CN103421389B - Water-based environment-friendly opaque medium-yellow color paste and preparation method thereof - Google Patents
Water-based environment-friendly opaque medium-yellow color paste and preparation method thereof Download PDFInfo
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- CN103421389B CN103421389B CN201310339077.7A CN201310339077A CN103421389B CN 103421389 B CN103421389 B CN 103421389B CN 201310339077 A CN201310339077 A CN 201310339077A CN 103421389 B CN103421389 B CN 103421389B
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Abstract
The invention discloses a water-based environment-friendly opaque medium-yellow color paste and a preparation method thereof. The color paste comprises the following components in percentage by weight: 45-50 percent of 313 superfine iron oxide yellow, 2-5 percent of 930 superfine rutile titanium dioxide, 35-40 percent of water, 5-10 percent of an HD-18 dispersing agent, 3-5 percent of HCH-195 propylene glycol, and 0.3-0.7 percent of environment-friendly triethanolamine, 0.1-0.4 percent of AF200 anti-corrosion disinfectant, and 0.1-0.4 percent of SPA-202 defoaming agent. The preparation method comprises the following steps: sequentially adding the components into a stirrer, and stirring by a stirrer. The preparation method is simple; the prepared color paste has the advantages of bright color, good environment-friendly performance, high dispersity, compatibility, tinting strength, light resistance, weather resistance, ultraviolet ray resistance and tensile resistance, lasting viscous force, no layering and no sediment after long-time storing, and high stability.
Description
Technical field
The present invention relates to a kind of tinting material, particularly opaque yellow adhesive tape mill base of a kind of aqueous, environmental protective for joint sealing and preparation method thereof.
Background technology
Mill base is to be dispersed in by pigment or pigment and stopping composition the work piece that form in paint vehicle, comprises oil pastes, resin mill base and aqueous color paste etc.Aqueous color paste is due to its good environmental-protecting performance and wide application field, and application prospect is good.In recent years, the opaque middle yellow adhesive tape color paste consumption in joint sealing market is increasing, but traditional opaque middle yellow adhesive tape mill base is due to reasons such as filler particles are large, component proportion is not good, there is photostabilization, weathering resistance, resistance to acids and bases, poor stability, tinting strength is not strong, the defects such as consistency is poor, toning property is poor, its application is restricted.
Summary of the invention
Object of the present invention is intended to solve the poor problem of stability, tinting strength, consistency, toning that traditional mill base exists, and alternative new mill base of a kind of aqueous, environmental protective and preparation method thereof is provided.
In order to achieve the above object, the technical scheme that the present invention takes is:
The opaque middle yellow adhesive tape mill base of a kind of aqueous, environmental protective, the quality percentage composition of each component is respectively: the yellow 45-50% of 313 superfine iron oxides, 930 ultra-fine rutile titanium white 2-5%, water 35-40%, HD-18 dispersion agent 5-10%, HCH-195 propylene glycol 3-5%, environmental protection trolamine 0.3-0.7%, AF200 anticorrosion and bactericidal agent 0.1-0.4%, SPA-202 defoamer 0.1-0.4%.Best results when wherein 313 superfine iron oxides Huangs and 930 ultra-fine rutile titanium whites are 1000 order.
The preparation method of the opaque middle yellow adhesive tape mill base of above-mentioned aqueous, environmental protective, comprises the following steps:
A, respectively water, the yellow 930 ultra-fine rutile titanium whites of 313 superfine iron oxides are added in agitator, start stirrer, rotating speed 2500r/min, power 200w, stirs 10-30 minute;
B, respectively HD-18 dispersion agent, HCH-195 propylene glycol, environmental protection trolamine are added in above-mentioned agitator and stir 20-40 minute;
C, respectively AF200 anticorrosion and bactericidal agent, SPA-202 defoamer are added in aforementioned agitator and stir 20-40 minute;
D, the material that step C is made JM-125Q colloidal mill, power of motor 7.5kw, rotating speed 2900r/min, grinds 3-5 time, and barrelling is filtered in discharging.
In aforesaid method, when steps A stirs 20 minutes, step B and C all stir 30 minutes; When step D grinds 5 times, the mill base best results making.
The opaque middle yellow adhesive tape mill base of aqueous, environmental protective of the present invention is compared with traditional mill base, and its performance comparison is as following table:
The opaque middle yellow adhesive tape mill base of aqueous, environmental protective is compared with traditional mill base performance
Therefore advantage of the present invention and beneficial effect are mainly:
1, mill base is bright in colour, and lead, cadmium, chromium, mercury heavy metal content decline greatly, good environmental protection, and good dispersity, consistency is good, and tinting strength is high; Photostabilization, weather resisteant, acid and alkali-resistance, UV resistant performance are good; There is high resistance pulling force and lasting viscous force; Long-time store not stratified, do not precipitate, there is satisfactory stability.2, preparation technology is simple, is easy to apply.
Embodiment
In order to deepen the understanding of the present invention, below in conjunction with specific examples, technical scheme of the present invention is described in further detail.Following examples only, for explaining the present invention, do not form limiting the scope of the present invention.
Embodiment 1
One, fill a prescription by mass percentage:
The ultra-fine rutile titanium white 2% of 313 superfine iron oxide Huang 45%, 930, water 39%, HD-18 dispersion agent 10%, HCH-195 propylene glycol 3%, environmental protection trolamine 0.3%.AF200 anticorrosion and bactericidal agent 0.3%, SPA-202 defoamer 0.4%.
Two, preparation process:
A, water, 313 superfine iron oxides is yellow, 930 ultra-fine rutile titanium whites add in agitator respectively, start stirrer, rotating speed 2500r/min, and power 200w, stirs 15-25 minute;
B, respectively HD-18 dispersion agent, HCH-195 propylene glycol, environmental protection trolamine are added in above-mentioned agitator and stir 25-35 minute;
C, respectively AF200 anticorrosion and bactericidal agent, SPA-202 defoamer are added in aforementioned agitator and stir 25-35 minute;
D, by the material of first three step system JM-125Q colloidal mill, power of motor 7.5kw, rotating speed 2900r/min, grinds 5 times, barrelling is filtered in discharging.
Embodiment 2
One, fill a prescription by mass percentage:
The ultra-fine rutile titanium white 3% of 313 superfine iron oxide Huang 47%, 930, water 40%, HD-18 dispersion agent 5%, HCH-195 propylene glycol 4%, environmental protection trolamine 0.7%.AF200 anticorrosion and bactericidal agent 0.2%, SPA-202 defoamer 0.1%.
Claims (6)
1. the opaque middle yellow adhesive tape mill base of aqueous, environmental protective, it is characterized in that, the quality percentage composition of each component is respectively: 313 superfine iron oxide Huangs are 45-50%, 930 ultra-fine rutile titanium whites are 2-5%, and water is 35-40%, and HD-18 dispersion agent is 5-10%, HCH-195 propylene glycol is 3-5%, environmental protection trolamine is 0.3-0.7%, and AF200 anticorrosion and bactericidal agent is 0.1-0.4%, and SPA-202 defoamer is 0.1-0.4%; Wherein said 313 superfine iron oxides Huangs and 930 ultra-fine rutile titanium whites are 1000 orders.
2. the opaque middle yellow adhesive tape mill base of aqueous, environmental protective as claimed in claim 1, it is characterized in that, the quality percentage composition of each component is respectively: 313 superfine iron oxide Huangs 45%, 930 ultra-fine rutile titanium whites 2%, water 39%, HD-18 dispersion agent 10%, HCH-195 propylene glycol 3%, environmental protection trolamine 0.3%, AF200 anticorrosion and bactericidal agent 0.3%, SPA-202 defoamer 0.4%.
3. the opaque middle yellow adhesive tape mill base of aqueous, environmental protective as claimed in claim 1, it is characterized in that, the quality percentage composition of each component is respectively: 313 superfine iron oxide Huangs 47%, 930 ultra-fine rutile titanium whites 3%, water 40%, HD-18 dispersion agent 5%, HCH-195 propylene glycol 4%, environmental protection trolamine 0.7%, AF200 anticorrosion and bactericidal agent 0.2%, SPA-202 defoamer 0.1%.
4. the opaque middle yellow adhesive tape mill base of aqueous, environmental protective as claimed in claim 1, it is characterized in that, the quality percentage composition of each component is respectively: 313 superfine iron oxide Huangs 49%, 930 ultra-fine rutile titanium whites 4%, water 37%, HD-18 dispersion agent 6%, HCH-195 propylene glycol 3%, environmental protection trolamine 0.4%, AF200 anticorrosion and bactericidal agent 0.4%, SPA-202 defoamer 0.2%.
5. a preparation method for the opaque middle yellow adhesive tape mill base of aqueous, environmental protective as claimed in claim 1, is characterized in that, comprises the following steps:
A, water, 313 superfine iron oxides is yellow, 930 ultra-fine rutile titanium whites add in agitator respectively, start stirrer, rotating speed 2500r/min, and power 200W, stirs 10-30 minute;
B, respectively HD-18 dispersion agent, HCH-195 propylene glycol, environmental protection trolamine are added in above-mentioned agitator and stir 20-40 minute;
C, respectively AF200 anticorrosion and bactericidal agent, SPA-202 defoamer are added in aforementioned agitator and stir 20-40 minute;
D, the material that step C is made JM-125Q colloidal mill, power of motor 7.5kW, rotating speed 2900r/min, grinds 3-5 time, and barrelling is filtered in discharging.
6. the preparation method of the opaque middle yellow adhesive tape mill base of aqueous, environmental protective as claimed in claim 5, is characterized in that, stirs 20 minutes in described steps A, all stirs 30 minutes in step B and C; Step D grinds 5 times.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310339077.7A CN103421389B (en) | 2013-08-06 | 2013-08-06 | Water-based environment-friendly opaque medium-yellow color paste and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310339077.7A CN103421389B (en) | 2013-08-06 | 2013-08-06 | Water-based environment-friendly opaque medium-yellow color paste and preparation method thereof |
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| CN103421389A CN103421389A (en) | 2013-12-04 |
| CN103421389B true CN103421389B (en) | 2014-12-10 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103937331A (en) * | 2014-03-25 | 2014-07-23 | 浙江纳美材料科技有限公司 | High-moisture-retention VOC-free iron oxide color paste and preparation method thereof |
| CN108841251A (en) * | 2018-07-04 | 2018-11-20 | 浙江大利实业有限公司 | Opaque adhesive tape mill base of a kind of aqueous, environmental protective for joint sealing and preparation method thereof |
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| US7402627B2 (en) * | 2003-08-18 | 2008-07-22 | Columbia Insurance Company | Precursor colorant composition for latex paint |
| CN101469155A (en) * | 2007-12-24 | 2009-07-01 | 深圳市海川实业股份有限公司 | Environment friendly transparent iron oxide yellow superfine aqueous color sizing dispersion and preparation thereof |
| CN101760088B (en) * | 2009-04-13 | 2012-04-18 | 昆山市世名科技开发有限公司 | Color paste for nanometer modified environmentally-friendly ferric oxide machine and preparation method thereof |
| CN102146234B (en) * | 2011-01-20 | 2013-07-03 | 佩特化工(上海)有限公司 | Water-based paint dispersing technology |
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| TR01 | Transfer of patent right |
Effective date of registration: 20190328 Address after: 226156 999 Harbour Road, Binhai New Area, Haimen, Nantong, Jiangsu Patentee after: HAIMEN HUANGHAI PIONEER PARK SERVICES CO., LTD. Address before: No. 2, Mengxi Road, Zhenjiang, Jiangsu Province, Jiangsu Patentee before: Jiangsu University of Science and Technology |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190716 Address after: 528300 Youtan Industrial Zone, Xingtan Town, Shunde District, Foshan City, Guangdong Province, No. 6 Patentee after: Foshan Shunde Kaili Adhesive Products Co., Ltd. Address before: 226156 Nantong Binhai New Area, Haimen City, Hong Kong West Road, No. 999, No. Patentee before: HAIMEN HUANGHAI PIONEER PARK SERVICES CO., LTD. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141210 Termination date: 20190806 |