CN103483916A - 一种颜料红146乳液的制备方法 - Google Patents

一种颜料红146乳液的制备方法 Download PDF

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CN103483916A
CN103483916A CN201310411025.6A CN201310411025A CN103483916A CN 103483916 A CN103483916 A CN 103483916A CN 201310411025 A CN201310411025 A CN 201310411025A CN 103483916 A CN103483916 A CN 103483916A
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pigment red
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emulsion
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powder
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CN103483916B (zh
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李小福
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Wujiang Bingxin Cultural & Educational Goods Co Ltd
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Wujiang Bingxin Cultural & Educational Goods Co Ltd
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Abstract

本发明涉及一种颜料红146乳液的制备方法，制备过程步骤如下：取颜料红146粉末为15～18份，用研磨机研磨至1000目；将研磨后颜料红146粉末放入反应器中，加入乳化硅油12～16份并同时搅拌；再加入乳化剂OP-9为21～23份，同时搅拌；再加入乙二醇为11～14份，同时搅拌；再加入水为80～85份，搅拌均匀；最后使用均质机进行均质，均质压力为17MPa，均质时间为25min。制备得到的颜料红146乳液有很好的分散性和较小的粒径。

Description

一种颜料红146乳液的制备方法
技术领域
本发明涉及一种颜料乳液的制备方法，特别是涉及一种颜料红146乳液的制备方法。
背景技术
颜料性质不同，可以分为油溶性和水溶性颜料等。在颜料的应用途径中，油溶性颜料无法应用于水溶性体系中，水溶性颜料无法应用在油溶性体系中。由于上述性质的区别，限制了其应用空间。如果将油溶性颜料通过乳化的方式应用在水溶性体系中，或者将水溶性颜料通过乳化方式应用在油溶性体系中，会扩大不同性质颜料的使用范围。
发明内容
要解决的技术问题：将颜料红146应用在水溶性体系中。
技术方案：本发明公开了一种颜料红146乳液的制备方法，制备过程步骤如下：取颜料红146粉末为15～18份，用研磨机研磨至1000目；将研磨后颜料红146粉末放入反应器中，加入乳化硅油12～16份并同时搅拌；再加入乳化剂OP-9为21～23份，同时搅拌；再加入乙二醇为11～14份，同时搅拌；再加入水为80～85份，搅拌均匀；最后使用均质机进行均质，均质压力为17MPa，均质时间为25min。其中，颜料红146优选为18份；乳化硅油优选为12份；乳化剂OP-9优选为23份；乙二醇优选为11份。
有益效果：制备得到的颜料红146乳液具有良好的分散性，同时也有较小的粒径。将颜料红146乳液均匀撒入水中后，可迅速分散开，无固形物。经粒径仪测定，本发明的颜料红146乳液粒径只有12至18um。避免了常规颜料使用过程中的颗粒感。
具体实施方式
实施例1
取颜料红146粉末为15kg，用研磨机研磨至1000目；将研磨后颜料红146粉末放入反应器中，加入乳化硅油12kg并同时搅拌；再加入乳化剂OP-9为23kg，同时搅拌；再加入乙二醇为14kg，同时搅拌；再加入水为85kg，搅拌均匀；最后使用均质机进行均质，均质压力为17MPa，均质时间为25min。制备得到颜料红146乳液。
实施例2
取颜料红146粉末为16kg，用研磨机研磨至1000目；将研磨后颜料红146粉末放入反应器中，加入乳化硅油14kg并同时搅拌；再加入乳化剂OP-9为21kg，同时搅拌；再加入乙二醇为11kg，同时搅拌；再加入水为80kg，搅拌均匀；最后使用均质机进行均质，均质压力为17MPa，均质时间为25min。制备得到颜料红146乳液。
实施例3
取颜料红146粉末为18kg，用研磨机研磨至1000目；将研磨后颜料红146粉末放入反应器中，加入乳化硅油16kg并同时搅拌；再加入乳化剂OP-9为22kg，同时搅拌；再加入乙二醇为12kg，同时搅拌；再加入水为82kg，搅拌均匀；最后使用均质机进行均质，均质压力为17MPa，均质时间为25min。制备得到颜料红146乳液。
将实施例1、实施例2、实施例3的产品各取100g，倒入1000g水中，乳液迅速分散均匀，都具有良好的分散性。对实施例1、实施例2、实施例3的乳液使用粒径仪进行粒径测定，实施例1、实施例2、实施例3的粒径分别为12um、15um、18um。都具有很小的粒径，避免了常规颜料使用过程中的颗粒感。

Claims (5)

1.一种颜料红146乳液的制备方法，其特征在于制备过程步骤如下：取颜料红146粉末为15～18份，用研磨机研磨至1000目；将研磨后颜料红146粉末放入反应器中，加入乳化硅油12～16份并同时搅拌；再加入乳化剂OP-9为21～23份，同时搅拌；再加入乙二醇为11～14份，同时搅拌；再加入水为80～85份，搅拌均匀；最后使用均质机进行均质，均质压力为17MPa，均质时间为25min。
2.根据权利要求1所述的一种颜料红146乳液的制备方法，其特征在于颜料红146为18份。
3.根据权利要求1所述的一种颜料红146乳液的制备方法，其特征在于乳化硅油为12份。
4.根据权利要求1所述的一种颜料红146乳液的制备方法，其特征在于乳化剂OP-9为23份。
5.根据权利要求1所述的一种颜料红146乳液的制备方法，其特征在于乙二醇为11份。
CN201310411025.6A 2013-09-11 2013-09-11 一种颜料红146乳液的制备方法 Expired - Fee Related CN103483916B (zh)

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