CN103330207A - DHA powder grease with soluble dietary fiber as wall materials and preparation method thereof - Google Patents
DHA powder grease with soluble dietary fiber as wall materials and preparation method thereof Download PDFInfo
- Publication number
- CN103330207A CN103330207A CN2013102871746A CN201310287174A CN103330207A CN 103330207 A CN103330207 A CN 103330207A CN 2013102871746 A CN2013102871746 A CN 2013102871746A CN 201310287174 A CN201310287174 A CN 201310287174A CN 103330207 A CN103330207 A CN 103330207A
- Authority
- CN
- China
- Prior art keywords
- dha
- dietary fiber
- wall material
- water
- soluble dietary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Abstract
The invention discloses a DHA powder grease product rich in dietary fiber. The DHA powder grease product is prepared by following steps: taking soluble rice bran dietary fiber and maltodextrin as wall materials; designing and optimizing a formula; subjecting DHA to double-phase emulsion process, high pressure homogenization, freeze-drying, and the like so as to microencapsulate DHA. The DHA powder grease product is widely used in milk powder, milk tea, solid beverage and other health food so as to increase the nutritional value of the products, improve the organizational structure, exterior quality and palatability of food, prolong shelf life of the products and improve the safety of powder grease products.
Description
Technical field
The present invention relates to a kind of is DHA powdered oil and the production method thereof of wall material with the soluble dietary fiber, belongs to the food additives field.
Background technology
Microcapsules technology is a kind ofly with filmogen solid or liquid to be carried out embedding, thereby the protection core is avoided adverse environmental factors such as influences such as temperature, pH value, to improve stability and the shelf life of encapsulation object, expands a kind of controlled-release technology of encapsulation object range of application.Utilize microcapsules technology that unrighted acid is coated, thereby improve the stability of grease, its nutritive value and local flavor are maximized the retention, have broad application prospects.
The selection of microcapsule wall material and proportioning are the keys that successfully prepares microcapsule product.Different wall materials is determining the physicochemical property of product to a great extent.The general principle of wall material of selecting is that the oiliness core material should adopt water-soluble coating material, and should have characteristics such as emulsifying capacity is strong, good film-forming property, and drying property is good, and solution viscosity is low.At present, the wall material of the microcapsule powder powder oil on the market mainly is based on casein.Yet because casein has potential safety issue, so the selection of novel microcapsule wall material becomes the focus of paying close attention in recent years with exploitation.
Dietary fiber is because of its special physiological properties, to reducing the important function that has of ciril disease.It is called " the 7th nutrient " by the nutritionist, be one of necessary nutritional labeling of human health.Studies show that soluble dietary fiber in the dietary fiber (SDF) more brings into play metabolic function, become a key factor that determines physiological function of diet fiber.Soluble dietary fiber can not only add the nutritive peculiarity of improving product in the varieties of food items such as bread, steamed bun, puffed sweet potato chips to as nutrition fortifier at present.Because it has certain emulsibility and film forming, also be used as thickener and stabilizing agent, add in the products such as beverage, jam.Application possibility that also makes it have microcapsule wall material.
For overcoming the caseic security flaw of conventional wall material, the present invention is main wall material with solubility rice bran dietary fiber and maltodextrin, adopt the emulsifying two phases method, high pressure homogenization technique, the design of processing and fill a prescription such as Freeze Drying Technique, the little gel parcel of DHA is prepared into the DHA powdered oil that is rich in dietary fiber, can be extensively with being applied to milk powder, milk tea, in solid beverage and other health foods, improve the nutritive value of product, improve the institutional framework of food, exterior quality and palatability, improve the shelf life of product, significant to improving the powdered oil security of products simultaneously.
Summary of the invention
It is main wall material with solubility rice bran dietary fiber and maltodextrin that the object of the invention provides a kind of, is rich in DHA powdered oil and the production method of dietary fiber.
Technical solution of the present invention:
Be the DHA powdered oil of wall material with the soluble dietary fiber, as follows with its each constituent content of butt weight percentage calculation:
Compound stabilizer is that 3: 1: 0.5 ratio mixes by sodium pyrophosphate, sodium hydrogen phosphate and sodium dihydrogen phosphate by weight.
The production method of above-mentioned DHA powdered oil (as shown in Figure 1) comprises following steps successively:
A. core oil phase preparation: take by weighing a certain amount of DHA and place Cooling or heating jar, 45-50 ℃ of insulation 35r/min stirs; Take by weighing a certain amount of methyl glycol fatty acid ester, lecithin adding by prescription then, continue insulated and stirred and be prepared into oil phase liquid;
B. wall material water preparation: by prescription take by weighing a certain amount of solubility rice bran dietary fiber, maltodextrin is wall material, Tween 80 and compound stabilizer, adds a certain proportion of water and places another Cooling or heating jar, 50-65 ℃ of insulation 35r/min stirs, and is prepared into water liquid;
C. emulsifying two phases: in water liquid, pump into oil phase liquid, add base-material 8-10 water doubly, and the total solids content of regulating mixed liquor is about 30% that the HLB value is 13.2,50-60 ℃ of insulated and stirred 20min;
D. high-pressure homogeneous: adopt valve formula high pressure homogenizer, homogeneous is 2 times under the pressure of 15-40MPa;
E. low temperature pre-freeze: the emulsion behind the homogeneous is through-80 ℃ of sharp freezing 12h;
F. freeze drying: material loads thickness 8mm, 15 ℃ of sublimation temperatures, 60 ℃ of resolution temperatures, dry 24h;
G. cryodesiccated material is sieved by the 40-80 order, namely obtain product.
The leading indicator of product of the present invention is:
The organoleptic indicator
Physical and chemical index
| Project | Index |
| Moisture (%) | ≤4.5％ |
| Fat content (%) | 30-35％ |
| Protein content (%) | ≥1.0 |
| Acid value (KOH) mg/g | ≤0.8 |
| Peroxide value g/100g | ≤0.1 |
| Total arsenic (in AS) mg/kg | ≤1.0 |
| Plumbous (in Pb) mg/kg | ≤0.5 |
| Copper (in Cu) mg/kg | ≤5.0 |
| Nickel (in Ni) mg/kg | ≤1.0 |
Microbiological indicator
| Project | Index |
| Total plate count cuf/g | ≤10000 |
| Coliform MPN/100g | ≤40 |
| Mould cfu/g | ≤50 |
| Pathogenic bacteria (salmonella, Shigella, staphylococcus aureus) | Must not detect |
Description of drawings
Fig. 1 is process chart of the present invention.
The specific embodiment
Embodiment 1:
A. oil phase liquid preparation: take by weighing 25kgDHA and place Cooling or heating jar, 45-50 ℃ of insulation 35r/min stirs; Take by weighing methyl glycol fatty acid ester 1.2kg, lecithin 0.15kg by prescription then, continue insulated and stirred and be prepared into oil phase liquid.
B. water liquid preparation: take by weighing solubility rice bran dietary fiber 12kg, maltodextrin 40kg, Tween 80 2.1kg and compound stabilizer 2kg, add the 600kg pure water and place another Cooling or heating jar, 50-65 ℃ of insulation 35r/min stirs, and is prepared into water liquid.
C. stirring and emulsifying: oil phase liquid is pumped in the water liquid, and adding water, to regulate the total solids content of mixed liquor be about 30% that the HLB value is 13.2,50-60 ℃ of insulated and stirred 20min.
D. high-pressure homogeneous: above-mentioned emulsion is through valve formula high pressure homogenizer 15-40MPa homogeneous 2 times.
E. low temperature pre-freeze: the emulsion behind the homogeneous is through-80 ℃ of sharp freezing 12h.
F. freeze drying: material loads thickness 8mm, 15 ℃ of sublimation temperatures, 60 ℃ of resolution temperatures, dry 24h.
G. cryodesiccated material is sieved by the 40-80 order, namely obtain product.
Embodiment 2:
A. oil phase liquid preparation: take by weighing 40kgDHA and place Cooling or heating jar, 45-50 ℃ of insulation 35r/min stirs; Take by weighing methyl glycol fatty acid ester 1.4kg, lecithin 0.2kg by prescription then, continue insulated and stirred and be prepared into oil phase liquid.
B. water liquid preparation: take by weighing solubility rice bran dietary fiber 17kg, maltodextrin 60kg, Tween 80 2.4kg and compound stabilizer 2kg, add the 800kg pure water and place another Cooling or heating jar, 50-65 ℃ of insulation 35r/min stirs, and is prepared into water liquid.
C. stirring and emulsifying: oil phase liquid is pumped in the water liquid, and adding water, to regulate the total solids content of mixed liquor be about 30% that the HLB value is 13.2,50-60 ℃ of insulated and stirred 20min.
D. high-pressure homogeneous: above-mentioned emulsion is through valve formula high pressure homogenizer 15-40MPa homogeneous 2 times.
E. low temperature pre-freeze: the emulsion behind the homogeneous is through-80 ℃ of sharp freezing 12h.
F. freeze drying: material loads thickness 8mm, 15 ℃ of sublimation temperatures, 60 ℃ of resolution temperatures, dry 24h.
G. cryodesiccated material is sieved by the 40-80 order, namely obtain product.
Claims (3)
1. one kind is the DHA powdered oil of wall material with the soluble dietary fiber, it is characterized in that: as follows with each constituent content of butt weight percentage calculation:
According to claim 1 a kind of be the DHA powdered oil of wall material with the soluble dietary fiber, it is characterized in that: described compound stabilizer is that 3: 1: 0.5 ratio mixes by sodium pyrophosphate, sodium hydrogen phosphate and sodium dihydrogen phosphate by weight.
3. one kind is the production method of the DHA powdered oil of wall material with the soluble dietary fiber, it is characterized in that: comprise following steps successively:
A. core oil phase preparation: take by weighing a certain amount of DHA and place Cooling or heating jar, 45-50 ℃ of insulation 35r/min stirs; Take by weighing a certain amount of methyl glycol fatty acid ester, lecithin adding by prescription then, continue insulated and stirred and be prepared into oil phase liquid;
B. wall material water preparation: by prescription take by weighing a certain amount of solubility rice bran dietary fiber, maltodextrin is wall material, Tween 80 and compound stabilizer, adds a certain proportion of water and places another Cooling or heating jar, 50-65 ℃ of insulation 35r/min stirs, and is prepared into water liquid;
C. emulsifying two phases: in water liquid, pump into oil phase liquid, add base-material 8-10 water doubly, and the total solids content of regulating mixed liquor is about 30% that the HLB value is 13.2,50-60 ℃ of insulated and stirred 20min;
D. high-pressure homogeneous: adopt valve formula high pressure homogenizer, homogeneous is 2 times under the pressure of 15-40MPa;
E. low temperature pre-freeze: the emulsion behind the homogeneous is through-80 ℃ of sharp freezing 12h;
F. freeze drying: material loads thickness 8mm, 15 ℃ of sublimation temperatures, 60 ℃ of resolution temperatures, dry 24h;
G. cryodesiccated material is sieved by the 40-80 order, namely obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102871746A CN103330207A (en) | 2013-07-10 | 2013-07-10 | DHA powder grease with soluble dietary fiber as wall materials and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102871746A CN103330207A (en) | 2013-07-10 | 2013-07-10 | DHA powder grease with soluble dietary fiber as wall materials and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103330207A true CN103330207A (en) | 2013-10-02 |
Family
ID=49238466
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013102871746A Pending CN103330207A (en) | 2013-07-10 | 2013-07-10 | DHA powder grease with soluble dietary fiber as wall materials and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103330207A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107668377A (en) * | 2017-10-10 | 2018-02-09 | 潜山县馨牧畜禽养殖专业合作社 | A kind of production method for the feed for preventing and treating laying hen fatty liver syndrome |
| CN108783460A (en) * | 2018-06-28 | 2018-11-13 | 广州富诺营养科技有限公司 | A kind of nutrient powder and preparation method thereof containing alpha-linolenic acid, lecithin, vitamin E, soluble dietary fiber element |
| CN109588687A (en) * | 2018-11-20 | 2019-04-09 | 阜阳九珍食品有限公司 | A kind of process preparing microcapsules powdered soy for carrier using okara powder |
| JP2021511813A (en) * | 2018-02-02 | 2021-05-13 | コモンウェルス サイエンティフィック アンド インダストリアル リサーチ オーガナイゼーション | Protection of bioactive substances and / or precursors thereof |
-
2013
- 2013-07-10 CN CN2013102871746A patent/CN103330207A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107668377A (en) * | 2017-10-10 | 2018-02-09 | 潜山县馨牧畜禽养殖专业合作社 | A kind of production method for the feed for preventing and treating laying hen fatty liver syndrome |
| JP2021511813A (en) * | 2018-02-02 | 2021-05-13 | コモンウェルス サイエンティフィック アンド インダストリアル リサーチ オーガナイゼーション | Protection of bioactive substances and / or precursors thereof |
| CN108783460A (en) * | 2018-06-28 | 2018-11-13 | 广州富诺营养科技有限公司 | A kind of nutrient powder and preparation method thereof containing alpha-linolenic acid, lecithin, vitamin E, soluble dietary fiber element |
| CN108783460B (en) * | 2018-06-28 | 2021-06-11 | 广州富诺营养科技有限公司 | Nutritional powder containing alpha-linolenic acid, lecithin, vitamin E and soluble dietary cellulose, and its preparation method |
| CN109588687A (en) * | 2018-11-20 | 2019-04-09 | 阜阳九珍食品有限公司 | A kind of process preparing microcapsules powdered soy for carrier using okara powder |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Radziejewska-Kubzdela et al. | Applicability of vacuum impregnation to modify physico-chemical, sensory and nutritive characteristics of plant origin products—a review | |
| Lucatto et al. | Performance of different microbial cultures in potentially probiotic and prebiotic yoghurts from cow and goat milks | |
| CN110742278B (en) | Vegetable protein system oil microcapsule powder and preparation method thereof | |
| Celli et al. | Degradation kinetics of anthocyanins in freeze-dried microencapsulates from lowbush blueberries (Vaccinium angustifolium Aiton) and prediction of shelf-life | |
| Ibrahim et al. | Date fruit: A review of the chemical and nutritional compounds, functional effects and food application in nutrition bars for athletes | |
| CN103330207A (en) | DHA powder grease with soluble dietary fiber as wall materials and preparation method thereof | |
| CN103027180A (en) | Potato ice cream | |
| CN104256595A (en) | Intacted protein enteral nutrition multi-polymerization agent | |
| CN102657340A (en) | Fresh conditioning duck breast meat product and production process thereof | |
| CN104687178A (en) | Solid beverage capable of being directly taken orally and preparation method thereof | |
| CN101611901A (en) | A kind of convenient soup blend and preparation method | |
| CN104938944A (en) | Nutritional noodles for children and production technology thereof | |
| CN108783437A (en) | A kind of the inflammatory bowel disease full nutrition formula food and its preparation process of predigestion | |
| CN102349673A (en) | Preparation method of purple potato drink | |
| CN102228084A (en) | Yoghurt powder, preparation methods thereof and method for preparing yoghurt by fermenting yoghurt powder | |
| CN101999683B (en) | Pure chicken powder and production process thereof | |
| CN103749790B (en) | Broccoli tea making method | |
| Khoshdouni Farahani et al. | The influence of sodium alginate and sodium alginate/WPI as coating material on microcapsules of Jujube extract produced by spray dryer | |
| CN105285651A (en) | Instant composite tremella solid beverage and preparation method thereof | |
| CN107258908A (en) | A kind of lyophilized fruits and vegetables probiotics cube and its processing method | |
| CN102771619A (en) | Double-protein cold drink product and production method thereof | |
| CN104000092A (en) | Instant vermicelli and preparation technology thereof | |
| CN103082035A (en) | Formula for preparing novel functional non-dairy creamer by taking rice fructose syrup and rice protein peptide as wall materials to micro-gelatinize and cover and production method thereof | |
| CN105454772B (en) | Alcohol component or malt extract granule and food and drink containing the same | |
| KR101481866B1 (en) | Method for manufacturing wonso-byung, and wonso-byung manufactured by the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20131002 |