly separating machine gained to ruin and be oxidized, lemon oil sealing is temporary in bottom to be had in the cone-shaped stainless steel bucket of discharge outlet, 48 hours are left standstill in the storehouse of 0-10 DEG C, discharge the moisture being deposited on bottom.
3. the production method of lemon quintessence oil as claimed in claim 2, is characterized in that, the rotating speed of described butterfly separating machine 7000 revs/min, and oil-water residue mixture feed rate controls identical with mill fruit spray water, maintenance 1.2-1.5 ton/hour.
4. the production method of the lemon quintessence oil as described in any one of claims 1 to 3, it is characterized in that, the described lemon fresh fruit selected remove after plucking for tree is upper rot to go mouldy, disease and pest fruit, transverse diameter >=40mm, from the Lemon fruit plucked to the shelf-time of processing and be no more than 48 hours.
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| CN103834465A (en) * | 2014-03-07 | 2014-06-04 | 安岳安德利柠檬产业科技有限公司 | Method for extracting and processing high-purity lemon oil |
| WO2017020254A1 (en) * | 2015-08-04 | 2017-02-09 | 张甘霖 | Sweet orange essential oil preparation device and process |
| CN109363021A (en) * | 2018-10-16 | 2019-02-22 | 宾川县华侨庄园农业科技开发有限公司 | A kind of processing method of orange blossom |
| CN109480130A (en) * | 2018-10-25 | 2019-03-19 | 重庆尚蔬坊饮料食品股份有限公司 | Reduce the mill oil method of skin oil and its fruit juice obtained in citrus fruit juice |
| CN109674090B (en) * | 2019-01-18 | 2022-03-22 | 深圳市新宜康科技股份有限公司 | Aerosol generator and method of manufacturing the same |
| CN112006946A (en) * | 2020-09-28 | 2020-12-01 | 宁波捷通机械有限公司 | Preparation process of skin care product lemon essential oil |
| CN112522023B (en) * | 2020-11-30 | 2021-08-03 | 重庆檬泰生物科技有限公司 | Citrus fruit peeling device |
| CN116172152A (en) * | 2023-02-23 | 2023-05-30 | 北京火星补给科技文化有限公司 | Process for preparing lemon raw juice by adding water-washed lemon oil |
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