CN103331076A - A mass and heat transfer device combining an absorbing tower and a heat exchanger and a preparation method of the mass and heat transfer device - Google Patents

A mass and heat transfer device combining an absorbing tower and a heat exchanger and a preparation method of the mass and heat transfer device Download PDF

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Publication number
CN103331076A
CN103331076A CN201210276548XA CN201210276548A CN103331076A CN 103331076 A CN103331076 A CN 103331076A CN 201210276548X A CN201210276548X A CN 201210276548XA CN 201210276548 A CN201210276548 A CN 201210276548A CN 103331076 A CN103331076 A CN 103331076A
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tube
heat
heat exchanger
mass
transfer device
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CN103331076B (en
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赵新岭
赵俊芳
张丽楠
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ZHONG YUAN DAHUA GROUP Ltd OF HENAN PROVINCE
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ZHONG YUAN DAHUA GROUP Ltd OF HENAN PROVINCE
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Abstract

The invention relates to a mass and heat transfer device combining an absorbing tower and a heat exchanger and an operating method of the mass and heat transfer device, and belongs to the field of gas discharging technologies for chemical engineering, petrochemical engineering, environmental protection, medicine and the like. An upper shell cover is disposed on the top end of pipe bundle. The right side of the top end of the upper end shell cover is provided with a gas outlet. The top end of the upper end shell cover is provided with an absorbent inlet tube. A side of the upper end of the pipe bundle is provided with a cooling water inlet. A side of the lower end of the pipe bundle is provided with a cooling water outlet, and the other side of the lower end of the pipe bundle is provided with a water outlet. The bottom of the pipe bundle (7) is provided with a lower shell cover. A side of the lower shell cover is provided with a gas inlet. The lower end of the lower shell cover is provided with a liquid outlet. Five baffle plates with one-fourth gaps, and two pipe plates are disposed between an upper sieve plate and a lower sieve plate. A plurality of heat exchanging pipes, arranged in regular triangles, are disposed between the two pipe plates. The heat exchanging pipes are filled with packing having the diameter of 1.5mm-2.0mm.

Description

Mass-and heat-transfer device and preparation method that a kind of absorption tower and heat exchanger unite two into one
  
Technical field: the present invention relates to gas draining technologies such as chemical industry, petrochemical industry, environmental protection, medicine, mass-and heat-transfer device and method of work that especially a kind of absorption tower and heat exchanger unite two into one.
Background technology: in Chemical Manufacture, the recycling fully of a large amount of ammonia, caused a large amount of ammonia gas to be discharged in the atmosphere with emptying, ammonia is a kind of colourless toxic gas that the excitant foul odour is arranged, environment has been caused great pollution, also caused a large amount of wastes, economic loss is serious.Because factors such as design and structures, some tail gas absorbers do not play the effect of absorption, especially when summer temp is high.Because the ammonia gas in the tail gas will be emitted a large amount of heats when being absorbed, and heat can't be taken away in common absorption tower, make the temperature in the absorption tower continue to rise, when temperature rising solubility reduces, can't absorb fully at all.
Summary of the invention: the purpose of this invention is to provide mass-and heat-transfer device and method of work that a kind of absorption tower and heat exchanger unite two into one, it has overcome the shortcoming of original technology, the object of the present invention is achieved like this, it is by gas vent, the absorbent inlet tube, shower nozzle, sieve plate, cooling water inlet, deflection plate, tube bank, coolant outlet, low head, liquid outlet, gas feed, tube sheet, discharge outlet, heat exchanger tube, upper cover, flange, filler is formed by connecting, top in tube bank is installed with upper cover, there is gas vent in front, top at upper cover, and an absorbent inlet tube is installed on the upper cover top; Upper end one side in tube bank is provided with cooling water inlet, is provided with coolant outlet in lower end one side of restraining, and is provided with discharge outlet at the lower end opposite side of restraining; Bottom in tube bank 7 is installed with low head, and the side of low head is provided with gas feed, is provided with liquid outlet in the bottom of low head.
Bottom at the absorbent inlet tube is installed with shower nozzle, and at the absorbent inlet tube flange is installed; Shower nozzle is the corrosion resistant plate of arc, and with square arrangement, hole count is a plurality of.
A sieve plate is being fixed by the bottom of shower nozzle, and another piece sieve plate is being fixed by bottom in tube bank, and porose on two sieve plates, arrange with equilateral triangle in the hole.
Be installed with by two tube sheets, five deflection plates to be 1/4 breach, several heat exchanger tubes are installed that heat exchanger tube is arranged with equilateral triangle between two tube sheets in the centre of two sieve plates up and down; The filler of filling Φ 1.5mm-2.0mm in the heat exchanger tube.
During work, the present invention takes away heat by increasing heat-exchanging tube bundle, makes shower water can absorb ammonia in the tail gas fully.Tail gas is walked tube side from lower to upper by gas feed, and shower water is also walked tube side from top to down from shower nozzle, after the ammonia in the tail gas is absorbed by shower water in tube bank, is discharged by the bottom and to recycle residual exhaust emptying; For guarantee absorbing the heat that must take away generation fully, so recirculated water walks shell side, by the cooling water inlet coolant outlet water outlet of intaking, forms circulation.
Meaning of the present invention is: 1, reduced the temperature of this equipment, realized the absorption of device to ammonia in the tail gas, reduced the waste of ammonia, reduced production cost; 2, realized the multipurpose on similar absorption tower, multi-state uses.Realized the ammonia present situation of recycling fully in the Chemical Manufacture tail gas; 3, by increasing former tower height degree, tube bank and internals, realize different instructions for uses, can satisfy the production demand, atmospheric environment has also obtained very big improvement; 4, can better solve the gas plant ammonia with the irretrievable problem of exhaust emissions, for gas plant high load capacity long-term operation lays the first stone.
The structural representation of the mass-and heat-transfer device that description of drawings: Fig. 1 unites two into one for a kind of absorption tower and heat exchanger is among the figure 1, gas vent 2, absorbent inlet tube 3, shower nozzle 4, sieve plate 5, cooling water inlet 6, deflection plate 7, tube bank 8, coolant outlet 9, low head 10, liquid outlet 11, gas feed 12, tube sheet 13, discharge outlet 14, heat exchanger tube 15, upper cover 16, flange 17, filler
The specific embodiment: embodiment 1, the present invention are formed by connecting by gas vent 1, absorbent inlet tube 2, shower nozzle 3, sieve plate 4, cooling water inlet 5, deflection plate 6, tube bank 7, coolant outlet 8, low head 9, liquid outlet 10, gas feed 11, tube sheet 12, discharge outlet 13, heat exchanger tube 14, upper cover 15, flange 16, filler 17, top in tube bank 7 is installed with upper cover 15, there is gas vent 1 in front, top at upper cover 15, and an absorbent inlet tube 2 is installed on upper cover 15 tops; Upper end one side in tube bank 7 is provided with cooling water inlet 5, is provided with coolant outlet 8 in lower end one side of restraining 7, is provided with discharge outlet 13 at the lower end opposite side of restraining 7; Bottom in tube bank 7 is installed with low head 9, and the side of low head 9 is provided with gas feed 11, is provided with liquid outlet 10 in the bottom of low head 9.
Embodiment 2, in the bottom of absorbent inlet tube 2 shower nozzle 3 is installed, and at absorbent inlet tube 2 flange 16 is installed; Shower nozzle 3 is the corrosion resistant plate of arc, and with square arrangement, hole count is a plurality of.
A sieve plate 4 is being fixed by the bottom of embodiment 3, shower nozzle 3, and another piece sieve plate 4 is being fixed by 7 bottoms in tube bank, and porose on two sieve plates 4, arrange with equilateral triangle in the hole.
Embodiment 4, be installed with by two tube sheets 12, five deflection plates 6 to be 1/4 breach, several heat exchanger tubes 14 are installed that heat exchanger tube 14 is arranged with equilateral triangle between two tube sheets 12 in the centre of two sieve plates 4 up and down; The filler 17 of filling Φ 1.5mm-2.0mm in the heat exchanger tube 14.
Embodiment 5, method of work of the present invention are: take away heat by increasing heat-exchanging tube bundle 7, make shower water can absorb ammonia in the tail gas fully.Tail gas is walked tube side from lower to upper by gas feed 11, and shower water is also walked tube side from top to down from shower nozzle 3, after the ammonia in the tail gas is absorbed by shower water in tube bank 7, is discharged by the bottom and to recycle residual exhaust emptying; For guarantee absorbing the heat that must take away generation fully, so recirculated water walks shell side,, formed and circulates to coolant outlet 8 water outlets by cooling water inlet 5 water inlets.

Claims (5)

1. the mass-and heat-transfer device that unites two into one of an absorption tower and heat exchanger, it is by gas vent (1), absorbent inlet tube (2), shower nozzle (3), sieve plate (4), cooling water inlet (5), deflection plate (6), tube bank (7), coolant outlet (8), low head (9), liquid outlet (10), gas feed (11), tube sheet (12), discharge outlet (13), heat exchanger tube (14), upper cover (15), flange (16), filler (17) is formed by connecting, it is characterized in that: the top in tube bank (7) is installed with upper cover (15), in the front, top of upper cover (15) gas vent (1) is arranged, an absorbent inlet tube (2) is installed on upper cover (15) top; Upper end one side in tube bank (7) is provided with cooling water inlet (5), is provided with coolant outlet (8) in lower end one side of restraining (7), is provided with discharge outlet (13) at the lower end opposite side of restraining (7); Bottom in tube bank (7) is installed with low head (9), and the side of low head (9) is provided with gas feed (11), is provided with liquid outlet (10) in the bottom of low head (9).
2. the mass-and heat-transfer device that unites two into one of a kind of absorption tower according to claim 1 and heat exchanger is characterized in that: in the bottom of absorbent inlet tube (2) shower nozzle (3) is installed, and at absorbent inlet tube (2) flange (16) is installed; Shower nozzle (3) is the corrosion resistant plate of arc, and with square arrangement, hole count is a plurality of.
3. the mass-and heat-transfer device that unites two into one of a kind of absorption tower according to claim 1 and heat exchanger, it is characterized in that: a sieve plate (4) is being fixed by the bottom of shower nozzle (3), another piece sieve plate (4) is being fixed by (7) bottom in tube bank, upward porose at two sieve plates (4), arrange with equilateral triangle in the hole.
4. the mass-and heat-transfer device that unites two into one of a kind of absorption tower according to claim 1 and heat exchanger, it is characterized in that: being installed with by two tube sheets (12), five deflection plates (6) in the centre of two sieve plates (4) up and down is 1/4 breach, several heat exchanger tubes (14) are installed between two tube sheets (12), and heat exchanger tube (14) is arranged with equilateral triangle; The filler (17) of filling Φ 1.5mm-2.0mm in the heat exchanger tube (14).
5. the described a kind of absorption tower of claim 1 and the heat exchanger method of work of mass-and heat-transfer device that unites two into one is characterized in that: take away heat by increasing heat-exchanging tube bundle (7), make shower water can absorb ammonia in the tail gas fully; Tail gas is walked tube side from lower to upper by gas feed (11), and shower water is also walked tube side from top to down from shower nozzle (3), after the ammonia in the tail gas is absorbed by shower water in tube bank (7), is discharged by the bottom and to recycle residual exhaust emptying; For guarantee absorbing the heat that must take away generation fully, so recirculated water walks shell side,, formed and circulates to coolant outlet (8) water outlet by cooling water inlet (5) water inlet.
CN201210276548.XA 2012-08-06 2012-08-06 The mass-and heat-transfer device that a kind of absorption tower and heat exchanger unite two into one and preparation method Expired - Fee Related CN103331076B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108267043A (en) * 2018-03-06 2018-07-10 中大空调集团有限公司 A kind of central air-conditioning pipe for shell-and-tube exchanger journey water outlet side jettison gear
CN109200767A (en) * 2018-10-24 2019-01-15 东莞埃欧热能技术有限公司 A kind of ammonia absorption device
CN109554299A (en) * 2018-12-12 2019-04-02 大化集团有限责任公司 Carbonate the application method of tail gas and carbonating column cooling water heat in algae or Bacteria Culture

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101791510A (en) * 2010-04-14 2010-08-04 天津大学 Film-falling absorption tower
CN201899898U (en) * 2010-12-08 2011-07-20 湖北江钻天祥化工有限公司 Exhaust gas treatment device for synthesis of trichlorosilane
WO2011122525A1 (en) * 2010-03-31 2011-10-06 新日鉄エンジニアリング株式会社 Carbon dioxide gas recovery device
CN203030165U (en) * 2012-08-06 2013-07-03 河南省中原大化集团有限责任公司 Absorption tower and heat exchanger combined mass and heat transfer device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011122525A1 (en) * 2010-03-31 2011-10-06 新日鉄エンジニアリング株式会社 Carbon dioxide gas recovery device
CN101791510A (en) * 2010-04-14 2010-08-04 天津大学 Film-falling absorption tower
CN201899898U (en) * 2010-12-08 2011-07-20 湖北江钻天祥化工有限公司 Exhaust gas treatment device for synthesis of trichlorosilane
CN203030165U (en) * 2012-08-06 2013-07-03 河南省中原大化集团有限责任公司 Absorption tower and heat exchanger combined mass and heat transfer device

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108267043A (en) * 2018-03-06 2018-07-10 中大空调集团有限公司 A kind of central air-conditioning pipe for shell-and-tube exchanger journey water outlet side jettison gear
CN108267043B (en) * 2018-03-06 2023-09-19 中大空调集团有限公司 Tube side water outlet side water discharging device of shell-and-tube heat exchanger of central air conditioner
CN109200767A (en) * 2018-10-24 2019-01-15 东莞埃欧热能技术有限公司 A kind of ammonia absorption device
CN109200767B (en) * 2018-10-24 2024-06-11 东莞埃欧热能技术有限公司 Ammonia gas absorbing device
CN109554299A (en) * 2018-12-12 2019-04-02 大化集团有限责任公司 Carbonate the application method of tail gas and carbonating column cooling water heat in algae or Bacteria Culture

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