CN103485180B - The method for sizing of camp bed OXFORD - Google Patents
The method for sizing of camp bed OXFORD Download PDFInfo
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- CN103485180B CN103485180B CN201310454070.XA CN201310454070A CN103485180B CN 103485180 B CN103485180 B CN 103485180B CN 201310454070 A CN201310454070 A CN 201310454070A CN 103485180 B CN103485180 B CN 103485180B
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Abstract
The invention discloses a kind of method for sizing of camp bed OXFORD, comprise the preparation of performed polymer, the preparation of slurry, the preliminary treatment of OXFORD, slashing operation, hang steps such as draining.Adopt method for sizing of the present invention to arrange OXFORD, there is the advantages such as coverage rate is high, increase fabric intensity.
Description
Technical field
The present invention relates to a kind for the treatment of process of fabric, be specifically related to a kind of method for sizing of camp bed OXFORD.
Background technology
OXFORD is as a kind of fabric of high strength, also be widely used in except daily case and bag in the outdoor goods such as tent and camp bed, the high strength of OXFORD itself can keep long-term effectively under indoor environment, but out of doors under service condition, be subject to sunshine direct projection, thermal shock, and light, heat, wet comprehensive function, easily cause fading of dyestuff to decline with the intensity of fabric fibre, at present the weather resisteant adopting the mode of coating to strengthen OXFORD more.No matter adopt roller coat or the mode sprayed, the complexity of its equipment, technique is all higher.And clothes arrange the sizing technique operation relative ease of the maturation adopted at present, but formula of size significantly can increase the weight of fabric, and to fabric intensity, the humidification of surface coverage is limited, limits application.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the invention provides the high method for sizing that also can increase the camp bed OXFORD of fabric intensity of a kind of coverage rate.
Technical scheme: for solving the problems of the technologies described above, the method for sizing of camp bed OXFORD provided by the invention, comprises the following steps:
1) preparation of performed polymer, by the polyethylene glycol 3 ~ 6 parts according to weight proportion, ethyl acrylate 0.7 ~ 2 part, polyvinyl acetate 4 ~ 7 parts, toluene di-iso-cyanide ester 1 ~ 3 part, adds reactor, add 10 ~ 15 parts of acetone and make solvent, stirring is warming up to 70 DEG C of reaction 4h and obtains performed polymer;
2) preparation of slurry, by the weight ratio thin up of step 1) gained performed polymer according to 1:50 ~ 70, and add in solution after dilution percetage by weight be 2% ~ 4% crosslinking agent obtain slurry;
3) preliminary treatment of OXFORD, adopts the N-methyl oil acylamino-ethylsulfonic acid sodium water solution of 2% to carry out rinsing to OXFORD;
4) slashing operation, immerses step 2 by OXFORD rinsed for step 3)) in the slurry prepared, heat slurry and maintain the temperature at 40 ~ 60 DEG C, dip time is 1.5 ~ 3h;
5) suspension drains, and the OXFORD after dipping is hung on the top of heating tank, utilizes heating tank to reclaim slurry, utilizes gravity-flow ventilation to dry.
As preferably, the temperature of flooding in step 4) is 50 DEG C.
As preferably, in described slurry, the concentration of crosslinking agent is 3%.
Beneficial effect: the present invention adopts the method for operating of starching to arrange OXFORD, simplifies the technique of arrangement, and after process, weight increases few, coverage rate is high, and humidification is remarkable.
Detailed description of the invention
Embodiment 1
Get the 420D OXFORD of 2m*2m, adopt following steps to carry out starching:
1) preparation of performed polymer, by the polyethylene glycol 3 parts according to weight proportion, ethyl acrylate 0.7 part, polyvinyl acetate 4 parts, toluene di-iso-cyanide ester 1 part, adds reactor, adds 10 parts of acetone and makees solvent, and stirring is warming up to 70 DEG C of reaction 4h and obtains performed polymer;
2) preparation of slurry, by the weight ratio thin up of step 1) gained performed polymer according to 1:50, and add in solution after dilution percetage by weight be 2% crosslinking agent obtain slurry;
3) preliminary treatment of OXFORD, adopts the N-methyl oil acylamino-ethylsulfonic acid sodium water solution of 2% to carry out rinsing to OXFORD;
4) slashing operation, immerses step 2 by OXFORD rinsed for step 3)) in the slurry prepared, heat slurry and maintain the temperature at 60 DEG C, dip time is 3h;
5) suspension drains, and the OXFORD after dipping is hung on the top of heating tank, utilizes heating tank to reclaim slurry, utilizes gravity-flow ventilation to dry.
Embodiment 2
Get the 420D OXFORD of 2m*2m, adopt following steps to carry out starching:
1) preparation of performed polymer, by the polyethylene glycol 6 parts according to weight proportion, ethyl acrylate 2 parts, polyvinyl acetate 7 parts, toluene di-iso-cyanide ester 3 parts, adds reactor, adds 15 parts of acetone and makees solvent, and stirring is warming up to 70 DEG C of reaction 4h and obtains performed polymer;
2) preparation of slurry, by the weight ratio thin up of step 1) gained performed polymer according to 1:70, and add in solution after dilution percetage by weight be 3% crosslinking agent obtain slurry;
3) preliminary treatment of OXFORD, adopts the N-methyl oil acylamino-ethylsulfonic acid sodium water solution of 2% to carry out rinsing to OXFORD;
4) slashing operation, immerses step 2 by OXFORD rinsed for step 3)) in the slurry prepared, heat slurry and maintain the temperature at 50 DEG C, dip time is 1.5h;
5) suspension drains, and the OXFORD after dipping is hung on the top of heating tank, utilizes heating tank to reclaim slurry, utilizes gravity-flow ventilation to dry.
Wherein crosslinking agent can be the conventional various crosslinking agents in this area, as based on 1,3-dihydroxymethyl-4,5-dihydroxy ethylene carbamide resin (DMDHEU) and derivative thereof.
Weigh before and after starching process, test intensity, obtain data as follows:
Before process | Embodiment 1 | Embodiment 2 | |
Weight | 402g | 410g | 413g |
Tensile strength | 198NT | 220NT | 241NT |
Visible, the weightening finish of method for sizing of the present invention to OXFORD is not obvious, effectively improves tearing strength and fracture strength.
Claims (1)
1. a method for sizing for camp bed OXFORD, is characterized in that comprising the following steps:
1) preparation of performed polymer, by the polyethylene glycol 3 ~ 6 parts according to weight proportion, ethyl acrylate 0.7 ~ 2 part, polyvinyl acetate 4 ~ 7 parts, toluene di-iso-cyanide ester 1 ~ 3 part, adds reactor, add 10 ~ 15 parts of acetone and make solvent, stirring is warming up to 70 DEG C of reaction 4h and obtains performed polymer;
2) preparation of slurry, by the weight ratio thin up of step 1) gained performed polymer according to 1:50 ~ 70, and add in solution after dilution percetage by weight be 3% crosslinking agent obtain slurry;
3) preliminary treatment of OXFORD, described camp bed OXFORD is 420D OXFORD, adopts the N-methyl oil acylamino-ethylsulfonic acid sodium water solution of 2% to carry out rinsing to OXFORD;
4) slashing operation, immerses step 2 by OXFORD rinsed for step 3)) in the slurry prepared, heat slurry and maintain the temperature at 50 DEG C, dip time is 1.5 ~ 3h;
5) suspension drains, and the OXFORD after dipping is hung on the top of heating tank, utilizes heating tank to reclaim slurry, utilizes gravity-flow ventilation to dry.
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Citations (4)
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CN101481443A (en) * | 2009-01-23 | 2009-07-15 | 华南理工大学 | Polyurethane-polyacrylacid ester interpenetrating network polymer, preparation and use thereof |
CN102392360A (en) * | 2011-08-25 | 2012-03-28 | 吴江市北厍盛源纺织品助剂厂 | Fabric coating slurry prepared by modified polyurethane |
CN102433758A (en) * | 2011-08-25 | 2012-05-02 | 吴江市北厍盛源纺织品助剂厂 | Fabric coating slurry prepared by modified environment-friendly polyurethane |
EP2530199A1 (en) * | 2010-01-20 | 2012-12-05 | Toray Industries, Inc. | Carbon fiber bundles |
Family Cites Families (4)
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US5173526A (en) * | 1991-04-26 | 1992-12-22 | Air Products And Chemicals, Inc. | Aqueous polyurethane-vinyl polymer dispersions for coating applications |
US6787226B2 (en) * | 2001-10-23 | 2004-09-07 | Asahi Fiber Glass Company Limited | Chopped strands and molded product of unsaturated polyester resin BMC employing them |
EP2348061A1 (en) * | 2010-01-21 | 2011-07-27 | Bayer MaterialScience AG | Method for producing water emulsion polyurethane polyacrylate hybrid systems |
CN102977282B (en) * | 2012-12-06 | 2014-06-04 | 陕西科技大学 | Preparation method of anionic organic-solvent-free and emulsifier-free polyurethane microemulsion |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101481443A (en) * | 2009-01-23 | 2009-07-15 | 华南理工大学 | Polyurethane-polyacrylacid ester interpenetrating network polymer, preparation and use thereof |
EP2530199A1 (en) * | 2010-01-20 | 2012-12-05 | Toray Industries, Inc. | Carbon fiber bundles |
CN102392360A (en) * | 2011-08-25 | 2012-03-28 | 吴江市北厍盛源纺织品助剂厂 | Fabric coating slurry prepared by modified polyurethane |
CN102433758A (en) * | 2011-08-25 | 2012-05-02 | 吴江市北厍盛源纺织品助剂厂 | Fabric coating slurry prepared by modified environment-friendly polyurethane |
Non-Patent Citations (1)
Title |
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