CN103393854B - A kind of god's moxibustion plants essential oil and preparation method and application - Google Patents
A kind of god's moxibustion plants essential oil and preparation method and application Download PDFInfo
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Abstract
The invention belongs to middle Aesculapius's moxibustion field, particularly relate to a kind of god's moxibustion plants essential oil and preparation method and application, it is characterised in that: formula is made up of the material component of following mass parts: Radix Aconiti 10 40 parts, Herba speranskiae tuberculatae 25 55 parts, Radix Angelicae Pubescentis 20 50 parts, 7 22 parts of Borneolum Syntheticum, 23 56 parts of FENGXIAN clothing, Radix Clematidis 16 48 parts, Radix Scutellariae 61 95 parts, Radix Et Rhizoma Nardostachyos 45 83 parts, Stigma Croci 37 68 parts, Herba Taraxaci 50 88 parts, Herba Menthae 10 30 parts.Moxibustion plants essential oil is nontoxic, have no side effect for god, and soothing the channels and quicking the network vessels, quickly alleviating pain；More traditional to process the method moxibustion time short, and ordinary people is easily mastered, and adapts to the live and work rhythm needs of modern；Have only to, the spray gently toward affected part of " god processs " quintessence oil, cover 30 seconds with palm (Laogongxue) immediately, it is possible to reach the effect of traditional moxibustion, safety and stability.
Description
Technical field
The invention belongs to middle Aesculapius's moxibustion field, particularly relate to a kind of god's moxibustion plants essential oil and preparation method and application.
Background technology
The demand of the demand health that human survival is most basic, the mankind, except eating, wear, and are secondly exactly healthy. at present, and cervical vertebra
The sickness rate of the common chronic diseases such as disease, scapulohumeral periarthritis, lumbago, intervertebral disk hernia, dysmenorrhea, prostatosis, rheumatism and asthma is very
Greatly, it may be said that the people of 90% has the disease that one or more are above-mentioned.But, these diseases, current treatment means is nothing but hands
Art, traction, massage, and analgesic.The expense of operation is huge, and risk is the hugest, simultaneously it cannot be guaranteed that effect a radical cure；Massage only serves slow
The effect solved；Analgesic is the most interim, and has the biggest toxic and side effects, and cannot cure at all, eats medicines many more also
It it is waste.And long-time, strong dose thing has the biggest toxic and side effects.
People carry out treating or alleviating slight illness with acupuncture again.Acupuncture, is the rarity of Chinese medical culture.But, pin and moxibustion are to have
The biggest difference, it is impossible to mutually replace.Pin, it is simply that use acupuncture skin point；Moxibustion, it is simply that be placed on body with Folium Artemisiae Argyi or other drug
Burn on the acupuncture point of table, temperature is pressed, and borrows heating power and the effect of medicine of moxibustion fire, by the conduction of meridians, plays temperature venting QI-blood, holds up
The most eliminating evil effect；Thus reach to treat disease and the purpose one outer treating method of prevention and health care.Gu has saying of " moxibustion treatment all kinds of diseases and ailments "
Method.In moxibustion therapy can extensively be treated, outward, woman, youngster, five official rank each section diseases, to various acute diseases, chronic disease, commonly encountered diseases, difficult disease
All can treat.
Although moxibustion therapy effect is magical, but in traditional use, there are two big defects；1, fire-cure the acupuncture point time too with Folium Artemisiae Argyi
Long, general seance needs half an hour more than, one day minimum needs twice.2, use strongly professional, common people are not
Being easily mastered, this can not meet the live and work rhythm of modern.
In recent years, the development advanced by leaps and bounds along with biological purification technique, " god's moxibustion " this traditional Chinese medical science rarity starts to show up prominently.
Acupuncture can control all kinds of diseases and ailments, and god's moxibustion is then to develop to come on the basis of the curative principle of acupuncture, eliminates the suffering of flesh of acupuncture, onset
Speed is fast, more powerful, blood circulation promoting and blood stasis dispelling and analgesic effect faster, more thoroughly.And above disease can cross use plants essential oil, " god's moxibustion "
Quickly, well alleviate, and reach clinical symptom disappearance, reach the effect cured.
Therefore, a kind of needed for the quintessence oil used by god's moxibustion treatment treatment is at present.
Summary of the invention
In order to solve above technical problem, the present invention provides a kind of god's moxibustion plants essential oil and preparation method and application, god
Moxibustion plants essential oil is nontoxic, have no side effect, and soothing the channels and quicking the network vessels, quickly alleviating pain；Application process is simple, and the time is fast, easily grasps.
Solve a kind of god's moxibustion plants essential oil of above technical problem, it is characterised in that: formula is by the raw material of following mass parts
Component forms: Radix Aconiti 10-40 part, Herba speranskiae tuberculatae 25-55 part, Radix Angelicae Pubescentis 20-50 part, Borneolum Syntheticum 7-22 part, FENGXIAN clothing 23-56 part, Wheeling
Celestial 16-48 part, Radix Scutellariae 61-95 part, Radix Et Rhizoma Nardostachyos 45-83 part, Stigma Croci 37-68 part, Herba Taraxaci 50-88 part, Herba Menthae 10-30 part.
In the present invention, this formula also can be made up of the material component of following mass parts: Radix Aconiti 15-35 part, Herba speranskiae tuberculatae 30-50
Part, Radix Angelicae Pubescentis 25-45 part, Borneolum Syntheticum 10-19 part, FENGXIAN clothing 30-50 part, Radix Clematidis 20-42 part, Radix Scutellariae 68-87 part, Radix Et Rhizoma Nardostachyos 50-75
Part, Stigma Croci 40-60 part, Herba Taraxaci 55-80 part, Herba Menthae 15-25 part.
Further formula can be made up of the material component of following mass parts: Radix Aconiti 25 parts, Herba speranskiae tuberculatae 40 parts, Radix Angelicae Pubescentis 35 parts,
15 parts of Borneolum Syntheticum, 45 parts of FENGXIAN clothing, Radix Clematidis 30 parts, Radix Scutellariae 80 parts, Radix Et Rhizoma Nardostachyos 60 parts, Stigma Croci 50 parts, Herba Taraxaci 65 parts, Herba Menthae 20
Part.
The preparation method of a kind of god's moxibustion plants essential oil in the present invention, it is characterised in that: comprise the following steps:
(1) screening raw material, weighs the Radix Aconiti of weight portion in formula, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, sweet
Pine, Stigma Croci, Herba Taraxaci, pulverize with pulverizer after cleaning;
(2) Radix Angelicae Pubescentis after pulverizing in step (1), FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and thin
Lotus is placed in steeping tank, is subsequently adding the ethanol solution mix and blend of 50-75% in terms of total raw material weight portion, is heated to temperature 60-
65 DEG C, 20-60 minute time, cooling is soaked；Continuously repeat 6 days, then filter, by filtrate heating and refluxing extraction, reclaim ethanol,
Reclaim the filtrate after ethanol standby;
(3) by the filtrate carbon dioxide supercritical fluid extraction after recovery ethanol in step (2), pressure 25-35MPa, temperature
450-550 DEG C, time 2-4 h, CO2 flow 10-18 kg/h, collects volatile oil A storage standby;
(4) Radix Aconiti of weight portion in formula, Herba speranskiae tuberculatae are added 7-13 times of deionized water and soak, with Radix Aconiti, Herba speranskiae tuberculatae
Listed as parts by weight；Again with carbon dioxide supercritical fluid extraction, pressure 25-35 MPa, temperature 35-45 DEG C, time 1-3 h,
CO2Flow 10-18 kg/h, collects quintessence oil B storage standby;
(5) quintessence oil A, quintessence oil B, Borneolum Syntheticum and ethanol with the ratio mixed preparing of 1:1:0.5:4 and be get final product.
The preparation method of further plants essential oil in the present invention, it is characterised in that: comprise the following steps:
(1) screening raw material, weighs the Radix Aconiti of weight portion in formula, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, sweet
Pine, Stigma Croci, Herba Taraxaci, pulverize with pulverizer after cleaning;
(2) Radix Angelicae Pubescentis after pulverizing in step (1), FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and thin
Lotus is placed in steeping tank, is subsequently adding the ethanol solution mix and blend of in terms of total raw material weight portion 60%, is heated to temperature 62 DEG C,
40 minutes time, cooling is soaked；Continuously repeat 6 days, then filter, by filtrate heating and refluxing extraction, reclaim ethanol, reclaim ethanol
After filtrate standby;
(3) by the filtrate carbon dioxide supercritical fluid extraction after recovery ethanol in step (2), pressure 30 MPa, temperature 500
DEG C, time 3 h, CO2 flow 14 kg/h, collects volatile oil A storage standby;
(4) Radix Aconiti of weight portion, Herba speranskiae tuberculatae in formula are added 10 times of deionized waters and soak, with Radix Aconiti, the weight of Herba speranskiae tuberculatae
Amount part calculates；Again with carbon dioxide supercritical fluid extraction, pressure 30 MPa, temperature 40 DEG C, time 1.5 h, CO2Flow 14
Kg/h, collects quintessence oil B storage standby;(5) by quintessence oil A, quintessence oil B, Borneolum Syntheticum and ethanol with the ratio mixed preparing of 1:1:0.5:4
Obtain.
Elite after natural Chinese medicinal herb separates is applied in moxibustion product, it is possible to reaches soothing the channels and quicking the network vessels, quickly alleviating pain, eradicates
The effect of disease.Quintessence oil molecule is nano molecular, the god in the present invention is processed quintessence oil and is sprayed at sufferer, then cover 25-with palm
35 seconds, it is possible to reach traditional moxibustion effect.Disease can be alleviated, stop pain, relieving fatigue: stiff neck, toothache, lumbago,
Cervical vertebra pain, scapulohumeral periarthritis, arthritis, headache, relieving alcoholic intoxication, tired etc..
Combine with Long-term clinical experience first with motherland's theories of Chinese materia medica and traditional Chinese medical science sunburn treatment therapy, multiple by using
Technological means filter out Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, Borneolum Syntheticum, FENGXIAN clothing, Radix Clematidis, Herba Menthae, Borneolum Syntheticum, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci,
Chinese herbal medicine primary raw material and the consumptions such as Herba Taraxaci, in conjunction with preparation technology, carry out the compound recipe filtered out extracting deep processing, according to
Formula, meets and extracts it and play useful effect, the liquid of the moxibustion prescription of extraction, and is applied in god's moxibustion, produces safe nothing
The product of side effect.Stigma Croci in god's moxibustion, Moschus, Radix Clematidis, FENGXIAN clothing, chase after the rare Chinese medicines such as saturating, the GUCAO of wind and there is work
Blood goes to become silted up;Clearing away heat and cooling blood effect, with Herba Menthae, the strong permeability of Borneolum Syntheticum does propellant, the efficacy of a drug and moxibustion power and thoroughly can suffer from 7-11 second power
Place, antiinflammatory detumescent, alleviating pain.
Preparation method of the present invention is realized by the method such as supercritical carbon dioxide extraction (SC-CO2), with traditional method and newly
Technology is compared, and has transitory efficient, clean environment firendly, the excellent advantage of quality.Modern technologies are used to extract Chinese herbal medicine, maximum
That changes utilizes Chinese material medicine resource.
In the present invention, quintessence oil molecule is nano molecular, makes " god's moxibustion " quintessence oil liquid immersion power higher, and curative effect is more rapid bright
Aobvious.The superpower infiltration of ionic state medicine, hasty breaching epidermis cell tissue barrier, penetrates into focus deep layer, through pathological tissues, onset
Need only 10 seconds, thus the symptom that reaches to ease the pain at once, the effect for the treatment of both the principal and secondary aspects of a disease.Affected part target footpath is administered, and high concentration medicine goes directly
Focus, gets through passages through which vital energy circulates, convenient and swift, efficiently concentrates.Ionic state active factors repairs damaged part, drives away numbness and trembles with fear, does not stay future trouble.
The present invention is more traditional, and to process the method moxibustion time short, and ordinary people is easily mastered, and adapts to the live and work rhythm of modern
Need；Have only to, the spray gently toward affected part of " god processs " quintessence oil, cover 30 seconds with palm (Laogongxue) immediately, it is possible to reach
The effect of traditional moxibustion, safety and stability.
Figure of description
Fig. 1 is the human skin patch result in the present invention
Fig. 2 is guinea pig skin allergy result of the test in the present invention
Fig. 3 is Micro biological Tests result in the present invention
Detailed description of the invention
Embodiment 1
Concrete steps include the following:
(1) screening raw material, weighs the Radix Aconiti 10 parts of weight portion in formula, Herba speranskiae tuberculatae 25 parts, Radix Angelicae Pubescentis 20 parts, FENGXIAN clothing 23
Part, Radix Clematidis 16 parts, Radix Scutellariae 61 parts, Radix Et Rhizoma Nardostachyos 45 parts, Stigma Croci 37 parts, Herba Taraxaci 50 parts, pulverize with pulverizer after cleaning;
(2) Radix Angelicae Pubescentis after pulverizing in step (1), FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and thin
Lotus 10 parts is placed in steeping tank, is subsequently adding the ethanol solution mix and blend of 50-75% in terms of total raw material weight portion, is heated to temperature
Spending 60-65 DEG C, 20-60 minute time, cooling is soaked；Continuously repeat 6 days, then filter, by filtrate heating and refluxing extraction, reclaim
Ethanol, reclaims the filtrate after ethanol standby;
(3) by the filtrate carbon dioxide supercritical fluid extraction after recovery ethanol in step (2), pressure 30MPa, temperature 500
DEG C, time 3h, CO2 flow 14kg/h, collects volatile oil A storage standby;
(4) Radix Aconiti after pulverizing in step (1), Herba speranskiae tuberculatae are soaked with 7-13 times of deionized water in adding steeping tank, with
Radix Aconiti, the listed as parts by weight of Herba speranskiae tuberculatae；Again with carbon dioxide supercritical fluid extraction, pressure 30 MPa, temperature 40 DEG C, time 2h,
CO2Flow 14 kg/h, collects quintessence oil B storage standby;
(5) quintessence oil A, quintessence oil B, 7 parts of Borneolum Syntheticum and ethanol are obtained with the ratio mixed preparing of 1:1:0.5:4.
God's moxibustion therapy comes from Tibetan medicine in ancient times, with Chinese medicine meridian theory as rationale, gathers the medical herbs that power of impregnation is strong, to execute
The heating power in the person centre of the palm and intrinsic vigour are motive force, play curative effect of medication, thermotherapy and three kinds of curative effects of acupoint stimulation in affected part.My god
Elite after so Chinese herbal medicine separates is applied in moxibustion product, it is possible to reaches soothing the channels and quicking the network vessels, quickly alleviating pain, eradicates the work of disease
With.God in the present invention is processed quintessence oil be sprayed at sufferer, then cover 25-35 second with palm, it is possible to reach traditional moxibustion effect
Really.
The present invention is under hiding the guidance passing medical science QI and blood meridian theory, on the basis of hiding biography ancient prescription, uses in the modern times
Medicine purifies the extractive technique a kind of palm moxibustion therapy auxiliary agent from multiple rare Chinese medicine purification.According to human lesion meeting
The principle sensed by relevant meridians, the thermodynamic activity produced when sending out merit by palm penetrates into skin, reaches medication, moxibustion, pin
Treat the purpose of triple effect unification.
Embodiment 2
Raw material dosage Radix Aconiti 15 parts, Herba speranskiae tuberculatae 30 parts, Radix Angelicae Pubescentis 25 parts, 10 parts of Borneolum Syntheticum, 30 parts of FENGXIAN clothing, Radix Clematidis 20 parts,
Radix Scutellariae 68 parts, Radix Et Rhizoma Nardostachyos 50 parts, Stigma Croci 40 parts, Herba Taraxaci 55 parts, Herba Menthae 15 parts.
Concrete steps such as embodiment 1.
Screening draws effective ingredient, and has drawn the monomer of physiotherapy function；Elite application after natural Chinese medicinal herb is separated
In moxibustion product, it is possible to reach soothing the channels and quicking the network vessels, quickly alleviating pain, eradicate the effect of disease.
Embodiment 3
Radix Aconiti 35 parts, Herba speranskiae tuberculatae 50 parts, Radix Angelicae Pubescentis 45 parts, 19 parts of Borneolum Syntheticum, 50 parts of FENGXIAN clothing, Radix Clematidis 42 parts, Radix Scutellariae 87 parts,
Radix Et Rhizoma Nardostachyos 75 parts, Stigma Croci 60 parts, Herba Taraxaci 80 parts, Herba Menthae 25 parts.
Extracting pressure 25MPa in step (3), temperature 450 DEG C, time 4 h, CO2 flow 18 kg/h；
Extracting pressure 25 MPa in step (4), temperature 35 DEG C, time 3 h, CO2Flow 18 kg/h
Other concrete steps such as embodiment 1.
Embodiment 4
Radix Aconiti 40 parts, Herba speranskiae tuberculatae 55 parts, Radix Angelicae Pubescentis 50 parts, 22 parts of Borneolum Syntheticum, 56 parts of FENGXIAN clothing, Radix Clematidis 48 parts, Radix Scutellariae 95 parts,
Radix Et Rhizoma Nardostachyos 83 parts, Stigma Croci 68 parts, Herba Taraxaci 88 parts, Herba Menthae 30 parts.
Extracting pressure 35MPa in step (3), temperature 550 DEG C, time 2h, CO2 flow 10 kg/h；
Extracting pressure 35 MPa in step (4), temperature 45 C, time 1 h, CO2Flow 10 kg/h
Other concrete steps such as embodiment 1.
Embodiment 5
Radix Aconiti 25 parts, Herba speranskiae tuberculatae 40 parts, Radix Angelicae Pubescentis 35 parts, 15 parts of Borneolum Syntheticum, 45 parts of FENGXIAN clothing, Radix Clematidis 30 parts, Radix Scutellariae 80 parts,
Radix Et Rhizoma Nardostachyos 60 parts, Stigma Croci 50 parts, Herba Taraxaci 65 parts, Herba Menthae 20 parts.
Concrete steps such as embodiment 1.
Embodiment 6
Radix Aconiti 20 parts, Herba speranskiae tuberculatae 35 parts, Radix Angelicae Pubescentis 30 parts, 12 parts of Borneolum Syntheticum, 38 parts of FENGXIAN clothing, Radix Clematidis 25 parts, Radix Scutellariae 75 parts,
Radix Et Rhizoma Nardostachyos 55 parts, Stigma Croci 45 parts, Herba Taraxaci 60 parts, Herba Menthae 18 parts.
Concrete steps such as embodiment 1.
Embodiment 7
Radix Aconiti 30 parts, Herba speranskiae tuberculatae 45 parts, Radix Angelicae Pubescentis 39 parts, 16 parts of Borneolum Syntheticum, 47 parts of FENGXIAN clothing, Radix Clematidis 35 parts, Radix Scutellariae 82 parts,
Radix Et Rhizoma Nardostachyos 63 parts, Stigma Croci 35 parts, Herba Taraxaci 70 parts, Herba Menthae 22 parts.
Concrete steps such as embodiment 1.
God's moxibustion plants essential oil and tradition palm moxibustion liquid comparison in performance and functional parameter in the present invention: table 1
Refreshing moxibustion plants essential oil from the present invention understands in comparing with the performance indications of traditional product, and this product is natural, steady
Fixed, the feature such as safely, effectively.
The present invention has also done following experiment, further illustrates the performance that god's moxibustion plants essential oil is relevant:
Experimental example 1
Human skin patch
Test number 30 people, age 20-59 year, male 2 people, female 28 people.
Test method: select qualified speckle examination device, to close patch test method, tested contributing 0.03mL is applied to speckle examination
In device, external special adhesive tape is pasted on experimenter back, removes tested material after 24 hours, after patch test 0.5,24,
Within 28 hours, observe dermoreaction, record its result by dermoreaction grade scale in " cosmetics health specification " (2007 editions).
Result of the test such as Fig. 1.
Result of the test shows, in 30 people, 1 example occurs that two grades of skin adverse reactions occur in one-level skin adverse reaction, 1 example.This
In invention, god's moxibustion quintessence oil sound response reaches more than 93%.
Experimental example 2
Guinea pig skin allergy is tested
Subjects: the Albino guinea pig 40 just grown up, male and female half and half, body weight 200-500 gram.
Test method: Cavia porcellus is placed on temperature 18-25 degree, after observing 5 days, determines skin in the environment of relative humidity 40-70%
Skin stands intact.Test the previous day remove Cavia porcellus shoulder left dorsal 4*6cm region by hair, go to hair-fields with distilled water after being sufficiently humidified so as to
After, take induced concentration tested material 0.2Ml, be evenly coated in left side and go on hair-fields, cover with two-layer gauze and one layer of cellophane, then with
Non-stimulated immobilization with adhesive tape 6h.The 14d of 7d is repeated once in the same way, 14d after last is induced, and will excite being subject to of concentration
Examination thing 0.2mL is coated directly on the right side of 2*4cm and goes to hair-fields (24h depilation before contact), then covers with two-layer gauze and one layer of cellophane
Lid, then with non-stimulated immobilization with adhesive tape 6h, excite contact to terminate rear 24h, 28h and observe dermoreaction.By " cosmetics health specification "
In (2007 editions), regulation, carries out sensitization strength grading to experimental animal.
Result of the test such as Fig. 2.
Result of the test shows: erythema, edema does not occurs in negative control treated animal, to Cavia porcellus sensitization rate 0%；Tested material group is moved
There is not erythema, edema in thing, to Cavia porcellus sensitization rate 0%；Positive control treated animal all occurs that erythema in various degree and part are dynamic
There is edema, sensitization rate 100% in thing.
(note: positive thing is the 2 of Solution on Chemical Reagents in Shanghai company, 4-dinitro-chloro-benzene, concentration 2% excites concentration 1%, with third
Ketone makees solvent preparation.Tested material is the refreshing moxibustion plants essential oil in the present invention, induced concentration and to excite concentration to be former during test
Sample.)
Experimental example 3
Micro biological Tests
Result of the test such as Fig. 3, in microorganism tolerance band.
Claims (7)
1. a refreshing moxibustion plants essential oil, it is characterised in that: it is made up of the material component of following weight portion: Radix Aconiti 10-40 part, deep
Grass 25-55 part, Radix Angelicae Pubescentis 20-50 part, Borneolum Syntheticum 7-22 part, Impatientis clothing 23-56 part, Radix Clematidis 16-48 part, Radix Scutellariae 61-95 part, Radix Et Rhizoma Nardostachyos
45-83 part, Stigma Croci 37-68 part, Herba Taraxaci 50-88 part, Herba Menthae 10-30 part.
A kind of god's moxibustion plants essential oil the most according to claim 1, it is characterised in that: by the material component system of following weight portion
Become: Radix Aconiti 15-35 part, Herba speranskiae tuberculatae 30-50 part, Radix Angelicae Pubescentis 25-45 part, Borneolum Syntheticum 10-19 part, Impatientis clothing 30-50 part, Radix Clematidis 20-
42 parts, Radix Scutellariae 68-87 part, Radix Et Rhizoma Nardostachyos 50-75 part, Stigma Croci 40-60 part, Herba Taraxaci 55-80 part, Herba Menthae 15-25 part.
A kind of god's moxibustion plants essential oil the most according to claim 2, it is characterised in that: by the material component system of following weight portion
Become: Radix Aconiti 25 parts, Herba speranskiae tuberculatae 40 parts, Radix Angelicae Pubescentis 35 parts, 15 parts of Borneolum Syntheticum, 45 parts of Impatientis clothing, Radix Clematidis 30 parts, Radix Scutellariae 80 parts, Radix Et Rhizoma Nardostachyos
60 parts, Stigma Croci 50 parts, Herba Taraxaci 65 parts, Herba Menthae 20 parts.
The preparation method of a kind of god's moxibustion plants essential oil the most according to claim 3, it is characterised in that: comprise the following steps:
(1) screening raw material, weighs Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, Impatientis clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, safranine according to weight portion
Flower, Herba Taraxaci, pulverize with pulverizer after cleaning;
(2) Radix Angelicae Pubescentis, Impatientis clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthae after pulverizing in step (1) are put
In steeping tank, it is subsequently adding the ethanol solution mix and blend of 50-75% in terms of total raw material weight portion, is heated to temperature 60-65
DEG C, 20-60 minute time, cooling is soaked；Continuously repeat 6 days, then filter, by filtrate heating and refluxing extraction, reclaim ethanol, return
Receive the filtrate after ethanol standby;
(3) by the filtrate carbon dioxide supercritical fluid extraction after recovery ethanol in step (2), pressure 25-35MPa, temperature 450-
550 DEG C, time 2-4 h, CO2 flow 10-18 kg/h, collects volatile oil A storage standby;
(4) Radix Aconiti of weight portion, Herba speranskiae tuberculatae in formula are added 7-13 times of deionized water and soak, with Radix Aconiti, the weight of Herba speranskiae tuberculatae
Part calculates；Again with carbon dioxide supercritical fluid extraction, pressure 25-35 MPa, temperature 35-45 DEG C, time 1-3 h, CO2 flow
Amount 10-18 kg/h, collects quintessence oil B storage standby;
(5) quintessence oil A, quintessence oil B, Borneolum Syntheticum and ethanol are obtained with the ratio mixed preparing of 1:1:0.5:4.
The preparation method of a kind of god's moxibustion plants essential oil the most according to claim 4, it is characterised in that: comprise the following steps:
(1) screening raw material, weighs Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, Impatientis clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, safranine according to weight portion
Flower, Herba Taraxaci, pulverize with pulverizer after cleaning;
(2) Radix Angelicae Pubescentis, Impatientis clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthae after pulverizing in step (1) are put
In steeping tank, it is subsequently adding the ethanol solution mix and blend of in terms of total raw material weight portion 60%, is heated to temperature 62 DEG C, time
40 minutes, cooling was soaked；Continuously repeat 6 days, then filter, by filtrate heating and refluxing extraction, reclaim ethanol, after reclaiming ethanol
Filtrate is standby;
(3) by the filtrate carbon dioxide supercritical fluid extraction after recovery ethanol in step (2), pressure 30 MPa, temperature 500 DEG C,
Time 3 h, CO2 flow 14 kg/h, collects volatile oil A storage standby;
(4) Radix Aconiti of weight portion, Herba speranskiae tuberculatae in formula are added 10 times of deionized waters and soak, with Radix Aconiti, the weight portion of Herba speranskiae tuberculatae
Calculate；Again with carbon dioxide supercritical fluid extraction, pressure 30 MPa, temperature 40 DEG C, time 1.5 h, CO2 flow 14 kg/
H, collects quintessence oil B storage standby;
(5) quintessence oil A, quintessence oil B, Borneolum Syntheticum and ethanol are obtained with the ratio mixed preparing of 1:1:0.5:4.
6. according to a kind of god's moxibustion plants essential oil described in claim 1, it is characterised in that: described god processs the quintessence oil of plants essential oil
Molecule is nano molecular.
7. according to a kind of god's moxibustion plants essential oil described in claim 1, it is characterised in that: described god is processed plants essential oil and is sprayed on
At sufferer, then cover 25-35 second with palm, it is possible to reach moxibustion effect.
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| CN201310327572.6A CN103393854B (en) | 2013-07-31 | 2013-07-31 | A kind of god's moxibustion plants essential oil and preparation method and application |
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| CN107929681A (en) * | 2017-10-30 | 2018-04-20 | 岳阳市翻天应生物科技有限公司 | One kind palm moxibustion essential oil |
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