CN103361153B - Water-based cutting solution and method for preparing same - Google Patents
Water-based cutting solution and method for preparing same Download PDFInfo
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- CN103361153B CN103361153B CN201310247512.3A CN201310247512A CN103361153B CN 103361153 B CN103361153 B CN 103361153B CN 201310247512 A CN201310247512 A CN 201310247512A CN 103361153 B CN103361153 B CN 103361153B
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- water
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- based cutting
- cutting solution
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 238000005520 cutting process Methods 0.000 title abstract description 7
- 238000000034 method Methods 0.000 title abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 229920001732 Lignosulfonate Polymers 0.000 claims abstract description 7
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 claims abstract description 7
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 7
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 7
- 229940068968 polysorbate 80 Drugs 0.000 claims abstract description 7
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims abstract description 7
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims abstract description 7
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 claims abstract description 7
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 4
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000011701 zinc Substances 0.000 claims abstract description 4
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 4
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 239000002173 cutting fluid Substances 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 claims description 9
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 6
- VGGLHLAESQEWCR-UHFFFAOYSA-N N-(hydroxymethyl)urea Chemical compound NC(=O)NCO VGGLHLAESQEWCR-UHFFFAOYSA-N 0.000 claims description 6
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- WERKSKAQRVDLDW-ANOHMWSOSA-N [(2s,3r,4r,5r)-2,3,4,5,6-pentahydroxyhexyl] (z)-octadec-9-enoate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO WERKSKAQRVDLDW-ANOHMWSOSA-N 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- LSXWFXONGKSEMY-UHFFFAOYSA-N di-tert-butyl peroxide Chemical compound CC(C)(C)OOC(C)(C)C LSXWFXONGKSEMY-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 235000019357 lignosulphonate Nutrition 0.000 claims description 6
- 229940045641 monobasic sodium phosphate Drugs 0.000 claims description 6
- WBHHMMIMDMUBKC-QJWNTBNXSA-N ricinoleic acid Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(O)=O WBHHMMIMDMUBKC-QJWNTBNXSA-N 0.000 claims description 6
- 229960003656 ricinoleic acid Drugs 0.000 claims description 6
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 6
- -1 2-amino-2-methyl-1-propyl Chemical group 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 abstract description 5
- 238000001816 cooling Methods 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract description 3
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
- 230000002411 adverse Effects 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 235000010299 hexamethylene tetramine Nutrition 0.000 abstract 1
- 230000001050 lubricating effect Effects 0.000 abstract 1
- 239000012528 membrane Substances 0.000 abstract 1
- 229960004011 methenamine Drugs 0.000 abstract 1
- 229910000403 monosodium phosphate Inorganic materials 0.000 abstract 1
- 235000019799 monosodium phosphate Nutrition 0.000 abstract 1
- 235000015393 sodium molybdate Nutrition 0.000 abstract 1
- 239000011684 sodium molybdate Substances 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Lubricants (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Abstract
The invention relates to a water-based cutting solution and a method for preparing the same. The water-based cutting solution is characterized by being prepared from the following raw materials in parts by weight: 3-4 parts of methenamine, 1-2 parts of zinc dialkyl dithiophosphate, 1-2 parts of sodium molybdate, 1-2 parts of sodium dihydrogen phosphate, 2-3 parts of polysorbate 80, 1-2 parts of lignin sulfonate, 2-3 parts of methyl triethoxysilane, 5-6 parts of a membrane additive and 260 parts of water. All the raw materials are non-toxic and environmental friendly. The water-based cutting solution provided by the invention is scientific in formula and has good lubricating, cooling and cleaning and rust preventing performances. With a rust removing function, the water-based cutting solution can protect a cutter so that the cutter has a long service life and can prevent a processed workpiece from rusting within 5 days so that the workpiece can be processed in the next procedure. The water-based cutting solution can not cause any adverse influence to the human body and the working environment in the operation process.
Description
Technical field
The invention belongs to cutting fluid technical field, relate to a kind of water-base cutting fluid and preparation method thereof.
Background technology
In mechanical processing industry, be use lubricating oil or use kerosene apply oil to carry out cutting lubrication and cooling substantially.In the course of processing, oil product waste is very serious, and causes very large injury to environment and operator; And be difficult to obtain desirable finished surface.And it is slow to add man-hour radiating rate, after processing work, very easily upper rust.
Present urgent need design oilness is good, and rustless property is superior, the cutting fluid that speed of cooling is fast, cleaning performance is good.
Summary of the invention
The object of this invention is to provide a kind of water-base cutting fluid and preparation method thereof.
The technical solution adopted in the present invention is:
A kind of water-base cutting fluid, is characterized in that being made up of the raw material of following weight part:
Urotropine 3-4, zinc dialkyl dithiophosphate 1-2, Sodium orthomolybdate 1-2, SODIUM PHOSPHATE, MONOBASIC 1-2, Polysorbate 80 2-3, sulfonated lignin 1-2, Union carbide A-162 2-3, film auxiliary agent 5-6, water 260.
Described film auxiliary agent is obtained by the raw material of following weight part: ricinolic acid 3-4,2-amino-2-methyl-1-propyl alcohol 2-3, Silane coupling agent KH550 1-2, sorbitol monooleate 1-2, vinyl cyanide 1-2, methylolurea 2-3, tertbutyl peroxide 0.2-0.3, morpholine 1-2.
Preparation method is: by ricinolic acid, 2-amino-2-methyl-1-propyl alcohol, vinyl cyanide, sorbitol monooleate mixing, add tertbutyl peroxide, stirring reaction 2-3 hour, be heated to 130-140 DEG C, add Silane coupling agent KH550, methylolurea, morpholine again, continue stirring reaction 1-2 hour and get final product.
The preparation method of described water-base cutting fluid, is characterized in that comprising the following steps:
Sodium orthomolybdate, SODIUM PHOSPHATE, MONOBASIC, Polysorbate 80, sulfonated lignin, Union carbide A-162 are added to the water, are heated to 80-90 DEG C, stir 60-80 minute, then add other remaining component, stir 40-60 minute and get final product.
The present invention's each raw material of filling a prescription all belongs to nontoxic; environmentally friendly; scientific formulation; there is oilness, cooling, cleaning, good antirust property, and there is rust removing function, protection cutter; extend cutting-tool's used life; processing work can not get rusty in 5 days, was conducive to workpiece and entered next procedure, can not cause any bad impact in operating process on human body and Working environment etc.
Embodiment
A kind of water-base cutting fluid, be made up of the raw material of following weight part (kilogram):
Urotropine 4, zinc dialkyl dithiophosphate 2, Sodium orthomolybdate 2, SODIUM PHOSPHATE, MONOBASIC 2, Polysorbate 80 3, sulfonated lignin 2, Union carbide A-162 3, film auxiliary agent 6, water 260.
Described film auxiliary agent is obtained by the raw material of following weight part (kilogram): ricinolic acid 4,2-amino-2-methyl-1-propyl alcohol 3, Silane coupling agent KH550 2, sorbitol monooleate 2, vinyl cyanide 2, methylolurea 2, tertbutyl peroxide 0.3, morpholine 1.
Preparation method is: by ricinolic acid, 2-amino-2-methyl-1-propyl alcohol, vinyl cyanide, sorbitol monooleate mixing, add tertbutyl peroxide, stirring reaction 2-3 hour, be heated to 130-140 DEG C, add Silane coupling agent KH550, methylolurea, morpholine again, continue stirring reaction 1-2 hour and get final product.
The preparation method of water-base cutting fluid, comprise the following steps: Sodium orthomolybdate, SODIUM PHOSPHATE, MONOBASIC, Polysorbate 80, sulfonated lignin, Union carbide A-162 are added to the water, are heated to 80-90 DEG C, stir 60-80 minute, then add other remaining component, stir 40-60 minute and get final product.
Utilize the present invention to carry out steel disc rust prevention test (55 ± 2 DEG C) entirely to soak: 30 with corrosion-free phenomenon of going up to the sky.
Claims (2)
1. a water-base cutting fluid, is characterized in that being made up of the raw material of following weight part:
Urotropine 3-4, zinc dialkyl dithiophosphate 1-2, Sodium orthomolybdate 1-2, SODIUM PHOSPHATE, MONOBASIC 1-2, Polysorbate 80 2-3, sulfonated lignin 1-2, Union carbide A-162 2-3, film auxiliary agent 5-6, water 260;
Described film auxiliary agent is obtained by the raw material of following weight part: ricinolic acid 3-4,2-amino-2-methyl-1-propyl alcohol 2-3, Silane coupling agent KH550 1-2, sorbitol monooleate 1-2, vinyl cyanide 1-2, methylolurea 2-3, tertbutyl peroxide 0.2-0.3, morpholine 1-2;
Preparation method is: by ricinolic acid, 2-amino-2-methyl-1-propyl alcohol, vinyl cyanide, sorbitol monooleate mixing, add tertbutyl peroxide, stirring reaction 2-3 hour, be heated to 130-140 DEG C, add Silane coupling agent KH550, methylolurea, morpholine again, continue stirring reaction 1-2 hour and get final product.
2. the preparation method of water-base cutting fluid according to claim 1, is characterized in that comprising the following steps:
Sodium orthomolybdate, SODIUM PHOSPHATE, MONOBASIC, Polysorbate 80, sulfonated lignin, Union carbide A-162 are added to the water, are heated to 80-90 DEG C, stir 60-80 minute, then add other remaining component, stir 40-60 minute and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310247512.3A CN103361153B (en) | 2013-06-21 | 2013-06-21 | Water-based cutting solution and method for preparing same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310247512.3A CN103361153B (en) | 2013-06-21 | 2013-06-21 | Water-based cutting solution and method for preparing same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103361153A CN103361153A (en) | 2013-10-23 |
| CN103361153B true CN103361153B (en) | 2015-03-18 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310247512.3A Active CN103361153B (en) | 2013-06-21 | 2013-06-21 | Water-based cutting solution and method for preparing same |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103361153B (en) |
-
2013
- 2013-06-21 CN CN201310247512.3A patent/CN103361153B/en active Active
Non-Patent Citations (3)
| Title |
|---|
| 丙烯腈毒性研究新进展;张正东等;《职业卫生与应急救援》;19970630;第15卷(第2期);79-82 * |
| 乌洛托品的毒性与污染防治;一民;《火炸药》;19811231(第1期);63-64 * |
| 硫酸锰和钼酸钠的毒性实验及文献复习;药理学教研室;《泰山医学院学报》;19851231(第2期);32-35 * |
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| Publication number | Publication date |
|---|---|
| CN103361153A (en) | 2013-10-23 |
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Address after: 210000 No. 73 Central North Road, Gulou District, Nanjing City, Jiangsu Province Patentee after: Duan Zhongda Address before: 312365 No. 90 North Bridge, Sanyou village, Shangyu District, Shaoxing, Zhejiang Patentee before: Duan Zhongda |
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Effective date of registration: 20181224 Address after: Room 1501, Haicang Commercial Building, No. 12 Zhonglin Road, Haicang Street, Haicang District, Xiamen City, Fujian Province Patentee after: Xiamen United States Petroleum Group Co., Ltd. Address before: 210000 No. 73 Central North Road, Gulou District, Nanjing City, Jiangsu Province Patentee before: Duan Zhongda |
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Denomination of invention: Water-based cutting fluid and its preparation method Effective date of registration: 20190325 Granted publication date: 20150318 Pledgee: Xiamen Haicang Financing Guarantee Co., Ltd. Pledgor: Xiamen United States Petroleum Group Co., Ltd. Registration number: 2019990000257 |
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Date of cancellation: 20220307 Granted publication date: 20150318 Pledgee: Xiamen Haicang Financing Guarantee Co.,Ltd. Pledgor: XIAMEN JAMA PETROLEUM GROUP CO.,LTD. Registration number: 2019990000257 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: The invention relates to a water-based cutting fluid and a preparation method thereof Effective date of registration: 20220308 Granted publication date: 20150318 Pledgee: Xiamen Haicang Financing Guarantee Co.,Ltd. Pledgor: XIAMEN JAMA PETROLEUM GROUP CO.,LTD. Registration number: Y2022110000052 |