CN103482888A - High-strength laminated glass manufacturing method - Google Patents

High-strength laminated glass manufacturing method Download PDF

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Publication number
CN103482888A
CN103482888A CN201310415217.4A CN201310415217A CN103482888A CN 103482888 A CN103482888 A CN 103482888A CN 201310415217 A CN201310415217 A CN 201310415217A CN 103482888 A CN103482888 A CN 103482888A
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Prior art keywords
glass
laminated glass
manufacturing
preparation
sheet
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CN201310415217.4A
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Chinese (zh)
Inventor
高源�
赵春新
刘娟娟
黎慧
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TIANJIN GUANGYUAN NEW MATERIAL TECH Co Ltd
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TIANJIN GUANGYUAN NEW MATERIAL TECH Co Ltd
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Priority to CN201310415217.4A priority Critical patent/CN103482888A/en
Publication of CN103482888A publication Critical patent/CN103482888A/en
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Abstract

The invention relates to a high-strength laminated glass manufacturing method. The high-strength laminated glass manufacturing method comprises the following steps that firstly, sheet combination is performed; EVA rubber sheets are flatly laid between two layers of tempered glass or more layers of tempered glass to carry out sheet combination; secondly, forming is performed in a composite mode; the glass undergoes sheet combination is preheated at a low temperature, and then heated at a high temperature; thirdly, cooling is performed; the glass heated at the high temperature is cooled and extracted; laminated glass is obtained. The high-strength laminated glass manufacturing method is simple in manufacturing technology and high in production efficiency. The obtained laminated glass has good weather resistance, is applicable to moisture and water-contact environments, high in anti-impact capability and transparency and can be widely applied to bath rooms, safety furniture, indoor partition plates, sightseeing elevator channels, glass guard bars and the like. A manufacturing device is simple, bubbles are not prone to occurring and glue disengagement and other phenomena are avoided.

Description

A kind of preparation method of high-strength laminated glass
Technical field
The present invention relates to a kind of preparation method of high-strength laminated glass, belong to the special glass technical field.
Background technology
Laminated glass can reduce greatly due to the broken injury caused of simple glass, thereby is widely applied to the aspects such as building doors and windows, curtain wall, noise barrier, safe furniture, glass stair.The America and Europe, most of building glass all adopts laminated glass, China's mandatory regulation, and all curtain walls and glass roof must adopt laminated glass.
CN101410341A discloses a kind of intermediate film for laminated glasses, use its laminated glass and preparation method thereof, the transparency of the laminated glass obtained, cohesiveness, penetration resistance, shock-resistance excellence, further photostabilization, weathering resistance improves and in the heating process of manufacturing, flavescence occurs hardly.But in this technical scheme, multilayer body consists of EVA layer and PVB layer, and makes laminated glass under high-temperature and high-pressure conditions, complex manufacturing, the equipment such as required autoclave also cause production cost higher, are unfavorable for enterprise's scale operation.
Summary of the invention
For addressing the above problem, the present invention proposes a kind of preparation method of high-strength laminated glass.
To achieve these goals, the present invention adopts following technical scheme.
A kind of preparation method of high-strength laminated glass, comprise the steps:
1) close sheet
Cleaning, the air-dry good toughened glass more than two or two and the EVA film between toughened glass are placed in to glass evacuated heat seal laminated rubber machine in clean room and are closed sheet;
Close in the sheet process and require that toughened glass keeps flat, the tiling of EVA film;
The thickness of described toughened glass is 5-12mm; Preferred 6-8mm;
Described EVA film is the commercially available film that can realize the object of the invention understood by one of ordinary skill in the art.
The thickness of described film is 0.38-0.76mm, preferably 0.38mm;
In order to obtain high strength, strong shock resistance, can control again the proportion of laminated glass simultaneously in certain tolerance range, described toughened glass layer is no more than 4 layers;
2) composite molding
By the first low-temperature prewarming of glass closed after sheet, then heat;
3) cooling
By the glass cools after heat, take out, obtain laminated glass.
In above-mentioned preparation method, in step 1), the described sheet condition of closing is: vacuum tightness 0.08-0.095MPa, 25 ℃ of temperature, humidity<30%;
In step 2) in, described low-temperature prewarming step is at 40-60 ℃ of lower preheating 10-40min; Described heat step for heating 80-120min under 100-110 ℃;
In step 3), described cooling temperature is 40-60 ℃, preferably 50 ℃;
The preparation technology of high-strength laminated glass of the present invention is simple, production efficiency is high, the laminated glass obtained, there is good weathering resistance, be applicable to environment moist and that contact with water, the phenomenons such as strong shock resistance, transparency is high, production unit is simple, be difficult for producing bubble, come unstuck, can be widely used in shower room, safe furniture, indoor partition, sightseeing elevator passage, glass guardrail etc.
The accompanying drawing explanation
The laminated glass structural representation that Fig. 1 is the embodiment of the present invention 1.
The laminated glass structural representation that Fig. 2 is the embodiment of the present invention 2.
Embodiment
Following examples are used for the present invention is described, but are not used for limiting the scope of the invention.
Embodiment 1
1) close sheet: be that 0.38mmEVA film 2 is laid between two toughened glass 1 that cleaning, air-dry good thickness are 6mm by two thickness, be placed in glass evacuated heat seal laminated rubber machine and closed sheet;
The described sheet condition of closing is: vacuum tightness 0.092MPa, 25 ℃ of temperature, humidity<30%;
2) composite molding: will close the first low-temperature prewarming of glass after sheet, then heat;
Described low-temperature prewarming step is at 50 ℃ of lower preheating 30min; Described heat step for heating 90min under 100 ℃;
3) cooling: as by ℃ taking-up of the glass cools to 50 after heat, to obtain laminated glass.
As shown in Figure 1, this laminated glass is applicable to shower house, glass stair, sightseeing elevator, partition, glass sunlight house etc. to gained laminated glass structure.
Embodiment 2
1) close sheet: be that 0.38mm EVA film 2 is laid between 4 toughened glass 1 that cleaning, air-dry good thickness are 8mm by three thickness, be placed in glass evacuated heat seal laminated rubber machine and closed sheet;
The described sheet condition of closing is: vacuum tightness 0.095MPa, 25 ℃ of temperature, humidity<30%;
2) composite molding: will close the first low-temperature prewarming of glass after sheet, then heat;
Described low-temperature prewarming step is at 50 ℃ of lower preheating 40min; Described heat step for heating 110min under 100 ℃;
3) cooling: as by ℃ taking-up of the glass cools to 50 after heat, to obtain laminated glass.
As shown in Figure 2, this laminated glass is applicable to fish jar, aquarium viewing window, platform corridor, glass floor plate and stage etc. to gained laminated glass structure.
Embodiment 3
1) close sheet: be that 0.38mm EVA film is laid between 4 toughened glass that cleaning, air-dry good thickness are 12mm by three thickness, be placed in glass evacuated heat seal laminated rubber machine and closed sheet;
The described sheet condition of closing is: vacuum tightness 0.095MPa, 25 ℃ of temperature, humidity<30%;
2) composite molding: will close the first low-temperature prewarming of glass after sheet, then heat;
Described low-temperature prewarming step is at 50 ℃ of lower preheating 40min; Described heat step for heating 110min under 110 ℃;
3) cooling: as by ℃ taking-up of the glass cools to 50 after heat, to obtain laminated glass.
Gained laminated glass can be used as splinter-proof glass, is widely used in the important places such as the sales counter of the units such as bank, postal service, telecommunications, security, insurance and museum, archives, high-end residential, prison.
Experimental example
By the laminated glass described in CN101410341A as a comparison case 1, carry out simultaneous test with embodiment of the present invention 1-3 laminated glass, result is as shown in table 1.Table 1 embodiment 1-3 and reference examples 1 performance comparison
Figure BDA0000381362960000041
As shown in Table 1, the described laminated glass of embodiment 1-3 is than Comparative Examples 1, and preparation technology is simple, and production efficiency is high, and the laminated glass obtained has good high transmittance, the phenomenon such as be difficult for to produce bubble, come unstuck, and shock resistance, weathering resistance do not reduce.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements, all belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.

Claims (6)

1. the preparation method of a high-strength laminated glass, is characterized in that, comprises the steps:
1) close sheet: the EVA film is laid between two-layer or multilayer toughened glass and is closed sheet;
2) composite molding: will close the first low-temperature prewarming of glass after sheet, then heat;
3) cooling: as by the glass cools after heat, to take out, obtain laminated glass.
2. preparation method according to claim 1, is characterized in that, in step 1), the thickness of described toughened glass is 5-12mm; The thickness of described film is 0.38-0.76mm.
3. preparation method according to claim 1, is characterized in that, in step 1), the described sheet condition of closing is: vacuum tightness 0.08-0.095MPa, 25 ℃ of temperature, humidity<30%.
4. preparation method according to claim 1, is characterized in that, in step 2) in, described low-temperature prewarming step is at 40-60 ℃ of lower preheating 10-40min.
5. preparation method according to claim 1, is characterized in that, in step 2) in, described heat step for to heat 80-120min under 100-110 ℃.
6. preparation method according to claim 1, is characterized in that, in step 3), described cooling temperature is 40-60 ℃.
CN201310415217.4A 2013-09-12 2013-09-12 High-strength laminated glass manufacturing method Pending CN103482888A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103963372A (en) * 2014-04-30 2014-08-06 中山市格兰特实业有限公司 LED pattern glass and manufacturing method
CN108372698A (en) * 2018-03-05 2018-08-07 天津泰立得塑胶制品有限公司 A kind of laminated glass molding machine
CN112192927A (en) * 2020-10-15 2021-01-08 洪雅竹元科技有限公司 Bamboo-sandwiched paper glass processing technology
CN112874071A (en) * 2021-01-26 2021-06-01 咸宁南玻节能玻璃有限公司 Preparation method of super-large four-glass three-interlayer glass

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1318468A (en) * 2000-04-19 2001-10-24 中国洛阳浮法玻璃集团加工玻璃有限公司 Two-sided perspective decorating sandwiched glass and its making process
CN102555397A (en) * 2011-08-29 2012-07-11 彭州市卓越工艺玻璃有限公司 Method for manufacturing screen glass

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1318468A (en) * 2000-04-19 2001-10-24 中国洛阳浮法玻璃集团加工玻璃有限公司 Two-sided perspective decorating sandwiched glass and its making process
CN102555397A (en) * 2011-08-29 2012-07-11 彭州市卓越工艺玻璃有限公司 Method for manufacturing screen glass

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103963372A (en) * 2014-04-30 2014-08-06 中山市格兰特实业有限公司 LED pattern glass and manufacturing method
CN108372698A (en) * 2018-03-05 2018-08-07 天津泰立得塑胶制品有限公司 A kind of laminated glass molding machine
CN112192927A (en) * 2020-10-15 2021-01-08 洪雅竹元科技有限公司 Bamboo-sandwiched paper glass processing technology
CN112874071A (en) * 2021-01-26 2021-06-01 咸宁南玻节能玻璃有限公司 Preparation method of super-large four-glass three-interlayer glass

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Application publication date: 20140101