CN103507351A - Fully anti-ultraviolet solar energy heat insulation film and making method thereof - Google Patents
Fully anti-ultraviolet solar energy heat insulation film and making method thereof Download PDFInfo
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- CN103507351A CN103507351A CN201210204998.8A CN201210204998A CN103507351A CN 103507351 A CN103507351 A CN 103507351A CN 201210204998 A CN201210204998 A CN 201210204998A CN 103507351 A CN103507351 A CN 103507351A
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Abstract
The invention discloses a fully anti-ultraviolet solar energy heat insulation film. The main structure of the fully anti-ultraviolet solar energy heat insulation film comprises a scratch-resistant layer, a main film, a polyurethane adhesive layer, a nano material layer, a polyethylene terephthalate (PET) base material, a mounting adhesive layer, a mounting adhesive protection film. The fully anti-ultraviolet solar energy heat insulation film uses a special nano material, the infrared ray shielding rate of the prepared fully anti-ultraviolet solar energy heat insulation film reaches 90%, and the ultraviolet ray resistant rate reaches 99%. The fully anti-ultraviolet solar energy heat insulation film also has the ability to effectively shield electromagnetic waves. The special nano material layer includes any one of a nano metal, a nano oxide, a nano nitride, a nano carbide, a nano fluoride, a nano sulfide, a nano antimonide, a nano selenide and a nano telluride or a composition of any two or more the above inorganic compounds. The fully anti-ultraviolet solar energy heat insulation film can be made into colorless or colored transparent products, is beautiful and clear, and can be widely applied to installation and use of automobile glass and construction glass. A making method of the fully anti-ultraviolet solar energy heat insulation film provided by the invention is simple, is easy to operate and suitable for industrial production.
Description
Technical field
The present invention relates to a kind of diaphragm, relate to specifically a kind of fully anti-ultraviolet solar energy thermal isolation film that shields electromagnetic wave and elimination static and preparation method thereof.
Background technology
Goal of the invention: the object of the invention is to overcome the deficiencies in the prior art, provide a kind of easy installation, anti-scraping, get rid of bubble fast, and can shield electromagnetic wave, eliminate the solar energy thermal isolation film of static, reflected infrared ray and fully anti-ultraviolet.
Technical scheme: to achieve these goals, the invention provides fully anti-ultraviolet solar energy thermal isolation film, it comprises: anti-scratch layer (1), main film PET base material (2), polyurethane glue-line (3), layer of nanomaterial (4), PET base material (5), installation glue-line (6), installation glue diaphragm PET base material (7);
Wherein, be coated with layer of nanomaterial (4) on the non-corona surface of PET base material (5), be coated with polyurethane glue-line (3) on the corona surface of main film PET base material (2), layer of nanomaterial (4) is compound with polyurethane glue-line (3); On the corona surface of PET base material (5), glue-line (6) is installed in coating, glue diaphragm PET base material (7) is installed compound with it; On the non-corona surface of main film PET base material (2), be coated with anti-scratch layer (1);
Described layer of nanomaterial (4) is the combination of any one or any two or more inorganic compounds in nano metal, nano-oxide, nano nitride, nano-carbide, nano fluoride, nanometer sulfide, nanometer antimonide, nanometer selenium compound, nano tellurium compound.
Described nano metal is tungsten; Described nano-oxide is selected from one or more in tin indium oxide, titanium dioxide, vanadium dioxide, aluminium oxide, tri-iron tetroxide or zinc oxide; Nano nitride is Nano titanium nitride; Nano-carbide is nano titanium carbide; Nano fluoride is nanometer magnesium fluoride; Nanometer sulfide is nano-zinc sulfide; Nanometer antimonide is nano antimony tin oxide; Nanometer selenium compound is cadmium selenide; Nano tellurium compound is nano tellurium cadmium.
The nano material particle size range of described layer of nanomaterial (4) is 1 ~ 300nm.
Described layer of nanomaterial (4) is combined closely by magnetron sputtering method, high temperature deposition method or chemical deposition and PET base material (5).By above-mentioned magnetron sputtering method, high temperature deposition method or chemical deposition and PET base material (5), combine closely, thereby make common PET base material (5) there is the ability of shielding electromagnetic wave, elimination static, reflected infrared ray and fully anti-ultraviolet.
The preparation method that above-mentioned fully anti-ultraviolet solar energy thermal isolation film is also provided in the present invention, the concrete steps of preparation method are as follows:
(1), on the non-corona surface of the PET of 16 um~36um base material (5) by magnetron sputtering method, high temperature deposition method or chemical deposition be coated with at least more than one deck, every layer thickness is the layer of nanomaterial (4) of 2 um~3 um;
(2), on the corona surface of the main film PET base material (2) of 16um~36um, be coated with the polyurethane glue-line (3) of one deck 4um~20um, again that layer of nanomaterial (4) and polyurethane glue-line (3) is compound, then on the corona surface of PET base material (5), be coated with the installation glue-line (6) of one deck 10um~40 um;
(3), with release of the installation glue diaphragm PET base material (7) of 12 um~50 um with that glue-line (6) is installed is compound;
(4) by the anti-scratch layer (1) of UV equipment coating one deck 2 um~8 um, obtain product of the present invention and then in an other side of main film PET base material (2).
Beneficial effect: fully anti-ultraviolet solar energy thermal isolation film of the present invention, adopt special nano material, infrared shield rate reaches more than 90%, and uvioresistant reaches more than 99%, has the electromagnetic ability of effective shielding simultaneously; The present invention can be made into colourless or colored transparent product, attractive in appearance, clear, can be widely used in installing and using of various vehicle glasses, building glass; The preparation method of fully anti-ultraviolet solar energy thermal isolation film of the present invention is simple, easy to operate, is applicable to industrial production.
Accompanying drawing explanation
Accompanying drawing is the structural representation of fully anti-ultraviolet solar energy thermal isolation film of the present invention.
The specific embodiment
Below in conjunction with specific embodiment, further illustrate the present invention, should understand these embodiment is only not used in and limits the scope of the invention for the present invention is described, after having read the present invention, those skilled in the art all fall within the application's claims to the modification of the various equivalent form of values of the present invention and limit.
A solar energy thermal isolation film, it comprises: the installation glue-line (6) that the main film PET base material (2) that thickness is 23um, the PET base material (5) that thickness is 23um, anti-scratch layer (1) that installation glue diaphragm PET base material (7), thickness that thickness is 23um are 3um, polyurethane glue-line (3) that thickness is 8um, layer of nanomaterial (4) that thickness is 8um and thickness are 8um; In the present embodiment, diaphragm glue-line (2), anti-scratch layer (3) are all acrylic resins with installation glue-line (6) employing; What polyurethane glue-line (5) adopted is polyurethanes resin; Layer of nanomaterial (4) adopts is that in polyurethane, polyester, acrylate or alkyd resins, in any one glue, to add average grain diameter be the nanometer tungsten of 30nm and the mixture of the nano vanadium dioxide that average grain diameter is 50nm, and these two kinds of materials mix with arbitrary proportion; Average grain diameter is the nanometer magnesium fluoride of 50nm and the mixture of the nano tellurium cadmium that average grain diameter is 50nm, and these two kinds of materials mix with arbitrary proportion; Average grain diameter is the nano titanium oxide of 40nm and the mixture of the nano aluminium oxide that average grain diameter is 60nm, and these two kinds of materials mix with arbitrary proportion.
The preparation method concrete steps of above-mentioned fully anti-ultraviolet solar energy thermal isolation film are as follows:
(1), on the non-corona surface of the PET of 23um base material (5), by magnetron sputtering method, be coated with the layer of nanomaterial that the mixture of the nano vanadium dioxide that nanometer tungsten that average grain diameter that one deck 2 um are thick is 30nm and average grain diameter are 50nm forms; The layer of nanomaterial that the mixture of the nano tellurium cadmium that the nanometer magnesium fluoride that to be again coated with average grain diameter that one deck 4um is thick in this layer of nanomaterial be 50nm and average grain diameter are 50nm forms; It is last that to be coated with a layer thickness be in the above average grain diameter that 2um the is thick nano titanium oxide that is 40nm again and the layer of nanomaterial of the mixture formation of the average grain diameter nano aluminium oxide that is 60nm, these three layers of layer of nanomaterial can reach infrared shield rate 92%, rate of ultraviolet shield 99.9%, the ability of full anti electromagnetic wave;
(2), on the corona surface of the main film PET base material (2) of 23um, be coated with the polyurethane glue-line (3) of one deck 8um; Compound with layer of nanomaterial (4) and polyurethane glue-line (3); And then on the corona surface of the PET of 23um base material (5), be coated with the installation glue-line (6) of one deck 8um; In described polyurethane glue-line (3) and installation glue-line (6), all contain 1%~3% ultra-violet absorber;
(3), with release of the installation glue diaphragm PET base material (7) of 23um with that glue-line (6) is installed is compound;
(4), then on the non-corona surface of the main film PET base material (2) of 23um, be coated with the anti-scratch layer (1) of one deck 3um, obtain product described in the present embodiment.
A solar energy thermal isolation film, it comprises: the installation glue-line (6) that the main film PET base material (2) that thickness is 23um, the PET base material (5) that thickness is 23um, anti-scratch layer (1) that installation glue diaphragm PET base material (7), thickness that thickness is 23um are 4um, polyurethane glue-line (3) that thickness is 8um, layer of nanomaterial (4) that thickness is 6um and thickness are 8um; In the present embodiment, diaphragm glue-line (2), anti-scratch layer (3) are all acrylic resins with installation glue-line (6) employing; What polyurethane glue-line (5) adopted is polyurethanes resin; Layer of nanomaterial (4) adopts is that in polyurethane, polyester, acrylate or alkyd resins, in any one glue, to add average grain diameter be the nano-indium stannum oxide of 50nm and the mixture of the nano zine oxide that average grain diameter is 40nm, and these two kinds of materials mix with arbitrary proportion; Average grain diameter is the nano antimony tin oxide of 80nm and the mixture of the nano silicon that average grain diameter is 60nm, and these two kinds of materials mix with arbitrary proportion; Average grain diameter is the nano ferriferrous oxide of 40nm and the mixture of the Nano titanium nitride that average grain diameter is 30nm, and these two kinds of materials mix with arbitrary proportion.
The preparation method concrete steps of above-mentioned fully anti-ultraviolet solar energy thermal isolation film are as follows:
(1), on the non-corona surface of the PET of 23um base material (5), by magnetron sputtering method, be coated with the layer of nanomaterial that the mixture of the nano zine oxide that nano-indium stannum oxide that average grain diameter that one deck 2 um are thick is 50nm and average grain diameter are 40nm forms; The layer of nanomaterial that the mixture of the nano silicon that the nano antimony tin oxide that to be again coated with average grain diameter that one deck 2um is thick in this layer of nanomaterial be 80nm and average grain diameter are 60nm forms; Last is average grain diameter that 2um the is thick nano ferriferrous oxide that is 40nm and the layer of nanomaterial of the mixture formation of the average grain diameter Nano titanium nitride that is 30nm by chemical vapor deposition method coating a layer thickness more in the above, these three layers of layer of nanomaterial can reach infrared shield rate 95%, rate of ultraviolet shield 99.9%, the ability of full anti electromagnetic wave;
(2), on the corona surface of the main film PET base material (2) of 23um, be coated with the polyurethane glue-line (3) of one deck 8um; Compound with layer of nanomaterial (4) and polyurethane glue-line (3); And then on the corona surface of the PET of 23um base material (5), be coated with the installation glue-line (6) of one deck 8um; In described polyurethane glue-line (3) and installation glue-line (6), all contain 1%~3% ultra-violet absorber;
(3), with release of the installation glue diaphragm PET base material (7) of 23um with that glue-line (6) is installed is compound;
(4), then on the non-corona surface of the main film PET base material (2) of 23um, be coated with the anti-scratch layer (1) of one deck 4um, obtain product described in the present embodiment.
Claims (10)
1. a fully anti-ultraviolet solar energy thermal isolation film, is characterized in that: it comprises: anti-scratch layer (1), main film PET base material (2), polyurethane glue-line (3), layer of nanomaterial (4), PET base material (5), installation glue-line (6), installation glue diaphragm PET base material (7);
Wherein, be coated with layer of nanomaterial (4) on the non-corona surface of PET base material (5), be coated with polyurethane glue-line (3) on the corona surface of main film PET base material (2), layer of nanomaterial (4) is compound with polyurethane glue-line (3); On the corona surface of PET base material (5), glue-line (6) is installed in coating, glue diaphragm PET base material (7) is installed compound with described installation glue-line (6); On the non-corona surface of main film PET base material (2), be coated with anti-scratch layer (1);
Wherein, the nano material in described layer of nanomaterial (4) is the composition of any one or any two or more inorganic compounds in nano metal, nano-oxide, nano nitride, nano-carbide, nano fluoride, nanometer sulfide, nanometer antimonide, nanometer selenium compound, nano tellurium compound.
2. a kind of fully anti-ultraviolet solar energy thermal isolation film according to claim 1, is characterized in that: described nano metal is tungsten; Described nano-oxide is one or more in tin indium oxide, titanium dioxide, vanadium dioxide, aluminium oxide, tri-iron tetroxide or zinc oxide; Nano nitride is Nano titanium nitride; Nano-carbide is nano titanium carbide; Nano fluoride is nanometer magnesium fluoride; Nanometer sulfide is nano-zinc sulfide; Nanometer antimonide is nano antimony tin oxide; Nanometer selenium compound is cadmium selenide; Nano tellurium compound is nano tellurium cadmium.
3. a kind of fully anti-ultraviolet solar energy thermal isolation film according to claim 2, is characterized in that: the nano material particle size range of described layer of nanomaterial (4) is 1 ~ 300nm.
4. according to a kind of fully anti-ultraviolet solar energy thermal isolation film described in claims 1 to 3 any one, it is characterized in that: described layer of nanomaterial (4) is combined closely by magnetron sputtering method, high temperature deposition method or chemical deposition and PET base material (5).
5. a kind of fully anti-ultraviolet solar energy thermal isolation film according to claim 4, is characterized in that: in described polyurethane glue-line and installation glue-line, have at least one deck to contain ultra-violet absorber.
6. fully anti-ultraviolet solar energy thermal isolation film according to claim 1, is characterized in that: each described rete, the thickness of each glue-line are respectively:
Anti-scratch layer (1) 2 um~8 um
Main film PET base material (2) 16 um~36 um
Polyurethane glue-line (3) 4 um~20 um
Layer of nanomaterial (4) 2 um~30um
PET base material (5) 16 um~36 um
Glue-line (6) 10 um~40 um are installed
Glue diaphragm (7) 12 um~50 um are installed.
7. fully anti-ultraviolet solar energy thermal isolation film according to claim 1, is characterized in that: what described anti-scratch layer (1), layer of nanomaterial (4), installation glue-line (6) adopted is all silicone based resin or acrylic resin.
8. fully anti-ultraviolet solar energy thermal isolation film according to claim 1, is characterized in that: main film PET base material (2), compound main film PET base material (5), installation glue diaphragm (7) are PET film.
9. fully anti-ultraviolet solar energy thermal isolation film according to claim 1, is characterized in that: the light transmittance of described PET film is more than 92%, mist degree < 1%.
10. a preparation method for fully anti-ultraviolet solar energy thermal isolation film according to claim 1, is characterized in that: the concrete steps of preparation method are as follows:
(1), on the non-corona surface of the PET of 16 um~36um base material (5) by magnetron sputtering method, high temperature deposition method or chemical deposition be coated with at least more than one deck, every layer thickness is the layer of nanomaterial (4) of 2 um~3 um;
(2), on the corona surface of the main film PET base material (2) of 16um~36um, be coated with the polyurethane glue-line (3) of one deck 4um~20um, again that layer of nanomaterial (4) and polyurethane glue-line (3) is compound, then on the corona surface of PET base material (5), be coated with the installation glue-line (6) of one deck 10um~40 um;
(3), with release of the installation glue diaphragm PET base material (7) of 12 um~50 um with that glue-line (6) is installed is compound;
(4) by the anti-scratch layer (1) of UV equipment coating one deck 2 um~8 um, obtain product of the present invention and then in an other side of main film PET base material (2).
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Cited By (10)
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CN104139585A (en) * | 2014-07-31 | 2014-11-12 | 苏州袭麟光电科技产业有限公司 | Heat reflection film for automotive glass |
CN104178047A (en) * | 2014-08-20 | 2014-12-03 | 昆山博益鑫成高分子材料有限公司 | Flexible transparent nano heat-insulation film and preparation method thereof |
CN104760374A (en) * | 2015-03-25 | 2015-07-08 | 超膜国际环保科技有限公司 | Ceramic magnetic-control film for glass and preparation method thereof |
CN105542405A (en) * | 2016-02-19 | 2016-05-04 | 浙江紫光科技有限公司 | Thermal insulation optical thin film material |
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CN104139585A (en) * | 2014-07-31 | 2014-11-12 | 苏州袭麟光电科技产业有限公司 | Heat reflection film for automotive glass |
CN104178047A (en) * | 2014-08-20 | 2014-12-03 | 昆山博益鑫成高分子材料有限公司 | Flexible transparent nano heat-insulation film and preparation method thereof |
CN104178047B (en) * | 2014-08-20 | 2016-06-08 | 昆山博益鑫成高分子材料有限公司 | A kind of flexible and transparent nano heat-insulating film and its preparation method |
CN104760374B (en) * | 2015-03-25 | 2017-07-25 | 超膜国际环保科技有限公司 | It is a kind of for ceramic magnetic control pad pasting of glass and preparation method thereof |
CN104760374A (en) * | 2015-03-25 | 2015-07-08 | 超膜国际环保科技有限公司 | Ceramic magnetic-control film for glass and preparation method thereof |
CN105542405A (en) * | 2016-02-19 | 2016-05-04 | 浙江紫光科技有限公司 | Thermal insulation optical thin film material |
CN105542405B (en) * | 2016-02-19 | 2018-05-08 | 浙江紫光科技有限公司 | A kind of heat-insulated optical film materials |
CN106003946A (en) * | 2016-06-30 | 2016-10-12 | 广东新视野薄膜有限公司 | Full ultraviolet-proof skin-protecting film and preparation method |
CN108047902A (en) * | 2017-11-28 | 2018-05-18 | 马鞍山蓝科再制造技术有限公司 | It is a kind of that there is the nano material for absorbing action of ultraviolet radiation |
CN108016101A (en) * | 2017-12-15 | 2018-05-11 | 东莞市达瑞电子股份有限公司 | A kind of MULTILAYER COMPOSITE high transparency protective film and preparation method thereof |
CN111944440A (en) * | 2020-06-29 | 2020-11-17 | 浙江欣麟新材料技术有限公司 | Bactericidal explosion-proof heat-insulation film for automobile, building glass and high-speed rail |
CN112048252A (en) * | 2020-08-26 | 2020-12-08 | 江苏鼎胜新能源材料股份有限公司 | Cold roofing that PET modified film prepared |
CN113214753A (en) * | 2021-04-30 | 2021-08-06 | 浙江紫光科技有限公司 | Low-light-transmission window film capable of reflecting near infrared rays and preparation method thereof |
CN113214753B (en) * | 2021-04-30 | 2023-02-28 | 浙江紫光科技有限公司 | Low-light-transmission window film capable of reflecting near infrared rays and preparation method thereof |
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