CN103406226A - Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant - Google Patents

Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant Download PDF

Info

Publication number
CN103406226A
CN103406226A CN2013103415577A CN201310341557A CN103406226A CN 103406226 A CN103406226 A CN 103406226A CN 2013103415577 A CN2013103415577 A CN 2013103415577A CN 201310341557 A CN201310341557 A CN 201310341557A CN 103406226 A CN103406226 A CN 103406226A
Authority
CN
China
Prior art keywords
spray
steam generator
connecting rod
nuclear power
nozzle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN2013103415577A
Other languages
Chinese (zh)
Other versions
CN103406226B (en
Inventor
余桐
李江
武伟让
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China General Nuclear Power Corp
Suzhou Nuclear Power Research Institute Co Ltd
CGNPC Inspection Technology Co Ltd
Original Assignee
China General Nuclear Power Corp
Suzhou Nuclear Power Research Institute Co Ltd
CGNPC Inspection Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China General Nuclear Power Corp, Suzhou Nuclear Power Research Institute Co Ltd, CGNPC Inspection Technology Co Ltd filed Critical China General Nuclear Power Corp
Priority to CN201310341557.7A priority Critical patent/CN103406226B/en
Publication of CN103406226A publication Critical patent/CN103406226A/en
Application granted granted Critical
Publication of CN103406226B publication Critical patent/CN103406226B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Cleaning By Liquid Or Steam (AREA)
  • Nozzles (AREA)

Abstract

本发明涉及一种用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,它包括:同轴设置有可转动传动轴的喷枪连接杆,三个喷头,所述三个喷头交替可拆卸地安装在所述的喷枪连接杆端部,喷头前端能够在传动轴的带动下在其A-A截面内作周向旋转,并且喷头的喷头前端轴心线与旋转轴的轴心线夹角分别呈60°、0°、-60。本发明蒸汽发生器泥渣清洗喷头装置配个三个不同角度的喷头,可以从不同角度喷水对蒸汽发生器进行清洁,提高了蒸汽发生器的清洁效果;另外喷头前端可以在传动轴的带动下作180°旋转,从而对整个蒸汽发生器传热管进行清洁,提高了工作效率。

Figure 201310341557

The present invention relates to a device for cleaning nozzles of steam generators in EPR nuclear power plants, which comprises: a connecting rod of a spray gun coaxially provided with a rotatable transmission shaft, and three nozzles, the three nozzles are alternately detachable Installed at the end of the connecting rod of the spray gun, the front end of the spray head can be driven by the transmission shaft to rotate circumferentially in its AA section, and the angle between the axis line of the front end of the spray head and the axis line of the rotating shaft is 60° °, 0°, -60. The steam generator sludge cleaning nozzle device of the present invention is equipped with three nozzles with different angles, which can spray water from different angles to clean the steam generator, which improves the cleaning effect of the steam generator; in addition, the front end of the nozzle can be driven by the transmission shaft Rotate 180° downwards to clean the entire heat transfer tube of the steam generator and improve work efficiency.

Figure 201310341557

Description

A kind of for EPR heap type Steam Generators in NPP body refuse cleaning ejecting device
Technical field
The present invention relates to a kind of cleaning device, be specifically related to a kind of for EPR heap type Steam Generators in NPP body refuse cleaning ejecting device.
Background technology
Steam generator is one of visual plant of nuclear power plant, plays one, heat exchange and the buffer action of secondary circuit.Steam generator secondary side under long-term Power operation easily produces subsidence settling at cold and hot boundary end, shows that through great many of experiments the body refuse of deposition can reduce the heat transfer efficiency of steam generator internal heat transfer pipe and increase the damaged probability of heat-transfer pipe.Therefore in order to remove this type of dislodged sludge, during nuclear power plant's overhaul, all can carry out the body refuse cleaning for steam generator secondary side.
At present both at home and abroad all exploitation has the body refuse cleaning equipment that is applied to different IPs power plant heap type, as the body refuse cleaning equipment of France's development in Daya Bay nuclear power plant's successful Application more than ten years.All there are corresponding special equipment in the U.S., Japan, Korea S for the exploitation of own national nuclear power plant simultaneously.These equipment major parts possess identical principle: by the spray gun propulsive mechanism changed manually or automatically by high-pressure water shot to target area that needs are removed contamination, the body refuse water that utilizes simultaneously retracting device will remain in steam generator tube sheet secondary side recycles and re-uses, and realizes on the basis of water circulation the cleaning to steam generator secondary side.
What domestic application was the widest now is the rigid sludge cleaning means, and its shower nozzle is only applicable to the steam generator that heat-transfer pipe is rectanglar arrangement, and the direction of water jet and the direction of shower nozzle can not change.And the heat-transfer pipe 6 that develops into the steam generator of the third generation of today Europe advanced pressurized water reactor (EPR) heap type is to adopt equilateral triangle to arrange, as shown in Figure 1, this setup is conducive to the sufficient heat exchange of heat-transfer pipe, has saved floor space, has but increased the difficulty that its body refuse cleans.In order to solve this difficult problem, design a kind of ejecting device that is applicable to the steam generator heat-transfer pipe that equilateral triangle arranges and just seem that tool has very important significance.
Summary of the invention
The present invention seeks to provide in order to overcome the deficiencies in the prior art a kind of ejecting device that steam generator heat-transfer pipe that equilateral triangle arranges and water jet direction can change that is applicable to.
For achieving the above object, the technical solution used in the present invention is: a kind of for EPR heap type Steam Generators in NPP body refuse cleaning ejecting device, it comprises:
The spray gun connecting rod, be coaxially arranged with rotating power transmission shaft in described spray gun connecting rod;
Three shower nozzles, described three shower nozzles alternately are removably mounted on described spray gun connecting rod end, it comprises nozzle housing, be located at the rotating shaft that nozzle housing central authorities are coaxial with described power transmission shaft and bond connected connects, the shower nozzle front end that seals mutually and be connected with described rotating shaft with described nozzle housing, described shower nozzle front end comprises the punching chamber of offering at the Yan Qi center, perpendicular with described punching chamber and be communicated with the spray orifice of offering, between described spray gun connecting rod and power transmission shaft, between nozzle housing and rotating shaft, be formed with the water stream channel be connected with described punching chamber, in described three shower nozzles, the shower nozzle front end axial line of one of them shower nozzle and the axial line angle of described rotating shaft are 0 °, the angle of the shower nozzle front end axial line of two other shower nozzle and the axial line of described rotating shaft is respectively ± and 60 °.
Optimally, described power transmission shaft is connected with rotating shaft by spline, and described rotating shaft is connected with the shower nozzle front end by gear pair.
Further, described gear pair adopts bevel gear.
Optimally, described spray gun connecting rod is fixed with shower nozzle phase bolt.
Optimally, between described spray gun connecting rod and shower nozzle, use seal with elastometic washer.
Optimally, between described nozzle housing and shower nozzle front end, use packing seal.
Because technique scheme is used, the present invention compared with prior art has following advantages: the ejecting device that steam generator body refuse of the present invention cleans is joined the shower nozzle of three different angles, can spray water steam generator is cleaned from different perspectives, improve the cleaning effect of steam generator; The shower nozzle front end can be done 180 ° of rotations under the drive of power transmission shaft in addition, thereby whole steam generator heat-transfer pipe is cleaned, and has improved operating efficiency.
The accompanying drawing explanation
Accompanying drawing 1 arranges for the steam generator heat-transfer pipe of existing EPR heap type the structural representation that is equilateral triangle;
Accompanying drawing 2 is used view for steam generator body refuse of the present invention cleans ejecting device;
Accompanying drawing 3 is that accompanying drawing 2 steam generator body refuses clean shower nozzle front cross-sectional view in ejecting device;
Accompanying drawing 4 is used view for steam generator body refuse of the present invention cleans ejecting device;
Accompanying drawing 5 is used view for steam generator body refuse of the present invention cleans ejecting device;
Wherein: 1, spray gun connecting rod; 2, shower nozzle; 21, nozzle housing; 22, rotating shaft; 23, shower nozzle front end; 231, punching chamber; 232, spray orifice; 2 ', shower nozzle; 21 ', nozzle housing; 22 ', rotating shaft; 23 ', shower nozzle front end; 231 ', punching chamber; 232 ', spray orifice; 2 ' ', shower nozzle; 21 ' ', nozzle housing; 22 ' ', rotating shaft; 23 ' ', shower nozzle front end; 231 ' ', punching chamber; 232 ' ', spray orifice; 3, water stream channel; 4, spline; 5, bevel gear; 6, steam generator heat-transfer pipe; 7, steam generator heat-transfer pipe corridor dividing plate.
The specific embodiment
Below in conjunction with accompanying drawing, the preferred embodiment of the invention is elaborated:
The heat-transfer pipe 6 of Europe third generation EPR heap type Steam Generators in NPP is equilateral triangle arranges, and as shown in Figure 1, both has been conducive to the sufficient heat exchange of heat-transfer pipe, has increased again the stacking degree of heat-transfer pipe, has saved floor space.Yet such set-up mode has increased the difficulty that its body refuse cleans, need to heat-transfer pipe 6, spray water respectively from tri-directions of a, b, c that mark Fig. 1, body refuse can be cleaned up.Heat-transfer pipe 6 belows are provided with heat transfer piping lane dividing plate 7 simultaneously, and the body refuse cleaning device can only be installed in the gap between heat-transfer pipe 6 and heat transfer piping lane dividing plate 7 in use, the limited space that can use.
Body refuse of the present invention cleans ejecting device and is applicable to heat-transfer pipe to be that equilateral triangle is arranged and institute takes up space less, it mainly comprises spray gun connecting rod 1 and three shower nozzles, wherein in spray gun connecting rod 1, be provided with 11, three shower nozzles of power transmission shaft and alternately be removably mounted on spray gun connecting rod 1 end.
As shown in Figure 2 and Figure 3, shower nozzle 2 mainly comprises nozzle housing 21, rotating shaft 22, shower nozzle front end 23.Rotating shaft 22 coaxially is arranged at nozzle housing 21 central authorities, and its end and power transmission shaft 11 bond connecteds connect, and can drive its synchronous rotary when under the driving of power transmission shaft 11 at servomotor, rotating; Its other end is connected with shower nozzle front end 23, in its A-A cross section, makes circumferential movement thereby drive shower nozzle front end 23.Shower nozzle front end 23 comprises punching chamber 231 and spray orifice 232, spray orifice 232 connections are offered and are perpendicular with punching chamber 231, space between space, nozzle housing 21 and rotating shaft 22 between they and spray gun connecting rod 1 and power transmission shaft 11 is interconnected and forms water stream channel 3, for delivery of water under high pressure.Shower nozzle front end 23 axial lines and rotating shaft 22 axial line angles are 60 °, so the c direction in the water outlet direction corresponding diagram 1 of shower nozzle 2.
In the present embodiment, rotating shaft 22 1 ends are connected with power transmission shaft 11 use splines 4, thereby make rotating shaft 22 under the drive of power transmission shaft 11, do and rotate in a circumferential direction in its cross section; Rotating shaft 22 other ends are connected with shower nozzle front end 23 with bevel gear 5, thereby are the circumferential movement of shower nozzle front end 23 in its A-A cross section by the conversion of motion of rotating shaft 22.By the anglec of rotation of controlling power transmission shaft 11, the anglec of rotation of shower nozzle front end 23 in its A-A cross section be can control, the incident angle of water jet between the heat-transfer pipe tube gap and the purpose of distance controlled thereby reach.In order to keep the pressure of water under high pressure, the gland sealed form is adopted in the sealing between shower nozzle front end 23 and nozzle housing 21, and the sealing means between spray gun connecting rod 1 and shower nozzle 2 adopts O type rubber ring.
As shown in Figure 4, Figure 5, shower nozzle 2 ', shower nozzle 2 ' ' overall structure and shower nozzle 2 roughly the same, different is that the axial line angle of their shower nozzle front end axial line and rotating shaft is respectively 0 ° ,-60 °, thereby water outlet direction difference, corresponding b, a both direction respectively.In the present embodiment, spray gun connecting rod 1 and three shower nozzles are alternately fixed by four bolts, after using 2 pairs of c directions of shower nozzle to clean, fast bolt is outwarded winding, change respectively shower nozzle 2 ', shower nozzle 2 ' ', again b, a both direction are cleaned, can complete the cleaning to heat-transfer pipe, greatly improved the clean-up performance of heat-transfer pipe 6 and workman's operating efficiency.
Above-mentionedly the present invention cleaned to the ejecting device structure for EPR heap type Steam Generators in NPP body refuse be illustrated, below its operation principle is done to brief description:
In use, select shower nozzle 2 to be installed on spray gun connecting rod 1 end, together with step device, be fixed on the flange at steam generator hand hole place subsequently; The power transmission shaft of spray gun connecting rod 1 11 is connected with the servomotor in the flange outside, switch on power, utilize servomotor to drive power transmission shaft 11 and do circumferential movement, and then drive driving rotating shaft 22 rotates together, the conversion of motion of rotating shaft 22 is the circumferential movement of shower nozzle front end 23 in its A-A cross section the most at last, so just the anglec of rotation of power transmission shaft 11 be can pass through to control, thereby water jet incident angle and distance on heat-transfer pipe controlled; Water under high pressure sprays clean body refuse from spray orifice 232 to the c direction through water stream channel 3 simultaneously, starts step device and regulates the length that spray gun connecting rod 1 enters steam generator, can clean the body refuse on heat-transfer pipe 6 in the Different Plane parallel with the c direction; After the body refuse on the c direction cleans up, cleaning device is taken out and changes respectively shower nozzle 2 ' and shower nozzle 2 ' ', similarly the body refuse on b, a direction is cleaned up and gets final product.
From above-mentioned principle, being not difficult, find, when heat-transfer pipe is arranged according to rectangle or Else Rule shape, still can adopt with the similar body refuse cleaning of the present invention ejecting device heat-transfer pipe is cleaned, the angle that only need change simply the axial line angle of shower nozzle front end axial line and rotating shaft gets final product.
Above-described embodiment only is explanation technical conceive of the present invention and characteristics; its purpose is to allow the person skilled in the art can understand content of the present invention and implement according to this; can not limit the scope of the invention with this; all equivalences that Spirit Essence is done according to the present invention change or modify, within all should being encompassed in protection scope of the present invention.

Claims (6)

1.一种用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,其特征在于:它包括: 1. A device for cleaning nozzles for steam generator sludge in an EPR reactor type nuclear power plant, characterized in that: it comprises: 喷枪连接杆,所述的喷枪连接杆内同轴设置有可转动的传动轴; A spray gun connecting rod, a rotatable transmission shaft is arranged coaxially inside the spray gun connecting rod; 三个喷头,所述三个喷头交替可拆卸地安装在所述的喷枪连接杆端部,其包括喷头壳体、设在喷头壳体中央与所述的传动轴同轴且相键连接的旋转轴、与所述的喷头壳体相密封且与所述旋转轴相连接的喷头前端,所述的喷头前端包括沿其中心开设的冲孔腔、与所述的冲孔腔相垂直且连通开设的喷孔,所述的喷枪连接杆与传动轴之间、喷头壳体与旋转轴之间形成有与所述的冲孔腔相连通的水流通道,所述的三个喷头中,其中一个喷头的喷头前端轴心线与所述的旋转轴的轴心线夹角为0°,另外两个喷头的喷头前端轴心线与所述的旋转轴的轴心线的夹角分别为±60°。 Three spray heads, the three spray heads are alternately and detachably mounted on the end of the spray gun connecting rod, which includes a spray head housing, a rotating shaft that is coaxially connected with the transmission shaft and is keyed in the center of the spray head housing. shaft, the front end of the spray head that is sealed with the spray head housing and connected with the rotating shaft, the front end of the spray head includes a punching cavity opened along its center, and is perpendicular to and communicated with the punching cavity The spray hole is formed between the spray gun connecting rod and the transmission shaft, between the spray head housing and the rotating shaft, and a water flow channel communicating with the punching cavity is formed. Among the three spray heads, one of the spray heads The angle between the axis line of the front end of the nozzle and the axis line of the rotation axis is 0°, and the angles between the axis line of the front end of the nozzle of the other two nozzles and the axis line of the rotation axis are ±60° . 2. 根据权利要求1或2所述的用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,其特征在于:所述的传动轴通过花键与旋转轴连接,所述的旋转轴通过齿轮副与喷头前端连接。 2. The device for cleaning nozzles for steam generator sludge in EPR nuclear power plants according to claim 1 or 2, characterized in that: the transmission shaft is connected to the rotating shaft through a spline, and the rotating shaft passes through The gear pair is connected with the front end of the nozzle. 3.根据权利要求2所述的用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,其特征在于:所述的齿轮副采用锥齿轮。 3. The spray nozzle device for cleaning sludge of steam generators in EPR nuclear power plants according to claim 2, characterized in that: said gear pair adopts bevel gears. 4.根据权利要求1或2所述的用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,其特征在于:所述的喷枪连接杆与喷头相螺栓固定。 4. The spray head device for cleaning steam generator sludge in EPR reactor type nuclear power plant according to claim 1 or 2, characterized in that: the spray gun connecting rod and the spray head are fixed with bolts. 5.根据权利要求1或2所述的用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,其特征在于:所述的喷枪连接杆与喷头间使用橡胶圈密封。 5. The nozzle device for cleaning the steam generator sludge of EPR nuclear power plant according to claim 1 or 2, characterized in that: the connecting rod of the spray gun and the nozzle are sealed with a rubber ring. 6.根据权利要求1或2所述的用于EPR堆型核电厂蒸汽发生器泥渣清洗喷头装置,其特征在于:所述的喷头壳体与喷头前端间使用填料密封。 6. The sprinkler device for cleaning sludge of steam generators in EPR nuclear power plants according to claim 1 or 2, characterized in that: the nozzle shell and the front end of the nozzle are sealed with packing.
CN201310341557.7A 2013-08-07 2013-08-07 Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant Active CN103406226B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310341557.7A CN103406226B (en) 2013-08-07 2013-08-07 Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310341557.7A CN103406226B (en) 2013-08-07 2013-08-07 Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant

Publications (2)

Publication Number Publication Date
CN103406226A true CN103406226A (en) 2013-11-27
CN103406226B CN103406226B (en) 2015-06-17

Family

ID=49599294

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310341557.7A Active CN103406226B (en) 2013-08-07 2013-08-07 Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant

Country Status (1)

Country Link
CN (1) CN103406226B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106513389A (en) * 2016-05-12 2017-03-22 苏州热工研究院有限公司 Cleaning device for steam generator and cleaning method
CN108266717A (en) * 2016-12-30 2018-07-10 核动力运行研究所 A kind of rinse-system for horizontal steam generator header blowdown cave room

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008037434A1 (en) * 2006-09-26 2008-04-03 Ideal Standard International Bvba Pulsating water jet massage assembly for showers and handsprays
CN201415170Y (en) * 2009-06-24 2010-03-03 扬州恒源自来水喷泉设备有限公司 One-dimensional digital control multi-headed burner cap
CN201423325Y (en) * 2009-03-04 2010-03-17 许茜 High-pressure water dynamic-sealing rotary-cleaning spraying head
CN203417802U (en) * 2013-08-07 2014-02-05 中广核检测技术有限公司 Sludge cleaning nozzle device used for steam generator in EPR type nuclear power plant

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008037434A1 (en) * 2006-09-26 2008-04-03 Ideal Standard International Bvba Pulsating water jet massage assembly for showers and handsprays
CN201423325Y (en) * 2009-03-04 2010-03-17 许茜 High-pressure water dynamic-sealing rotary-cleaning spraying head
CN201415170Y (en) * 2009-06-24 2010-03-03 扬州恒源自来水喷泉设备有限公司 One-dimensional digital control multi-headed burner cap
CN203417802U (en) * 2013-08-07 2014-02-05 中广核检测技术有限公司 Sludge cleaning nozzle device used for steam generator in EPR type nuclear power plant

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106513389A (en) * 2016-05-12 2017-03-22 苏州热工研究院有限公司 Cleaning device for steam generator and cleaning method
CN106513389B (en) * 2016-05-12 2019-03-26 苏州热工研究院有限公司 A kind of cleaning device and cleaning method of steam generator
CN108266717A (en) * 2016-12-30 2018-07-10 核动力运行研究所 A kind of rinse-system for horizontal steam generator header blowdown cave room
CN108266717B (en) * 2016-12-30 2023-11-24 核动力运行研究所 Flushing system for drain cavity of collecting pipe of horizontal steam generator

Also Published As

Publication number Publication date
CN103406226B (en) 2015-06-17

Similar Documents

Publication Publication Date Title
WO2024120465A1 (en) Concrete-lined hdpe pipe repair device
CN203417802U (en) Sludge cleaning nozzle device used for steam generator in EPR type nuclear power plant
CN106931825A (en) A kind of rubber ball cleaning robot device
CN103406226A (en) Vapor generator sludge washing nozzle device for EPR (European pressurized reactor) type nuclear power plant
CN203672224U (en) Automatic washing heat exchange device
CN106914355A (en) A kind of electric sprinkling spray gun
CN107088562A (en) Pipeline cleaning
CN206794287U (en) A kind of hydrogenerator aerial cooler cleaning means
CN103759576A (en) Heat exchange equipment with automatic cleaning function
CN109654938A (en) A kind of the condenser on-line cleaning device and cleaning method of supercavity high-pressure water jet
CN108889731A (en) A kind of high-pressure jet cleaning method and device
CN102364292B (en) High-pressure dirt flushing multi-tube pass shell-and-tube heat exchange equipment and high-pressure dirt flushing method
CN209909873U (en) Steam pocket buffer device of waste heat boiler
CN203750931U (en) Rotary cleaning and descaling device for oil pipe
CN109967422B (en) High-pressure water flushing nozzle for sludge of secondary side pipe plate of steam generator
CN202304587U (en) Multi-tube pass shell and tube heat exchange equipment employing high-pressure contaminant sluicing
CN208555351U (en) A kind of high-pressure jet cleaning device
CN203024648U (en) Multifunctional online cleaning device for steam condenser
CN215765038U (en) Steam soot blower for newly-added boiler superheater
CN204153929U (en) Hydraulically powered side thruster
CN109433705A (en) A kind of gun body rinsed for Steam Generator Support Plate body refuse
CN104595882A (en) Descaling device of gas steam generator
CN209663842U (en) A kind of gun body rinsed for Steam Generator Support Plate body refuse
CN107952769A (en) A kind of cleaning device of motorcycle tank
WO2021051998A1 (en) Boiler water-cooled wall cleaning apparatus and working method

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant