CN103387821B - Hydrogenation synthesis heat transfer oil and preparation method thereof - Google Patents
Hydrogenation synthesis heat transfer oil and preparation method thereof Download PDFInfo
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- CN103387821B CN103387821B CN201210146186.2A CN201210146186A CN103387821B CN 103387821 B CN103387821 B CN 103387821B CN 201210146186 A CN201210146186 A CN 201210146186A CN 103387821 B CN103387821 B CN 103387821B
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- transfer oil
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Abstract
The present invention relates to a kind of hydrogenation synthesis heat transfer oil and preparation method thereof, belong to the preparation field of chemical industry thermal oil, it is characterized in that adding functional agent by deep hydrogenation base oil obtains, wherein functional agent is prepared by the raw material of following massfraction: high-temperature antioxidant alkyl diphenylamine 20%; Antiager 2,6 di-t-butyl Pyrogentisinic Acids 10%; Purification agent calcium sulfenyl phenolate 25%; Purification agent middle calcium alkylbenzensulfonates 35%; KX-ZJ-01 high temperature anticoking agent 5%; KX-ZS-03 hydrogenation Scale inhibitors 5%.Molecular components is pure, can not import affect thermal oil quality and life-span organic impurity content as S, N, O and heavy metal, quality product is excellent, good heat-transfer, safety and environmental protection.
Description
Technical field
The present invention relates to a kind of hydrogenation synthesis heat transfer oil and preparation method thereof, belong to the preparation field of chemical industry thermal oil.
Background technology
At present, in the normal productive process of chemical field, often need to heat reactor etc., therefore the use of thermal oil just becomes the certainty of chemical industry, certainly not only in chemical industry, the use range of present thermal oil is more and more wider, it has and excellent reaches heat conductivility, simultaneously by the conduction of thermal oil, the object needing to receive heat is heated evenly, ensure that normally carrying out of reaction etc., but current thermal oil on the market, work-ing life is shorter, organic impurity content is introduced as S in preparation process, N, O and heavy metal, therefore cause work-ing life short, and easily cause environmental pollution.
Summary of the invention
According to the deficiencies in the prior art, the technical problem to be solved in the present invention is: provide a kind of hydrogenation synthesis heat transfer oil and preparation method thereof, good heat-transfer, the life-span is long, safety and environmental protection.
The technical solution adopted for the present invention to solve the technical problems is: provide a kind of hydrogenation synthesis heat transfer oil, it is characterized in that adding functional agent by deep hydrogenation base oil obtains, and wherein functional agent is prepared by the raw material of following massfraction:
The add-on of described functional agent is 1.5% of deep hydrogenation base oil quality.
The preparation method of described hydrogenation synthesis heat transfer oil is: proportionally joined by functional agent in deep hydrogenation base oil, fully merges obtained finished product by ultrasonic wave or mechanical stirring.
Described KX-ZJ-01 high temperature anticoking agent is that Shandong Ke Xin petrochemical complex company limited produces.
Described KX-ZS-03 hydrogenation Scale inhibitors is that Shandong Ke Xin petrochemical complex company limited produces.
The model that deep hydrogenation base oil wherein used generally uses is 60N, 100N or 150N.Wherein obtained product standard and type: K300, K320 or K350, wherein K represents hydrogenation, after digitized representation model.
The invention has the beneficial effects as follows: molecular components is pure, can not import affect thermal oil quality and life-span organic impurity content as S, N, O and heavy metal, quality product is excellent, good heat-transfer, safety and environmental protection.
Embodiment
Below in conjunction with embodiment, the present invention is described further:
Embodiment 1
Hydrogenation synthesis heat transfer oil, adds functional agent by deep hydrogenation base oil and obtains, and wherein functional agent is prepared by the raw material of following massfraction:
The add-on of functional agent is 1.5% of deep hydrogenation base oil quality.
KX-ZJ-01 high temperature anticoking agent is that Shandong Ke Xin petrochemical complex company limited produces.
KX-ZS-03 hydrogenation Scale inhibitors is that Shandong Ke Xin petrochemical complex company limited produces.
The preparation method of hydrogenation synthesis heat transfer oil is: proportionally joined by functional agent in deep hydrogenation base oil, fully merges obtained finished product by ultrasonic wave or mechanical stirring.
The performance index of product see the following form.
Claims (4)
1. a hydrogenation synthesis heat transfer oil, it is characterized in that adding functional agent by deep hydrogenation base oil obtains, and wherein functional agent is prepared by the raw material of following massfraction:
The add-on of described functional agent is 1.5% of deep hydrogenation base oil quality.
2. hydrogenation synthesis heat transfer oil according to claim 1, it is characterized in that the preparation method of described hydrogenation synthesis heat transfer oil is: proportionally joined by functional agent in deep hydrogenation base oil, fully merge obtained finished product by ultrasonic wave or mechanical stirring.
3. hydrogenation synthesis heat transfer oil according to claim 1, is characterized in that described KX-ZJ-01 high temperature anticoking agent is that Shandong Ke Xin petrochemical complex company limited produces.
4. hydrogenation synthesis heat transfer oil according to claim 1, is characterized in that described KX-ZS-03 hydrogenation Scale inhibitors is that Shandong Ke Xin petrochemical complex company limited produces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210146186.2A CN103387821B (en) | 2012-05-07 | 2012-05-07 | Hydrogenation synthesis heat transfer oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210146186.2A CN103387821B (en) | 2012-05-07 | 2012-05-07 | Hydrogenation synthesis heat transfer oil and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103387821A CN103387821A (en) | 2013-11-13 |
| CN103387821B true CN103387821B (en) | 2016-01-20 |
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| CN201210146186.2A Active CN103387821B (en) | 2012-05-07 | 2012-05-07 | Hydrogenation synthesis heat transfer oil and preparation method thereof |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104388056B (en) * | 2014-07-07 | 2018-05-18 | 山东华安新材料有限公司 | A kind of high preparation process and application method for leading conduction oil |
| CN105315969A (en) * | 2014-07-07 | 2016-02-10 | 上海久星导热油股份有限公司 | High temperature modified heat conduction oil and preparation method thereof |
| CN104893684B (en) * | 2015-06-29 | 2018-05-18 | 成都迈斯拓新能源润滑材料股份有限公司 | A kind of anti-coking hydrogenation conduction oil and preparation method thereof |
| CN105038719A (en) * | 2015-07-08 | 2015-11-11 | 新疆福克油品股份有限公司 | Chemically synthesized alkyl naphthalene heat transfer fluid composition |
| CN107059018A (en) * | 2017-05-27 | 2017-08-18 | 安徽卓远化工科技有限公司 | A kind of refinery's corrosion inhibiter and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1081198A (en) * | 1992-07-10 | 1994-01-26 | 广东石油化工专科学校科技开发公司 | A kind of heat-conducting oil for electric heating device |
| CN1803997A (en) * | 2005-12-12 | 2006-07-19 | 中国石油化工集团公司 | Method for preparing base oil of heat transfer oil |
| CN101679843A (en) * | 2006-09-26 | 2010-03-24 | 雪佛龙美国公司 | Heat transfer oil with high auto ignition temperature |
-
2012
- 2012-05-07 CN CN201210146186.2A patent/CN103387821B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1081198A (en) * | 1992-07-10 | 1994-01-26 | 广东石油化工专科学校科技开发公司 | A kind of heat-conducting oil for electric heating device |
| CN1803997A (en) * | 2005-12-12 | 2006-07-19 | 中国石油化工集团公司 | Method for preparing base oil of heat transfer oil |
| CN101679843A (en) * | 2006-09-26 | 2010-03-24 | 雪佛龙美国公司 | Heat transfer oil with high auto ignition temperature |
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| CN103387821A (en) | 2013-11-13 |
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Address after: 255400 Xinhua Road, Linzi District, Zibo, Shandong Province, No. 161 Patentee after: Shandong English New Material Technology Co., Ltd. Address before: 255434 Xinhua Road, Qilu Petrochemical, Zibo, Shandong Province, No. 161 Patentee before: Shandong Enkli Chemical Co., Ltd. |
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