CN103346288A - Preparation method of titanium dioxide thin-film electrode - Google Patents
Preparation method of titanium dioxide thin-film electrode Download PDFInfo
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- CN103346288A CN103346288A CN2013102260598A CN201310226059A CN103346288A CN 103346288 A CN103346288 A CN 103346288A CN 2013102260598 A CN2013102260598 A CN 2013102260598A CN 201310226059 A CN201310226059 A CN 201310226059A CN 103346288 A CN103346288 A CN 103346288A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
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Abstract
A provided preparation method of titanium dioxide thin-film electrode comprises: (1) adding a titanium dioxide powder and n-butanol into a container, grinding for 50-75 minutes, adding a binder and again grinding for 50-80 minutes; (2) adding an emulsifier, grinding for 20-40 minutes; (3)adding terpineol and methanol, mixing and again grinding for 30 minutes to form a slurry; (4) coating the slurry on the surface of electro-conductive glass, rubbing and leveling with soft cloth, drying for 1 hour at 60 DEG C, cooling to room temperature; and (5) immersing the electro-conductive glass coated with the slurry in alcohol for 10 minutes, taking out and drying to obtain the titanium dioxide thin-film electrode. Compared with the prior art, the titanium dioxide thin-film electrode obtained by using the preparation method is higher in density, and helpful for improving cell efficiency.
Description
Technical field
The present invention relates to a kind of preparation method, relate in particular to a kind of preparation method of titanium dioxide membrane electrode provided.
Background technology
Battery has been widely used on numerous occasions and the product, and wherein the efficient of battery is that people want the target that improves always.People have carried out effort from every side, and with the efficient of hope raising battery, for example from new material, new preparation process etc., the someone has adopted titanium deoxid film to be applied in the battery, however present titanium dioxide membrane electrode provided density deficiency, thus influence battery efficiency
Summary of the invention
The technical problem that the present invention mainly solves is present titanium dioxide membrane electrode provided density deficiency, thereby influences battery efficiency.
In order to solve the problems of the technologies described above, the embodiment of the invention discloses a kind of preparation method of titanium dioxide membrane electrode provided, may further comprise the steps:
(1), carbon dioxide powder and n-butanol are added in the container, ground 50-75 minute, the adding binding agent ground 50-80 minute again;
(2) add emulsifying agent, ground 20-40 minute;
(3) add terpinol and methyl alcohol, formed slurry after the mixing again in 30 minutes;
(4) slurry is coated in conductive glass surface, smooth with the soft cloth wiping, dried 1 hour, and be cooled to room temperature for 60 degrees centigrade;
(5) electro-conductive glass that will be coated with slurry enters in the alcohol 10 minutes, takes out the air-dry titanium dioxide membrane electrode provided that obtains.
In a preferred embodiment of the present invention, the milling time first time of step (1) is 63-68 minute, and milling time is 65-76 minute for the second time.
In a preferred embodiment of the present invention, the milling time of step (2) is 32-28 minute.
In a preferred embodiment of the present invention, the mass percent concentration of the alcohol of step (5) is 70%.
Compared to prior art, the titanium dioxide membrane electrode provided density that preparation method of the present invention obtains is higher, helps to improve the efficient of battery.
Embodiment
To the technical scheme in the embodiment of the invention be clearly and completely described below, obviously, described embodiment only is a part of embodiment of the present invention, rather than whole embodiment.Based on the embodiment among the present invention, those of ordinary skills belong to the scope of protection of the invention not making all other embodiment that obtain under the creative work prerequisite.
The embodiment of the invention discloses a kind of preparation method of titanium dioxide membrane electrode provided, may further comprise the steps:
(1), carbon dioxide powder and n-butanol are added in the container, ground 50-75 minute, the adding binding agent ground 50-80 minute again;
(2) add emulsifying agent, ground 20-40 minute;
(3) add terpinol and methyl alcohol, formed slurry after the mixing again in 30 minutes;
(4) slurry is coated in conductive glass surface, smooth with the soft cloth wiping, dried 1 hour, and be cooled to room temperature for 60 degrees centigrade;
(5) electro-conductive glass that will be coated with slurry enters in the alcohol 10 minutes, takes out the air-dry titanium dioxide membrane electrode provided that obtains.
In a preferred embodiment of the present invention, the milling time first time of step (1) is 63-68 minute, and milling time is 65-76 minute for the second time.
In a preferred embodiment of the present invention, the milling time of step (2) is 32-28 minute.
In a preferred embodiment of the present invention, the mass percent concentration of the alcohol of step (5) is 70%.
Compared to prior art, the titanium dioxide membrane electrode provided density that preparation method of the present invention obtains is higher, helps to improve the efficient of battery.
The above only is embodiments of the invention; be not so limit claim of the present invention; every equivalent structure or equivalent flow process conversion that utilizes description of the present invention to do; or directly or indirectly be used in other relevant technical field, all in like manner be included in the scope of patent protection of the present invention.
Claims (4)
1. the preparation method of a titanium dioxide membrane electrode provided is characterized in that, may further comprise the steps:
(1), carbon dioxide powder and n-butanol are added in the container, ground 50-75 minute, the adding binding agent ground 50-80 minute again;
(2) add emulsifying agent, ground 20-40 minute;
(3) add terpinol and methyl alcohol, formed slurry after the mixing again in 30 minutes;
(4) slurry is coated in conductive glass surface, smooth with the soft cloth wiping, dried 1 hour, and be cooled to room temperature for 60 degrees centigrade;
(5) electro-conductive glass that will be coated with slurry enters in the alcohol 10 minutes, takes out the air-dry titanium dioxide membrane electrode provided that obtains.
2. the preparation method of titanium dioxide membrane electrode provided according to claim 1 is characterized in that, the milling time first time of step (1) is 63-68 minute, and milling time is 65-76 minute for the second time.
3. the preparation method of titanium dioxide membrane electrode provided according to claim 1 is characterized in that, the milling time of step (2) is 32-28 minute.
4. the preparation method of titanium dioxide membrane electrode provided according to claim 1 is characterized in that, the mass percent concentration of the alcohol of step (5) is 70%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102260598A CN103346288A (en) | 2013-06-08 | 2013-06-08 | Preparation method of titanium dioxide thin-film electrode |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2013102260598A CN103346288A (en) | 2013-06-08 | 2013-06-08 | Preparation method of titanium dioxide thin-film electrode |
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| CN103346288A true CN103346288A (en) | 2013-10-09 |
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| CN2013102260598A Pending CN103346288A (en) | 2013-06-08 | 2013-06-08 | Preparation method of titanium dioxide thin-film electrode |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104129925A (en) * | 2014-08-06 | 2014-11-05 | 南京理工大学 | Disordered nano-porous film material and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003176130A (en) * | 2001-08-09 | 2003-06-24 | Masaharu Kaneko | METHOD OF FORMING TiO2 THIN FILM AND ELECTRODE FOR DYESTUFF SENSITIZING SOLAR CELL AND ELECTRODE FOR DYESTUFF SENSITIZING SOLAR CELL |
| CN101314523A (en) * | 2007-05-28 | 2008-12-03 | 比亚迪股份有限公司 | Titanium dioxide thin film and preparation thereof |
| CN102509623A (en) * | 2011-10-28 | 2012-06-20 | 奇瑞汽车股份有限公司 | Method for preparing photoanode coating of dye sensitized solar cell |
| CN102568844A (en) * | 2010-12-23 | 2012-07-11 | 海洋王照明科技股份有限公司 | Dye-sensitized n type doping titanium dioxide (TiO2) anode and method for producing same |
-
2013
- 2013-06-08 CN CN2013102260598A patent/CN103346288A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003176130A (en) * | 2001-08-09 | 2003-06-24 | Masaharu Kaneko | METHOD OF FORMING TiO2 THIN FILM AND ELECTRODE FOR DYESTUFF SENSITIZING SOLAR CELL AND ELECTRODE FOR DYESTUFF SENSITIZING SOLAR CELL |
| CN101314523A (en) * | 2007-05-28 | 2008-12-03 | 比亚迪股份有限公司 | Titanium dioxide thin film and preparation thereof |
| CN102568844A (en) * | 2010-12-23 | 2012-07-11 | 海洋王照明科技股份有限公司 | Dye-sensitized n type doping titanium dioxide (TiO2) anode and method for producing same |
| CN102509623A (en) * | 2011-10-28 | 2012-06-20 | 奇瑞汽车股份有限公司 | Method for preparing photoanode coating of dye sensitized solar cell |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104129925A (en) * | 2014-08-06 | 2014-11-05 | 南京理工大学 | Disordered nano-porous film material and preparation method thereof |
| CN104129925B (en) * | 2014-08-06 | 2016-03-02 | 南京理工大学 | A kind of unordered nano-porous film material and preparation method thereof |
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Owner name: ZHENG YULIN Free format text: FORMER OWNER: SUZHOU NUOXIN INNOVATION ENERGY CO., LTD. Effective date: 20140403 |
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Free format text: CORRECT: ADDRESS; FROM: 215121 SUZHOU, JIANGSU PROVINCE TO: 518052 SHENZHEN, GUANGDONG PROVINCE |
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Effective date of registration: 20140403 Address after: 518052 Guangdong city of Shenzhen province Nanshan District Nanshan digital and cultural industry base east tower room 407 Applicant after: Zheng Yulin Address before: 215121, No. 3, Jinling West Road, 288 Town, Suzhou Industrial Park, Jiangsu Province, 309 Applicant before: Suzhou Nuoxin Innovation Energy Co., Ltd. |
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Application publication date: 20131009 |