CN1034389A - Process of producing low white spirit by direct freezing method - Google Patents

Process of producing low white spirit by direct freezing method Download PDF

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Publication number
CN1034389A
CN1034389A CN 87107456 CN87107456A CN1034389A CN 1034389 A CN1034389 A CN 1034389A CN 87107456 CN87107456 CN 87107456 CN 87107456 A CN87107456 A CN 87107456A CN 1034389 A CN1034389 A CN 1034389A
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China
Prior art keywords
low
white spirit
low alcohol
freezing
cold
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Withdrawn
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CN 87107456
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Chinese (zh)
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CN1009206B (en
Inventor
孟昭叔
张朝鹏
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Individual
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Individual
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Priority to CN 87107456 priority Critical patent/CN1009206B/en
Publication of CN1034389A publication Critical patent/CN1034389A/en
Publication of CN1009206B publication Critical patent/CN1009206B/en
Expired legal-status Critical Current

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  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

Process of producing low white spirit by direct freezing method relates to the clarification technique of low alcohol.Known natural cold method is subjected to the restriction in geographical position and season; Refrigerator chamber storehouse cold method cost height, and do not meet the freezer management regulation; Indirect freezing method waste cold, operation inconvenience is difficult for forming industrial mass manufacture.The present invention utilizes the directly freezing low alcohol of blending of vaporizer of single-stage refrigeration plant.Low alcohol transparency height, raciness, the anti-storage of Sheng Chaning like this, big in batches, level of automation is higher, and is simple to operate, and production cost is low.

Description

Process of producing low white spirit by direct freezing method
Process of producing low white spirit by direct freezing method relates to the clarification technique of low alcohol white spirit.
The ethanol content of liquor is more than 50 ° the time, and is more as clear as crystal, and in the time of below 50 °, along with ethanol content reduces, transparency also decreases, even slight muddiness can occur.This will occur when liquor degree of falling adds slurry, is because higher alcohols, senior fat resin acid and the ester class thereof in the liquor wherein mainly is ethyl palmitate, and ethyl oleate, the ethyl linoleate solubleness in wine reduces and separates out.This phenomenon is more obvious when the production low alcohol.The solubleness of above-mentioned higher fatty acid ethyl esters in liquor also has much relations with temperature except that outside the Pass having with ethanol content.When temperature reduced, their solubleness also decreased.This is a reason of separating out the white opacity thing in the cold district wine in winter.So do not have again in the warehouse of heating at cold district, the liquor more than 50 ° also phenomenons such as loss of gloss, muddiness can occur.
The method that influences transparency behind the solution liquor degree of falling is a lot, the redistillation method is arranged, cold method and absorption method etc.What relatively be suitable at present has a starch absorption method; Resin adsorption method; Cellulose adsorption method etc.Adopt these methods, the little difficult formation industrial mass manufacture of the output that has; After the processing that has residue is arranged, product is difficult for keeping, is reluctant to sell through pipe department; The total fat loss of the total acid that has is more, influences the local flavor of wine, and fragrance is poor, and taste is light; The cost height that has; The bad grasp of the complex process that has.Though the temperature that adopts cold method to fill a wine cup for reduces, and filters the purpose that can reach raising bent cellar for storing things vinosity amount and production low alcohol at low temperatures, all there are various shortcomings in known cold method.Only limit to cold season of cold district as natural cold method, lack ubiquity; Refrigerator chamber storehouse cold method cost height, production cost is also high, does not also meet freezer store management regulation; Indirect freezing method (freezing as icy salt solution) waste cold, operation inconvenience is difficult for forming industrial mass manufacture.
The present invention adopts the direct freezing method filtration process to produce low alcohol white spirit, just can overcome above-mentioned shortcoming, realizes large batch of successive industrial production.
Process of producing low white spirit by direct freezing method is after base liquor is added slurry dilution, to be refrigerated to certain temperature, treat higher fatty acid ethyl esters solubleness reduce separate out after, filter at low temperatures and can obtain as clear as crystal low alcohol white spirit.Technical characterictic of the present invention is: the vaporizer of single-stage refrigeration plant is placed in the wine cooling tank, make the low alcohol of blending in the jar directly freezing outside evaporator tube, after temperature is reduced to-12 ℃~-15 ℃, wine liquid sent into leave standstill a few hours after-filtration, packing in the settling tank that can keep this cold condition.The wine cooling tank forms the continuous production device by wine pump and pipeline between settling tank, the strainer.
In this technological process because low alcohol leaves standstill under cold condition, help esterification and carry out, thereby products obtained therefrom fat is aromatic and, can play the ageing effect, and can keep song to store the original local flavor of wine.
Adopt the low alcohol of this explained hereafter, have the transparency height, raciness, anti-storage, in batches big, advantage such as level of automation is higher, and is simple to operate, and production cost is low.If the direct freezing method filtration process is used for song cellar for storing things wine production more than 50 °, can not only improve the quality of wine, guarantee at the various temperature conditions body of going with wine as clear as crystally, can also suitably reduce ethanol content, increase output.
Embodiment:
After base liquor more than 50 blent, add slurry and be diluted to 35 °~38 ° and blend, be pumped into the wine cooling tank of stainless steel then with wine, the ammonia evaporator with stainless steel is housed in jar, the wine in the cooling tank is directly freezing outside the ammonia evaporator pipe.The temperature for the treatment of wine is reduced to after-12 ℃~-15 ℃, with the wine pump freezing wine is sent into 1 of good heat insulation #In the settling tank, left standstill 24 hours, to strainer, wine after filtering can be packed by pipe-line transportation.
When 1 #When the wine in the settling tank left standstill, the wine that freezes can send into 2 #Settling tank, by that analogy.Produce 1000 tons of low alcohol per year and 2 cooling tanks can be set, 4~6 settling tanks.

Claims (1)

1, process of producing low white spirit by direct freezing method relates to the clarifying low alcohol white spirit technology, be after base liquor is added the slurry dilution, be refrigerated to certain temperature, after treating that the reduction of higher fatty acid ethyl esters solubleness is separated out, filter at low temperatures and can obtain as clear as crystal low alcohol white spirit, technical characterictic of the present invention is: the vaporizer of single-stage refrigeration plant is placed in the wine cooling tank, make the evaporator tube of the low alcohol of blending in the jar directly freezing outward, reduce to-12 ℃~-15 ℃ when temperature and send in the settling tank that can keep this cold condition and leave standstill after-filtration.
CN 87107456 1987-12-10 1987-12-10 Process of producing low white spirit by direct freezing method Expired CN1009206B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 87107456 CN1009206B (en) 1987-12-10 1987-12-10 Process of producing low white spirit by direct freezing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 87107456 CN1009206B (en) 1987-12-10 1987-12-10 Process of producing low white spirit by direct freezing method

Publications (2)

Publication Number Publication Date
CN1034389A true CN1034389A (en) 1989-08-02
CN1009206B CN1009206B (en) 1990-08-15

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 87107456 Expired CN1009206B (en) 1987-12-10 1987-12-10 Process of producing low white spirit by direct freezing method

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CN (1) CN1009206B (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1079113C (en) * 1998-12-14 2002-02-13 湘潭市德丰设备制造有限公司 Energy-saved freezing and filtering apparatus and process for wine
CN101085972B (en) * 2006-06-05 2010-05-12 宋德君 Clarification method for mild distilled spirit production
CN102676358A (en) * 2012-05-07 2012-09-19 泸州品创科技有限公司 Enrichment and separation method for flocculent suspended matters in fragrant white spirit
CN102676359A (en) * 2012-05-07 2012-09-19 泸州品创科技有限公司 Enriching and separating method for thick white liquor flocculent suspended substances
CN102676357A (en) * 2012-05-07 2012-09-19 泸州品创科技有限公司 Enrichment separation method for flocculent suspended matter of Maotai style white spirit
CN105368645A (en) * 2015-12-22 2016-03-02 湖北工业大学 Alcohol-free white liquor making method
CN106497754A (en) * 2016-12-29 2017-03-15 福建惠泽龙酒业股份有限公司 Prepare the device of low wine and the method for low wine being prepared using the device
CN108504529A (en) * 2018-06-10 2018-09-07 灵台县百里酒厂 A kind of method for effectively shortening the white spirit ageing time
CN111548894A (en) * 2020-06-10 2020-08-18 扬州润明智能装备股份有限公司 White spirit direct-cooling filtering device and method

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1079113C (en) * 1998-12-14 2002-02-13 湘潭市德丰设备制造有限公司 Energy-saved freezing and filtering apparatus and process for wine
CN101085972B (en) * 2006-06-05 2010-05-12 宋德君 Clarification method for mild distilled spirit production
CN102676358A (en) * 2012-05-07 2012-09-19 泸州品创科技有限公司 Enrichment and separation method for flocculent suspended matters in fragrant white spirit
CN102676359A (en) * 2012-05-07 2012-09-19 泸州品创科技有限公司 Enriching and separating method for thick white liquor flocculent suspended substances
CN102676357A (en) * 2012-05-07 2012-09-19 泸州品创科技有限公司 Enrichment separation method for flocculent suspended matter of Maotai style white spirit
CN105368645A (en) * 2015-12-22 2016-03-02 湖北工业大学 Alcohol-free white liquor making method
CN105368645B (en) * 2015-12-22 2017-10-24 湖北工业大学 A kind of method without alcohol brewed spirit
CN106497754A (en) * 2016-12-29 2017-03-15 福建惠泽龙酒业股份有限公司 Prepare the device of low wine and the method for low wine being prepared using the device
CN106497754B (en) * 2016-12-29 2019-06-28 福建惠泽龙酒业股份有限公司 Prepare the device of low wine and the method using device preparation low wine
CN108504529A (en) * 2018-06-10 2018-09-07 灵台县百里酒厂 A kind of method for effectively shortening the white spirit ageing time
CN111548894A (en) * 2020-06-10 2020-08-18 扬州润明智能装备股份有限公司 White spirit direct-cooling filtering device and method

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Publication number Publication date
CN1009206B (en) 1990-08-15

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