CN103393854A - Plant essential oil for miraculous moxibustion as well as preparation method and application - Google Patents
Plant essential oil for miraculous moxibustion as well as preparation method and application Download PDFInfo
- Publication number
- CN103393854A CN103393854A CN2013103275726A CN201310327572A CN103393854A CN 103393854 A CN103393854 A CN 103393854A CN 2013103275726 A CN2013103275726 A CN 2013103275726A CN 201310327572 A CN201310327572 A CN 201310327572A CN 103393854 A CN103393854 A CN 103393854A
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- CN
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- Prior art keywords
- parts
- radix
- herba
- moxibustion
- essential oil
- Prior art date
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 241000196324 Embryophyta Species 0.000 claims abstract description 23
- 230000000694 effects Effects 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 241000207929 Scutellaria Species 0.000 claims abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 40
- 241000903946 Clematidis Species 0.000 claims description 24
- 239000003921 oil Substances 0.000 claims description 24
- CURLTUGMZLYLDI-UHFFFAOYSA-N carbon dioxide Chemical compound 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- 231100000331 toxic Toxicity 0.000 abstract description 3
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound 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Abstract
The invention belongs to the field of traditional Chinese medicine miraculous moxibustion and in particular relates to plant essential oil for miraculous moxibustion as well as a preparation method and an application. The plant essential oil is characterized by being prepared from the following raw materials in parts by weight: 10-40 parts of common monkshood mother root, 25-55 parts of garden balsam stem, 20-50 parts of doubleteeth pubescent angelica root, 7-22 parts of borneol, 23-56 parts of Fengxianyi, 16-48 parts of Chinese clematis root, 61-95 parts of baical skullcap root, 45-83 parts of nardostachyos root and rhizome, 37-68 parts of saffron, 50-88 parts of dandelion and 10-30 parts of mint. The plant essential oil for miraculous moxibustion does not have toxic or side effects, relaxes tendons and activates collaterals, quickly stops pain, is shorter in moxibustion therapy than traditional moxibustion, is easily mastered by ordinary people, adapts to the requirements of living and working paces of modern people, can achieve the effects of the traditional moxibustion therapy only by gently spraying the essential oil onto the wounded parts and instantly covering the wounded parts with the Laogong acupoint in the palm for 30 seconds, and is safe and stable.
Description
Technical field
The invention belongs to middle Aesculapius's moxibustion field, relate in particular to a kind of refreshing moxibustion plants essential oil and preparation method and application.
Background technology
The demand of the most basic demand of human survival-health, the mankind are except eating, wear, secondly be exactly healthy. at present, the sickness rate of the common chronic diseases such as cervical spondylosis, scapulohumeral periarthritis, lumbago, intervertebral disk hernia, dysmenorrhea, prostatosis, rheumatism and asthma is very large, can say that 90% people has one or more above-mentioned diseases.Yet these diseases, present treatment means are nothing but operations, traction, massage, and analgesic.The expense of operation is huge, and risk is also huge, can not guarantee radical cure simultaneously; The effect of alleviation is only played in massage; Analgesic is interim especially, and very large toxic and side effects is arranged, and can't cure at all, and eating many again medicines is also waste.And long-time, the strong dose thing has very large toxic and side effects.
People treat with acupuncture again or alleviate slight illness.Acupuncture is the rarity of Chinese medical culture.But pin and moxibustion have very large difference, can not mutually replace.Pin, use the acupuncture skin point exactly; Moxibustion, with Folium Artemisiae Argyi or other drug, be placed on the acupuncture point of body surface exactly burn, temperature presses, and borrows the effect of heating power and the medicine of moxibustion light, by the conduction of meridians, plays warm venting QI-blood, the effect of strengthening vital QI to eliminate pathogenic factors; Thereby reach a kind of outer treating method of purpose for the treatment of disease and prevention and health care.Gu has the saying of " moxibustion treatment all kinds of diseases and ailments ".In moxibustion therapy can extensively be treated, outer, the woman, youngster, each section's disease such as face, to various acute diseases, chronic disease, commonly encountered diseases, difficult disease all can treat.
Although moxibustion therapy effect mystery, have two large defects in traditional use; 1, oversize with Folium Artemisiae Argyi acupuncture point time of fire-cureing, more than general seance needed half an hour, minimum needs were twice in one day.2, use strongly professionally, common people are not easy to grasp, and this can not meet modern's live and work rhythm.
In recent years, along with the development that biological purification technique is advanced by leaps and bounds, " refreshing moxibustion " this traditional Chinese medical science rarity starts to show up prominently.Acupuncture can be controlled all kinds of diseases and ailments, and refreshing moxibustion is to develop and come on the curative principle basis of acupuncture, has exempted the suffering of flesh of acupuncture, and onset speed is fast, and is more powerful, and blood circulation promoting and blood stasis dispelling and analgesic effect are faster, and be more thorough.And above disease can be crossed the use plants essential oil, and " refreshing moxibustion " is very fast, well alleviation, and reaches clinical symptom disappearance, reaches the effect of healing.
Therefore, a kind of is required at present for refreshing moxibustion treatment treatment quintessence oil used.
Summary of the invention
In order to solve above technical problem, the invention provides a kind of refreshing moxibustion plants essential oil and preparation method thereof and application, refreshing moxibustion plants essential oil is nontoxic, have no side effect, and soothing the channels and quicking the network vessels, quickly alleviating pain; Application process is simple, and the time is fast, easily grasps.
Solve a kind of refreshing moxibustion plants essential oil of above technical problem, it is characterized in that: formula is comprised of the material component of following mass parts: Radix Aconiti 10-40 part, Herba speranskiae tuberculatae 25-55 part, Radix Angelicae Pubescentis 20-50 part, Borneolum Syntheticum 7-22 part, FENGXIAN clothing 23-56 part, Radix Clematidis 16-48 part, Radix Scutellariae 61-95 part, Radix Et Rhizoma Nardostachyos 45-83 part, Stigma Croci 37-68 part, Herba Taraxaci 50-88 part, Herba Menthae 10-30 part.
In the present invention, this formula also can be comprised of the material component of following mass parts: Radix Aconiti 15-35 part, Herba speranskiae tuberculatae 30-50 part, Radix Angelicae Pubescentis 25-45 part, Borneolum Syntheticum 10-19 part, FENGXIAN clothing 30-50 part, Radix Clematidis 20-42 part, Radix Scutellariae 68-87 part, Radix Et Rhizoma Nardostachyos 50-75 part, Stigma Croci 40-60 part, Herba Taraxaci 55-80 part, Herba Menthae 15-25 part.
Further formula can be comprised of the material component of following mass parts: 25 parts of Radix Aconitis, 40 parts of Herba speranskiae tuberculataes, 35 parts of Radix Angelicae Pubescentiss, 15 parts, Borneolum Syntheticum, 45 parts, FENGXIAN clothing, 30 parts of Radix Clematidis, 80 parts of Radix Scutellariaes, 60 parts of Radix Et Rhizoma Nardostachyos, 50 parts of Stigma Crocis, 65 parts of Herba Taraxacis, 20 parts of Herba Menthaes.
A kind of preparation method of refreshing moxibustion plants essential oil in the present invention is characterized in that: comprise the following steps:
(1) screen raw material, take Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, the Herba Taraxaci of weight portion in formula, after cleaning, with pulverizer, pulverize;
(2) Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthae after in step (1), pulverizing are placed in steeping tank, then add the alcoholic solution mix and blend in total raw material weight portion 50-75%, be heated to temperature 60-65 ℃, time 20-60 minute, cooling immersion; Repeat 6 days continuously, then filter, by the filtrate heating and refluxing extraction, reclaim ethanol, the filtrate for later use after recovery ethanol;
(3) filtrate after recovery ethanol in step (2) is used to carbon dioxide supercritical fluid extraction, pressure 25-35 MPa, temperature 450-550 ℃, time 2-4 h, CO2 flow 10-18 kg/h, collect volatile oil A and store standby;
(4) will fill a prescription in Radix Aconiti, the Herba speranskiae tuberculatae of weight portion add 7-13 times of deionized water to soak, with the listed as parts by weight of Radix Aconiti, Herba speranskiae tuberculatae; Use again carbon dioxide supercritical fluid extraction, pressure 25-35 MPa, temperature 35-45 ℃, time 1-3 h, CO
2Flow 10-18 kg/h, collect quintessence oil B and store standby;
(5) by quintessence oil A, quintessence oil B, Borneolum Syntheticum and ethanol with the ratio mixed preparing of 1:1:0.5:4 and get final product.
The preparation method of further plants essential oil in the present invention is characterized in that: comprise the following steps:
(1) screen raw material, take Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, the Herba Taraxaci of weight portion in formula, after cleaning, with pulverizer, pulverize;
(2) Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthae after in step (1), pulverizing are placed in steeping tank, then add the alcoholic solution mix and blend in total raw material weight portion 60%, be heated to 62 ℃ of temperature, 40 minutes time, cooling immersion; Repeat 6 days continuously, then filter, by the filtrate heating and refluxing extraction, reclaim ethanol, the filtrate for later use after recovery ethanol;
(3) filtrate after recovery ethanol in step (2) is used to carbon dioxide supercritical fluid extraction, pressure 30 MPa, 500 ℃ of temperature, times 3 h, CO2 flow 14 kg/h, collect volatile oil A and store standby;
(4) will fill a prescription in Radix Aconiti, the Herba speranskiae tuberculatae of weight portion add 10 times of deionized waters to soak, with the listed as parts by weight of Radix Aconiti, Herba speranskiae tuberculatae; Use again carbon dioxide supercritical fluid extraction, pressure 30 MPa, 40 ℃ of temperature, times 1.5 h, CO
2Flow 14 kg/h, collect quintessence oil B and store standby; (5) by quintessence oil A, quintessence oil B, Borneolum Syntheticum and ethanol with the ratio mixed preparing of 1:1:0.5:4 and get final product.
Elite after natural Chinese medicinal herb is separated is applied to, in the moxibustion product, can reach soothing the channels and quicking the network vessels, quickly alleviating pain, the effect of eradicating disease.The quintessence oil molecule is nano molecular, the god in the present invention is processed to quintessence oil and be sprayed on the sufferer place, then cover 25-35 second with palm, just can reach the traditional moxibustion effect.Can alleviate disease, stop pain, relieving fatigue: stiff neck, toothache, lumbago, cervical vertebra pain, scapulohumeral periarthritis, arthritis, headache, relieving alcoholic intoxication, tired etc.
At first utilize motherland's theories of Chinese materia medica and traditional Chinese medical science sunburn treatment therapy to combine with the Long-term clinical experience, by using multiple technological means to filter out Chinese herbal medicine primary raw material and the consumptions such as Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, Borneolum Syntheticum, FENGXIAN clothing, Radix Clematidis, Herba Menthae, Borneolum Syntheticum, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci, again in conjunction with preparation technology, the compound recipe that filters out is extracted to deep processing, according to formula, meet and to extract it and play useful effect, the liquid of the moxibustion prescription that extracts, and be applied in refreshing moxibustion, produce the product that safety has no side effect.Stigma Croci in god's moxibustion, Moschus, Radix Clematidis, the FENGXIAN clothing, chase after the rare Chinese medicines such as wind is saturating, GUCAO and have the silt of invigorating blood circulation; The clearing away heat and cooling blood effect, use Herba Menthae, and the strong permeability of Borneolum Syntheticum is done propellant, and the efficacy of a drug and moxibustion power can be at the saturating affected part of 7-11 power second, antiinflammatory detumescent, alleviating pains.
Preparation method of the present invention realizes by methods such as supercritical carbon dioxide extractions (SC-CO2), with traditional method, with new technique, compares, and has transitory efficient, clean environment firendly, the excellent advantage of quality.Adopt modern technologies to extract Chinese herbal medicine, the maximized Chinese material medicine resource that utilizes.
In the present invention, the quintessence oil molecule is nano molecular, makes " refreshing moxibustion " quintessence oil liquid immersion power stronger, and curative effect more fast obviously.The superpower infiltration of ionic state medicine, the hasty breaching epidermis cell is organized barrier, infiltrates the focus deep layer, through pathological tissues, onset need only 10 seconds, thereby reach the symptom that eases the pain at once, the effect for the treatment of both the principal and secondary aspects of a disease.The footpath administration of affected part target, the high concentration medicine focus of going directly, get through passages through which vital energy circulates, and is convenient and swift, efficient concentrating.The ionic state active factors is repaired damaged part, drives away numbness and trembles with fear, and does not stay future trouble.
The present invention is more traditional, and to process the method moxibustion time short, and the ordinary people easily grasps, and adapts to modern's live and work rhythm needs; Only need, the spray gently toward affected part of " god processs " quintessence oil, to use immediately palm (Laogongxue) to cover for 30 seconds, just can reach the effect of traditional moxibustion, safety and stability.
Figure of description
Fig. 1 is the human skin patch result in the present invention
Fig. 2 is guinea pig skin allergy result of the test in the present invention
Fig. 3 is Micro biological Tests result in the present invention
The specific embodiment
?
?Embodiment 1
Concrete steps comprise as follows:
(1) screen raw material, take 37 parts of 45 parts of 61 parts of 16 parts of 23 parts, 20 parts of 25 parts of 10 parts of Radix Aconitis, Herba speranskiae tuberculataes, Radix Angelicae Pubescentiss, FENGXIAN clothing, Radix Clematidis, Radix Scutellariaes, Radix Et Rhizoma Nardostachyos, Stigma Crocis, 50 parts of the Herba Taraxacis of weight portion in formula, after cleaning, with pulverizer, pulverize;
(2) 10 parts of the Radix Angelicae Pubescentis after pulverizing in step (1), FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthaes are placed in steeping tank, then add the alcoholic solution mix and blend in total raw material weight portion 50-75%, be heated to temperature 60-65 ℃, time 20-60 minute, cooling immersion; Repeat 6 days continuously, then filter, by the filtrate heating and refluxing extraction, reclaim ethanol, the filtrate for later use after recovery ethanol;
(3) filtrate after recovery ethanol in step (2) is used to carbon dioxide supercritical fluid extraction, pressure 30MPa, 500 ℃ of temperature, time 3h, CO2 flow 14kg/h, collect volatile oil A and store standby;
(4) Radix Aconiti, Herba speranskiae tuberculatae after in step (1), pulverizing are added in steeping tank and soak with 7-13 times of deionized water, with the listed as parts by weight of Radix Aconiti, Herba speranskiae tuberculatae; Use again carbon dioxide supercritical fluid extraction, pressure 30 MPa, 40 ℃ of temperature, time 2h, CO
2Flow 14 kg/h, collect quintessence oil B and store standby;
(5) quintessence oil A, quintessence oil B, 7 parts, Borneolum Syntheticum and the ethanol ratio mixed preparing with 1:1:0.5:4 is obtained.
God's moxibustion therapy comes from the Tibetan medicine in ancient times, take the Chinese medicine meridian theory as rationale, gathers the strong medical herbs of power of impregnation, take the heating power in the person of the executing centre of the palm and intrinsic vigour as motive force, in affected part performance curative effect of medication, thermotherapy and three kinds of curative effects of acupoint stimulation.Elite after natural Chinese medicinal herb is separated is applied to, in the moxibustion product, can reach soothing the channels and quicking the network vessels, quickly alleviating pain, the effect of eradicating disease.God in the present invention is processed to quintessence oil and be sprayed on the sufferer place, then cover 25-35 second with palm, just can reach the traditional moxibustion effect.
The present invention passes under the guidance of medical science QI and blood meridian theory in Tibetan, is hiding on the basis that passes ancient prescription, and a kind of palm moxibustion therapy that uses modern Chinese medicine purification extractive technique to form from multiple rare Chinese medicine purification is assisted and used agent.Can be by the principle of relevant meridians sensing according to human lesion, the thermodynamic activity that produces while sending out merit by palm infiltrates skin, reaches the purpose of medication, moxibustion, the unification of pin treatment triple effect.
Embodiment 2
15 parts of raw material consumption Radix Aconitis, 30 parts of Herba speranskiae tuberculataes, 25 parts of Radix Angelicae Pubescentiss, 10 parts, Borneolum Syntheticum, 30 parts, FENGXIAN clothing, 20 parts of Radix Clematidis, 68 parts of Radix Scutellariaes, 50 parts of Radix Et Rhizoma Nardostachyos, 40 parts of Stigma Crocis, 55 parts of Herba Taraxacis, 15 parts of Herba Menthaes.
Concrete steps such as embodiment 1.
Screening draws effective ingredient, and has drawn the monomer of physiotherapy function; Elite after natural Chinese medicinal herb is separated is applied to, in the moxibustion product, can reach soothing the channels and quicking the network vessels, quickly alleviating pain, the effect of eradicating disease.
Embodiment 3
35 parts of Radix Aconitis, 50 parts of Herba speranskiae tuberculataes, 45 parts of Radix Angelicae Pubescentiss, 19 parts, Borneolum Syntheticum, 50 parts, FENGXIAN clothing, 42 parts of Radix Clematidis, 87 parts of Radix Scutellariaes, 75 parts of Radix Et Rhizoma Nardostachyos, 60 parts of Stigma Crocis, 80 parts of Herba Taraxacis, 25 parts of Herba Menthaes.
Extracting pressure 25 MPa in step (3), 450 ℃ of temperature, times 4 h, CO2 flow 18 kg/h;
Extracting pressure 25 MPa in step (4), 35 ℃ of temperature, times 3 h, CO
2Flow 18 kg/h
Other concrete steps such as embodiment 1.
Embodiment 4
40 parts of Radix Aconitis, 55 parts of Herba speranskiae tuberculataes, 50 parts of Radix Angelicae Pubescentiss, 22 parts, Borneolum Syntheticum, 56 parts, FENGXIAN clothing, 48 parts of Radix Clematidis, 95 parts of Radix Scutellariaes, 83 parts of Radix Et Rhizoma Nardostachyos, 68 parts of Stigma Crocis, 88 parts of Herba Taraxacis, 30 parts of Herba Menthaes.
Extracting pressure 35 MPa in step (3), 550 ℃ of temperature, time 2h, CO2 flow 10 kg/h;
Extracting pressure 35 MPa in step (4), temperature 45 C, time 1 h, CO
2Flow 10 kg/h
Other concrete steps such as embodiment 1.
Embodiment 5
25 parts of Radix Aconitis, 40 parts of Herba speranskiae tuberculataes, 35 parts of Radix Angelicae Pubescentiss, 15 parts, Borneolum Syntheticum, 45 parts, FENGXIAN clothing, 30 parts of Radix Clematidis, 80 parts of Radix Scutellariaes, 60 parts of Radix Et Rhizoma Nardostachyos, 50 parts of Stigma Crocis, 65 parts of Herba Taraxacis, 20 parts of Herba Menthaes.
Concrete steps such as embodiment 1.
Embodiment 6
20 parts of Radix Aconitis, 35 parts of Herba speranskiae tuberculataes, 30 parts of Radix Angelicae Pubescentiss, 12 parts, Borneolum Syntheticum, 38 parts, FENGXIAN clothing, 25 parts of Radix Clematidis, 75 parts of Radix Scutellariaes, 55 parts of Radix Et Rhizoma Nardostachyos, 45 parts of Stigma Crocis, 60 parts of Herba Taraxacis, 18 parts of Herba Menthaes.
Concrete steps such as embodiment 1.
Embodiment 7
30 parts of Radix Aconitis, 45 parts of Herba speranskiae tuberculataes, 39 parts of Radix Angelicae Pubescentiss, 16 parts, Borneolum Syntheticum, 47 parts, FENGXIAN clothing, 35 parts of Radix Clematidis, 82 parts of Radix Scutellariaes, 63 parts of Radix Et Rhizoma Nardostachyos, 35 parts of Stigma Crocis, 70 parts of Herba Taraxacis, 22 parts of Herba Menthaes.
Concrete steps such as embodiment 1.
Refreshing moxibustion plants essential oil and the comparison of tradition palm moxibustion liquid on performance and functional parameter in the present invention: table 1
As can be known in relatively from the performance indications of the refreshing moxibustion plants essential oil the present invention and traditional product, the characteristics such as this product is natural, stable, safe, effective.
The present invention has also done following experiment, further illustrates the performance that refreshing moxibustion plants essential oil is relevant:
Experimental example 1
Human skin patch
Test number 30 people, age 20-59 year, male 2 people, female 28 people.
Test method: select qualified speckle examination device, with sealing patch test method, tested contributing 0.03mL is applied in speckle examination device, the external special adhesive tape sticks in the experimenter back, after 24 hours, remove tested material, respectively at after patch test 0.5,24, observe dermoreaction in 28 hours, by dermoreaction grade scale in " cosmetics health standard " (2007 editions), record its result.
Result of the test such as Fig. 1.
The result of the test demonstration, in 30 people, the one-level skin adverse reaction appears in 1 example, the secondary skin adverse reaction appears in 1 example.In the present invention, refreshing moxibustion quintessence oil sound response reaches more than 93%.
Experimental example 2
The test of guinea pig skin allergy
Subjects: 40 of the Albino guinea pigs of just growing up, male and female half and half, body weight 200-500 gram.
Test method: Cavia porcellus is placed on to temperature 18-25 degree, observes after 5 days in the environment of relative humidity 40-70%, determine that skin is excellent.The previous day is removed 4*6cm zone, left side, Cavia porcellus shoulder back by hair in test, with behind the abundant moistening rear unhairing of distilled water district, get induced concentration tested material 0.2Ml, be evenly coated in unhairing district, left side, with two-layer gauze and one deck cellophane, cover, then with non-stimulated immobilization with adhesive tape 6h.The 14d of 7d repeats once with same method, 14d after last is induced, the tested material 0.2mL that excites concentration directly is coated in to unhairing district, 2*4cm right side (24h depilation before contact), then with two-layer gauze and one deck cellophane, cover, with non-stimulated immobilization with adhesive tape 6h, excite contact to finish rear 24h, 28h and observe dermoreaction again.By regulation in " cosmetics health standard " (2007 editions), experimental animal is carried out to the sensitization strength grading.
Result of the test such as Fig. 2.
Result of the test shows: erythema, edema do not appear in the negative control treated animal, to Cavia porcellus sensitization rate 0%; Erythema, edema do not appear in the tested material treated animal, to Cavia porcellus sensitization rate 0%; The positive control treated animal occurs that all sensitization rate 100% edema appears, in various degree erythema and Some Animals.
(annotate: positive thing is 2 of Solution on Chemical Reagents in Shanghai company, the 4-dinitro-chloro-benzene, and concentration 2%, excite concentration 1%, with acetone, does the solvent preparation.Tested material is the refreshing moxibustion plants essential oil in the present invention, induced concentration and excite concentration to be former state during test.)
Experimental example 3
Micro biological Tests
Result of the test such as Fig. 3, in the microorganism tolerance band.
Claims (7)
1. refreshing moxibustion plants essential oil is characterized in that: formula is comprised of the material component of following weight portion: Radix Aconiti 10-40 part, Herba speranskiae tuberculatae 25-55 part, Radix Angelicae Pubescentis 20-50 part, Borneolum Syntheticum 7-22 part, FENGXIAN clothing 23-56 part, Radix Clematidis 16-48 part, Radix Scutellariae 61-95 part, Radix Et Rhizoma Nardostachyos 45-83 part, Stigma Croci 37-68 part, Herba Taraxaci 50-88 part, Herba Menthae 10-30 part.
2. a kind of refreshing moxibustion plants essential oil according to claim 1 is characterized in that: formula is comprised of the material component of following weight portion: Radix Aconiti 15-35 part, Herba speranskiae tuberculatae 30-50 part, Radix Angelicae Pubescentis 25-45 part, Borneolum Syntheticum 10-19 part, FENGXIAN clothing 30-50 part, Radix Clematidis 20-42 part, Radix Scutellariae 68-87 part, Radix Et Rhizoma Nardostachyos 50-75 part, Stigma Croci 40-60 part, Herba Taraxaci 55-80 part, Herba Menthae 15-25 part.
3. a kind of refreshing moxibustion plants essential oil according to claim 2 is characterized in that: formula is comprised of the material component of following weight portion: 25 parts of Radix Aconitis, 40 parts of Herba speranskiae tuberculataes, 35 parts of Radix Angelicae Pubescentiss, 15 parts, Borneolum Syntheticum, 45 parts, FENGXIAN clothing, 30 parts of Radix Clematidis, 80 parts of Radix Scutellariaes, 60 parts of Radix Et Rhizoma Nardostachyos, 50 parts of Stigma Crocis, 65 parts of Herba Taraxacis, 20 parts of Herba Menthaes.
4. the preparation method of a kind of refreshing moxibustion plants essential oil according to claim 3 is characterized in that: comprise the following steps:
(1) screen raw material, take Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, the Herba Taraxaci of weight portion in formula, after cleaning, with pulverizer, pulverize;
(2) Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthae after in step (1), pulverizing are placed in steeping tank, then add the alcoholic solution mix and blend in total raw material weight portion 50-75%, be heated to temperature 60-65 ℃, time 20-60 minute, cooling immersion; Repeat 6 days continuously, then filter, by the filtrate heating and refluxing extraction, reclaim ethanol, the filtrate for later use after recovery ethanol;
(3) filtrate after recovery ethanol in step (2) is used to carbon dioxide supercritical fluid extraction, pressure 25-35 MPa, temperature 450-550 ℃, time 2-4 h, CO2 flow 10-18 kg/h, collect volatile oil A and store standby;
(4) will fill a prescription in Radix Aconiti, the Herba speranskiae tuberculatae of weight portion add 7-13 times of deionized water to soak, with the listed as parts by weight of Radix Aconiti, Herba speranskiae tuberculatae; Use again carbon dioxide supercritical fluid extraction, pressure 25-35 MPa, temperature 35-45 ℃, time 1-3 h, CO
2Flow 10-18 kg/h, collect quintessence oil B and store standby;
(5) quintessence oil A, quintessence oil B, Borneolum Syntheticum and the ethanol ratio mixed preparing with 1:1:0.5:4 is obtained.
5. the preparation method of a kind of refreshing moxibustion plants essential oil according to claim 4 is characterized in that: comprise the following steps:
(1) screen raw material, take Radix Aconiti, Herba speranskiae tuberculatae, Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, the Herba Taraxaci of weight portion in formula, after cleaning, with pulverizer, pulverize;
(2) Radix Angelicae Pubescentis, FENGXIAN clothing, Radix Clematidis, Radix Scutellariae, Radix Et Rhizoma Nardostachyos, Stigma Croci, Herba Taraxaci and Herba Menthae after in step (1), pulverizing are placed in steeping tank, then add the alcoholic solution mix and blend in total raw material weight portion 60%, be heated to 62 ℃ of temperature, 40 minutes time, cooling immersion; Repeat 6 days continuously, then filter, by the filtrate heating and refluxing extraction, reclaim ethanol, the filtrate for later use after recovery ethanol;
(3) filtrate after recovery ethanol in step (2) is used to carbon dioxide supercritical fluid extraction, pressure 30 MPa, 500 ℃ of temperature, times 3 h, CO2 flow 14 kg/h, collect volatile oil A and store standby;
(4) will fill a prescription in Radix Aconiti, the Herba speranskiae tuberculatae of weight portion add 10 times of deionized waters to soak, with the listed as parts by weight of Radix Aconiti, Herba speranskiae tuberculatae; Use again carbon dioxide supercritical fluid extraction, pressure 30 MPa, 40 ℃ of temperature, times 1.5 h, CO
2Flow 14 kg/h, collect quintessence oil B and store standby;
(5) quintessence oil A, quintessence oil B, Borneolum Syntheticum and the ethanol ratio mixed preparing with 1:1:0.5:4 is obtained.
6. a kind of refreshing moxibustion plants essential oil described according to claim 1, it is characterized in that: the quintessence oil molecule is nano molecular.
7. a kind of refreshing moxibustion plants essential oil described according to claim 1, is characterized in that: described god is processed to plants essential oil and be sprayed on the sufferer place, then cover 25-35 second with palm, just can reach the moxibustion effect.
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CN105748749A (en) * | 2014-12-15 | 2016-07-13 | 杨树强 | Traditional Chinese medicine formula for treating cerebral arteriosclerosis by means of external application of traditional Chinese medicine |
CN107929681A (en) * | 2017-10-30 | 2018-04-20 | 岳阳市翻天应生物科技有限公司 | One kind palm moxibustion essential oil |
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CN105748749A (en) * | 2014-12-15 | 2016-07-13 | 杨树强 | Traditional Chinese medicine formula for treating cerebral arteriosclerosis by means of external application of traditional Chinese medicine |
CN107929681A (en) * | 2017-10-30 | 2018-04-20 | 岳阳市翻天应生物科技有限公司 | One kind palm moxibustion essential oil |
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