CN103522736B - A kind of manufacture method of flame retardant plastic rubber roll - Google Patents
A kind of manufacture method of flame retardant plastic rubber roll Download PDFInfo
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- CN103522736B CN103522736B CN201310431053.4A CN201310431053A CN103522736B CN 103522736 B CN103522736 B CN 103522736B CN 201310431053 A CN201310431053 A CN 201310431053A CN 103522736 B CN103522736 B CN 103522736B
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- flame retardant
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Abstract
The invention belongs to machinery preparation field, refer to the manufacture method of a kind of flame retardant plastic rubber roll, it includes roller core, rubber roll extruder and coating machine, roller core is sent to the most with gap in the elastomeric material in rubber roll extruder forming room, by the roller core outer surface described in described elastomeric material cladding, the roller core that outer surface has been coated with elastomeric material puts into enforcement vulcanizing treatment in vulcanizer, form rubber rollers, again rubber rollers is loaded on coating machine, preheating, bonding agent is uniformly applied to rubber rollers outer surface, polyvinyl chloride pulp is poured on coating machine coating cutter, it is coated with 1~2mm polyvinyl chloride pulp at rubber rollers outer surface, nano flame retardant complex.The present invention utilizes rubber roll extruder to be coated with one layer of rubber layer on roller core; coating machine is utilized again to be coated with one layer of soft PVC plastic layer outside rubber layer; increase the protective effect to rubber layer; extend the service life of flame retardant plastic rubber roll, had at aspects such as easy cleaning, resistance to be full of cracks, use periodicity especially and be greatly improved.
Description
Technical field
The invention belongs to machinery preparation field, refer to the manufacture method of a kind of flame retardant plastic rubber roll.
Background technology
The operation strategies of flame retardant plastic rubber roll is very big, a lot of enterprises, industry or even national all kinds of printing machinery life-time service,
Owing to there is the deficiency of congenital material property so that flame retardant plastic roll surfaces is rougher, rubber surface is easily cracked thus shadow
Ring and use quality and life-span.
Summary of the invention
For not enough present on prior art, the present invention provides the one that a kind of smooth surface, rubber layer are not easily cracked
The manufacture method of flame retardant plastic rubber roll.
To achieve these goals, the present invention is to realize by the following technical solutions:
The manufacture method of a kind of flame retardant plastic rubber roll, including roller core, rubber roll extruder and coating machine, its described manufacture method
Comprise the steps:
1) kicker cylinder wicking surface impurity;
2) unvulcanized elastomeric material it is full of in the forming room of rubber roll extruder;
3) roller core is sent to the most with gap in the elastomeric material in rubber roll extruder forming room, by described rubber material
Roller core outer surface described in material cladding;
4) outer surface has been coated with the roller core of elastomeric material and has put into enforcement vulcanizing treatment in vulcanizer, rubber layer thickness 2mm,
Form rubber rollers;
5) preparation polyvinyl chloride pulp;
6) rubber rollers is loaded on coating machine, preheating;
7) bonding agent is uniformly applied to rubber rollers outer surface;
8) polyvinyl chloride pulp is poured on coating machine coating cutter, is coated with 1~2mm polychlorostyrene second at rubber rollers outer surface
Alkene, nano flame retardant complex slurry;The preparation method of described nano flame retardant complexing agent is:
(1) by silicone hydroxyl apatite, red phosphorus, attapulgite, brucite, montmorillonite, titanium dioxide, calcite, Kaolin according to
The mass fraction proportioning mixing of 25-35:15-20:10-15: 10-15:8-10:8-10:7-8:5-7, joins 200 parts of diformazans
In the mixed solution of sulfoxide (DMSO) and 50 parts of methanol, stir 60 hours in 65 DEG C, filter, and wash with the hot ethanol of 60 DEG C of temperature
The dimethyl sulfoxide (DMSO) that 3 times remove excess, puts into vacuum drying oven, is dried 24 hours 60 DEG C of temperature, and grinding is sieved, and obtains one
Secondary modified flame-retardant complex;
(2), by 1 part of modified flame-retardant complex, 10 parts of potassium acetates and 25 parts of distilled water mixing, stir in temperature 50 C
More than 10 hours, in temperature 30 DEG C, first disperse 2.5 hours under the conditions of ultrasonic electric power 350W, the most again at ultrasonic electric power
Disperse 3 hours under the conditions of 250W.Filtering, and wash 3 times with distillation, 80 DEG C are vacuum dried 24 hours, and grinding is sieved, and obtains secondary and changes
Property flame-retardant compounds;
(3), above-mentioned 1 part of twice-modified flame-retardant compounds is disperseed 40min at 600W power ultrasonic, fill by heated at constant temperature
Put and be heated to 90 DEG C, and stir (1200r/min) 60 minutes with mechanical agitator;Obtain nano flame retardant complex;
9), after cooling, step 8) 2 times are repeated;
10) turning outer surface, and clean polishing.
The manufacture method of above-mentioned flame retardant plastic rubber roll, its described elastomeric material calculates by weight, including 50~70
The epoxychloropropane of part and the calcium carbonate of 30~50 parts are mixed.
The manufacture method of above-mentioned flame retardant plastic rubber roll, its described bonding agent includes E-44 epoxy resin, E-54 asphalt mixtures modified by epoxy resin
Fat or 630 epoxy resin press the weight ratio composition of 1:1 with low molecular weight polycaprolactone phthalein polyimide resin, heat 10~20 minutes, heating-up temperature 180
~220 DEG C.
The manufacture method of above-mentioned flame retardant plastic rubber roll, its described polyvinyl chloride pulp includes calculating by weight, poly-
Vinyl chloride paste resin 80~120 parts, dioctyl phthalate 50~70 parts, dibutyitin maleate 1~3 parts, calcium carbonate 4~
6 parts, vacuum stirring, vacuum-0. below 9Mpa, stirs 60~80 minutes.
The manufacture method of above-mentioned flame retardant plastic rubber roll, its described roller core is metal roller core.
Beneficial effect:
The present invention utilizes rubber roll extruder to be coated with one layer of rubber layer on roller core, utilizes again coating machine to be coated with outside rubber layer
One layer of soft PVC plastic layer, increases the protective effect to rubber layer, extends the service life of flame retardant plastic rubber roll, especially
Have at aspects such as easy cleaning, resistance to be full of cracks, use periodicity and be greatly improved.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with
Detailed description of the invention, is expanded on further the present invention.
The present invention includes metal roller core, rubber roll extruder and coating machine, and its described manufacture method comprises the steps:
1) take prefabricated metal roller core, remove metallic roll wicking surface impurity, greasy dirt, improve the adhesive effect of bonding agent;
2) open rubber roll extruder, in making the forming room of rubber roll extruder, be full of unvulcanized elastomeric material, elastomeric material
Calculating by weight, the calcium carbonate including the epoxychloropropane of 70 parts and 30 parts is mixed;
3) surface is put in order the rubber material that clean metal roller core is sent in rubber roll extruder forming room successively, with gap
In material, by the metallic roll core outer surface described in described elastomeric material cladding;
4) the metal roller core that outer surface has been coated with elastomeric material puts into enforcement vulcanizing treatment, rubber layer thickness in vulcanizer
2mm, forms rubber rollers;
5) preparation polyvinyl chloride pulp, described polyvinyl chloride pulp includes calculating by weight, Welvic tree
100 parts of fat, dioctyl phthalate 50 parts, dibutyitin maleate 2 parts, calcium carbonate 5 parts, add vacuum in de-airing mixer
Stirring, vacuum-0. 9Mpa, stirs 60 minutes, obtains polyvinyl chloride pulp;
6) rubber rollers is loaded on coating machine, preheating;
7) preparing bonding agent, described bonding agent includes that E-44 epoxy resin and low molecular weight polycaprolactone phthalein polyimide resin are by the weight of 1:1
Amount, than composition, heats 20 minutes, heating-up temperature 200 DEG C, prepared bonding agent is uniformly applied to rubber rollers outer surface;
8) polyvinyl chloride pulp is poured on coating machine coating cutter, is coated with 1~2mm polychlorostyrene second at rubber rollers outer surface
Alkene, nano flame retardant complex slurry;The preparation method of described nano flame retardant complexing agent is:
(1) by silicone hydroxyl apatite, red phosphorus, attapulgite, brucite, montmorillonite, titanium dioxide, calcite, Kaolin according to
The mass fraction proportioning mixing of 25-35:15-20:10-15: 10-15:8-10:8-10:7-8:5-7, joins 200 parts of diformazans
In the mixed solution of sulfoxide (DMSO) and 50 parts of methanol, stir 60 hours in 65 DEG C, filter, and wash with the hot ethanol of 60 DEG C of temperature
The dimethyl sulfoxide (DMSO) that 3 times remove excess, puts into vacuum drying oven, is dried 24 hours 60 DEG C of temperature, and grinding is sieved, and obtains one
Secondary modified flame-retardant complex;
(2), by 1 part of modified flame-retardant complex, 10 parts of potassium acetates and 25 parts of distilled water mixing, stir in temperature 50 C
More than 10 hours, in temperature 30 DEG C, first disperse 2.5 hours under the conditions of ultrasonic electric power 350W, the most again at ultrasonic electric power
Disperse 3 hours under the conditions of 250W.Filtering, and wash 3 times with distillation, 80 DEG C are vacuum dried 24 hours, and grinding is sieved, and obtains secondary and changes
Property flame-retardant compounds;
(3), above-mentioned 1 part of twice-modified flame-retardant compounds is disperseed 40min at 600W power ultrasonic, fill by heated at constant temperature
Put and be heated to 90 DEG C, and stir (1200r/min) 60 minutes with mechanical agitator;Obtain nano flame retardant complex;
10) turning has been coated with the flame retardant plastic rubber roll of polyvinyl chloride pulp so that it is smooth outer surface, and cleans polishing,
I.e. can make flame retardant plastic rubber roll.
The present invention utilizes rubber roll extruder to be coated with one layer of rubber layer on roller core, utilizes again coating machine to be coated with outside rubber layer
One layer of soft PVC plastic layer, increases the protective effect to rubber layer, extends the service life of flame retardant plastic rubber roll, especially
Have at aspects such as easy cleaning, resistance to be full of cracks, use periodicity and be greatly improved.
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these become
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and
Equivalent defines.
Claims (5)
1. a manufacture method for flame retardant plastic rubber roll, said method with roller core as raw material, the equipment of employing be rubber roll extruder and
Coating machine, it is characterised in that described manufacture method comprises the steps:
1) kicker cylinder wicking surface impurity;
2) unvulcanized elastomeric material it is full of in the forming room of rubber roll extruder;
3) roller core is sent to the most with gap in the elastomeric material in rubber roll extruder forming room, by described elastomeric material bag
Cover described roller core outer surface;
4) roller core that outer surface has been coated with elastomeric material puts into enforcement vulcanizing treatment in vulcanizer, rubber layer thickness 2mm, is formed
Rubber rollers;
5) preparation polyvinyl chloride pulp;
6) rubber rollers is loaded on coating machine, preheating;
7) bonding agent is uniformly applied to rubber rollers outer surface;
8) polyvinyl chloride pulp is poured on coating machine coating cutter on, rubber rollers outer surface be coated with 1~2mm polrvinyl chloride,
Nano flame retardant complex slurry;The preparation method of described nano flame retardant complex is:
(1) by silicone hydroxyl apatite, red phosphorus, attapulgite, brucite, montmorillonite, titanium dioxide, calcite, Kaolin according to 25-35
: the mass fraction proportioning mixing of 15-20: 10-15: 10-15: 8-10: 8-10: 7-8: 5-7, join 200 part two
In the mixed solution of first sulfoxide (DMSO) and 50 parts of methanol, stir 60 hours in 65 DEG C, filter, and by the heat of 60 DEG C of temperature
The dimethyl sulfoxide (DMSO) removing excess washed 3 times by ethanol, puts into vacuum drying oven, is dried 24 hours 60 DEG C of temperature, grinds
Sieve, obtain a modified flame-retardant complex;
(2) by 1 part of modified flame-retardant complex, 10 parts of potassium acetates and 25 parts of distilled water mixing, 10 are stirred in temperature 50 C
More than hour, in temperature 30 DEG C, first disperse 2.5 hours under the conditions of ultrasonic electric power 350W, the most again at ultrasonic electric power
Disperseing 3 hours under the conditions of 250W, filter, and wash 3 times with distillation, 80 DEG C are vacuum dried 24 hours, and grinding is sieved, and obtains two
Secondary modified flame-retardant complex;
(3) above-mentioned twice-modified flame-retardant compounds is disperseed 40min at 600W power ultrasonic, heat with constant temperature heating device
To 90 DEG C, and stir 60 minutes with 1200r/min with mechanical agitator;Obtain nano flame retardant complex;
9), after cooling, step 8) 2 times are repeated;
10) turning outer surface, and clean polishing.
2. according to the manufacture method of the flame retardant plastic rubber roll described in claim 1, it is characterised in that described elastomeric material is by weight
Amount number calculates, and the calcium carbonate including the epoxychloropropane of 50~70 parts and 30~50 parts is mixed.
3. according to the manufacture method of the flame retardant plastic rubber roll described in claim 1, it is characterised in that described bonding agent includes E-
44 epoxy resin, E-54 epoxy resin or 630 epoxy resin and low molecular weight polycaprolactone phthalein polyimide resin press the weight ratio composition of 1:1,
Heat 10~20 minutes, heating-up temperature 180~220 DEG C.
4. according to the manufacture method of the flame retardant plastic rubber roll described in claim 1, it is characterised in that described polyvinyl chloride pulp
Including calculating by weight, PVC paste resin 80~120 parts, dioctyl phthalate 50~70 parts, horse
Come sour dibutyl tin 1~3 parts, calcium carbonate 4~6 parts, vacuum stirring, vacuum-0. below 9Mpa, stirring 60~
80 minutes.
5. according to the manufacture method of the flame retardant plastic rubber roll described in claim 1, it is characterised in that described roller core is metallic roll
Core.
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CN104043570B (en) * | 2014-07-01 | 2015-09-16 | 国家电网公司 | The coated guard method of a kind of transmission tower spraying hot melt high molecular polymer |
CN104646434A (en) * | 2015-02-11 | 2015-05-27 | 苏州市宝苏矿冶设备有限公司 | Particle rubber roll and manufacturing method thereof |
CN105437816A (en) * | 2015-12-21 | 2016-03-30 | 无锡科莱欣机电制造有限公司 | Printing and dyeing rubber roller sleeve for printing and dyeing machine |
CN105437817A (en) * | 2015-12-21 | 2016-03-30 | 无锡科莱欣机电制造有限公司 | Anti-abrasive rubber roller sleeve for printing and dyeing machine |
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CN101559667A (en) * | 2009-05-14 | 2009-10-21 | 中国印钞造币总公司 | Polyvinyl chloride plastic/rubber inking roller and preparation method thereof |
CN102002141A (en) * | 2010-11-19 | 2011-04-06 | 安徽大学 | Preparation method of polyurethane-nano kaolin composite material |
DE102009045751A1 (en) * | 2009-10-16 | 2011-04-21 | Manroland Ag | Printing machine-coating system for coating of printing machine components such as printing machine cylinder, printing machine rollers, printing machine protector or printing machine walls, comprises a coating base material |
CN102179937A (en) * | 2010-12-27 | 2011-09-14 | 东莞市新志密封技术有限公司 | Processing method and processing device for rubber tube material molding |
CN103112142A (en) * | 2011-11-16 | 2013-05-22 | 富士施乐株式会社 | Rubber roller manufacturing apparatus and rubber roller manufacturing method |
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JP3394404B2 (en) * | 1996-12-26 | 2003-04-07 | 三菱製紙株式会社 | Backing base material for flooring and method of manufacturing the same |
JP2000213082A (en) * | 1999-01-25 | 2000-08-02 | Sekisui Chem Co Ltd | Fire-resistant coating material |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN101559667A (en) * | 2009-05-14 | 2009-10-21 | 中国印钞造币总公司 | Polyvinyl chloride plastic/rubber inking roller and preparation method thereof |
DE102009045751A1 (en) * | 2009-10-16 | 2011-04-21 | Manroland Ag | Printing machine-coating system for coating of printing machine components such as printing machine cylinder, printing machine rollers, printing machine protector or printing machine walls, comprises a coating base material |
CN102002141A (en) * | 2010-11-19 | 2011-04-06 | 安徽大学 | Preparation method of polyurethane-nano kaolin composite material |
CN102179937A (en) * | 2010-12-27 | 2011-09-14 | 东莞市新志密封技术有限公司 | Processing method and processing device for rubber tube material molding |
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Effective date of registration: 20170302 Address after: 226400 Rudong City, Jiangsu Province, Yang Kou Chemical Industrial Park Patentee after: Jiangsu Xiangyuan Chemical Co., Ltd. Address before: 215100 Jiangsu, Xiangcheng District Yang Cheng lake town (Hunan City) figure ten Village Patentee before: Suzhou Xiangyuan Speical Fine Chemical Co., Ltd. |