CN103305928A - Heat treatment processing process for superfine denier imitated yarns - Google Patents

Heat treatment processing process for superfine denier imitated yarns Download PDF

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Publication number
CN103305928A
CN103305928A CN2012100574558A CN201210057455A CN103305928A CN 103305928 A CN103305928 A CN 103305928A CN 2012100574558 A CN2012100574558 A CN 2012100574558A CN 201210057455 A CN201210057455 A CN 201210057455A CN 103305928 A CN103305928 A CN 103305928A
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temperature
spinning
melt
yarns
district
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刘才洪
吴阿根
蒋云峰
周鑫
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Jiangsu Tiandi Chemical Fibre Co Ltd
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Jiangsu Tiandi Chemical Fibre Co Ltd
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Abstract

The invention discloses a heat treatment processing process for superfine denier imitated yarns. The superfine denier imitated yarns are produced according to a fully drawn yarn (FDY) chip spinning production line by the following steps of melting and extruding dry chips into melts by using a screw extruder, removing impurities from the melts by using a pre-filter, conveying the melts to each spinning position through a pipeline, quantitatively conveying the melts to each spinning component by using a metering pump at each spinning position, extruding and jetting the melts from spinneret holes of spinneret plates in the spinning components, sequentially performing cross air blowing cooling and solidification to form yarns, and performing bunching oiling, drafting sizing and mesh addition winding to form a spinning cake, wherein the screw extruder is divided into six areas, the temperature of the first area is set to be 270 to 276 DEG C, the temperature of the second area is 8 to 10 DEG C higher than that of the first area, and the temperature of each of the third to six areas is 1 to 3 DEG C higher than that of the previous area. According to the process, the problem of spinnability reduction caused by high end breaking rate and high fuzzing rate of the imitated yarns in a production process are maximally solved, the uniformity of pre-oriented yarns is improved, normal spinning is facilitated, and the full package rate is increased.

Description

A kind of heat-treatment processing process of super fine denier artificial real silk
Technical field
The invention belongs to textile technology field, the heat-treatment processing process of a kind of super super fine denier artificial real silk of specific design.
Background technology
The super fine denier artificial real silk is rapidly a kind of fibre in differentiation of development in recent years, as a kind of high-tech textile raw material in the synthetic fiber, at present at garment industry, obtained very large effect, it had both had the advantages such as the real silk moisture absorption is ventilative, comfortable and easy to wear, having overcome again the shortcomings such as silk fabric easily wrinkles, fastness is poor, is the product of high added value, high-tech, has wide market prospects and good economic benefit.The at present development of super fine polyester Silk rapidly, as a kind of high-tech product, Silk is when giving the excellent wearability of fabric, being faced with a lot of other synthetic fiber in post-production does not encounter problems yet, get each link processing in its process maximum to the performance impact of silk, heat treatment is exactly a wherein very important ring.
Although the super fine denier artificial real silk has brought good economic benefit and wide market prospects, its production difficulty increases than conventional silk, and wherein the selection of temperature control is particularly important.Silk requires melt flowability to get well in the spinning process, otherwise the buoyancy effect of melt can diminish, and is unfavorable for spinning moulding.
Summary of the invention
The super fine denier artificial real silk that proposes for background technology is high to the spinning temperature requirement in process of production, and temperature control precision is high, easily breaks end in the production, produces lousiness, and production difficulty strengthens, the problem of the rear processing characteristics of impact.The object of the present invention is to provide a kind of heat-treatment processing process of super fine denier artificial real silk.
Purpose of the present invention can be achieved through the following technical solutions:
A kind of heat-treatment processing process of super fine denier artificial real silk, it is that described super fine denier artificial real silk spins production line according to the FDY section and makes, do section and become melt through the screw extruder melt extruded, behind the impurity in the melt process prefilter removal melt, be transported to through piping and respectively spin the position, each spins the position and by measuring pump melt quantitative is delivered to each filament spinning component, melt is extruded the spray silk from the spinneret orifice of spinnerets in filament spinning component, then successively through encircling quenching, being frozen into strand, boundling oils, drafting forming, adds network and is wound into spinning cake again; Wherein screw extruder is divided into six districts, and the Temperature Setting in each district is: the first district is 270~276 ℃, and Second Region increases by 8~10 ℃ than the first district, and each district increases by 1~3 ℃ than last district temperature backward.
The heat-treatment processing process of above-mentioned super fine denier artificial real silk, it is in the drafting forming process, and the temperature of the first hot-rolling is 88~95 ℃, and the temperature of the second hot-rolling is 130~135 ℃, each hot-rolling to guarantee hot-rolling surface temperature uniformity, is heated evenly tow with incubator.
The heat-treatment processing process of above-mentioned super fine denier artificial real silk, it is melt in the process that piping is carried, and by the biphenyl insulation, the biphenyl temperature is controlled between 292~295 ℃, and the adding static mixer is even to guarantee melt temperature in pipeline.
The detailed technological process of production is: wet section → pulse conveying → pre-crystallizer → filling drying tower → screw extruder → prefilter → melt Conveying pipeline → spinning manifold → measuring pump → filament spinning component → ring quenching → oil nozzle oils → spinning shaft → pre-network → the first hot-rolling → second hot-rolling → master network → yarn break detector → coiling and molding → stripping silk → check classification → packing warehouse-in.
Adopt German Ba Mage screw extruder to prepare the PET melt.Improve spinning temperature on the basis that routine is spun, temperature increases by 2~5 ℃, reaches 290~295 ℃, so that fluidity of molten is good, and can avoid causing the polymer thermal degradation to strengthen the problem that causes spinnability to reduce because spinning temperature improves.
Spinning temperature is remained in the required scope, and it is crucial that each district of screw extruder sets out rational temperature, and screw extruder is divided into six districts, and every district temperature is all different, and first to the 6th district's temperature increases progressively.The temperature range in the first district is 270~276 ℃, and Second Region increases by 8~10 ℃ than the first district, and each district increases by 1~3 ℃ than last district temperature backward.To often make an inspection tour in the production process, guarantee that temperature does not have large fluctuation, the fluctuation be controlled at ± 0.5 ℃.
Adopted the down-mounting type manifold at spinning manifold, manifold is divided into dress formula manifold and down-mounting type manifold according to the mounting means of spinning pack at present.Upper dress formula manifold exists " stack effect " in process of production, and being looped around spinning pack ambient air absorption heat can get rid of from the top insulation, cause thermal loss, can make the assembly melt temperature inhomogeneous.And adopt the down-mounting type manifold to overcome the harmful effect that " stack effect " causes spinning.
By two pairs of hot-rollings, and set the purpose that the rational temperature of height reaches drafting forming, the first heat roller temperature is set as 88~95 ℃, the second heat roller temperature is higher than the first hot-rolling, and temperature is controlled at 130~135 ℃, and the hot-rolling surface is the temperature uniformity everywhere, thereby tow is heated evenly, each hot-rolling is opened during repiece with incubator, closes when normally moving.
The present invention is based on that the super fine denier artificial real silk is ultra-fine, the characteristics of porous, increases spinning temperature, improves 2~5 ℃ on the basis of normal conventional silk, improves melt rheological property, thereby improves spinnability.And the optimization heater improves the heating control mode of extruder, hot-rolling, improves the accuracy of heating, makes product satisfy the requirement of after-processing technology.The dyeing of Silk all reaches level Four with degree, meets national standard, and winding speed reaches 4800m/min, and production efficiency doubles.
The method that the present invention adopts extruder temperature and heating agent control temperature to combine when improving melt temperature, strengthen the sealed thermal insulating effect of each spinning zone, make spinnerets be in higher keeping warm mode, improve the uniformity of spun filament, be conducive to normal spinning, improve full-rolling rate.
This project is for solving the in process of production easy broken end of Silk, fluffing, and the problem that causes spinnability to reduce, and improve the temperature control of tow when drafting forming, improve heating uniformity and the dyeing uniformity of silk.Method of the present invention will improve the rear processing characteristics of super fine denier artificial real silk, so that the yields of finished silk improves.
Beneficial effect of the present invention:
Method of the present invention has been avoided easily breaking end in process of production of Silk to greatest extent, fluffing, and the problem that causes spinnability to reduce, the uniformity of raising spun filament is conducive to normal spinning, improves full-rolling rate.
The specific embodiment
Embodiment 1 produces 44dtex/144f super fine denier artificial real silk
Raw material: the PET polyester slice, chemical fibre Co., Ltd of Jiangsu DESAY produces, finish Huangma Chemical Group Co., Zhejiang produces: the HDG-2146 terylene FDY oil.
The detailed technological process of production is: wet section → pulse conveying → pre-crystallizer → filling drying tower → screw extruder → prefilter → melt Conveying pipeline → spinning manifold → measuring pump → filament spinning component → ring quenching → oil nozzle oils → spinning shaft → pre-network → the first hot-rolling → second hot-rolling → master network → yarn break detector → coiling and molding → stripping silk → check classification → packing warehouse-in.
Adopt German Ba Mage screw extruder, improve spinning temperature on the basis that routine is spun, temperature increases by 2~5 ℃, reaches 290~295 ℃, both so that fluidity of molten is good, and can avoid causing the polymer thermal degradation to strengthen the problem that causes spinnability to reduce because spinning temperature improves.
Set out and reasonably respectively distinguish temperature, screw extruder is divided into six districts, and every district temperature is all different, and first to the 6th district's temperature increases progressively, and controls well and respectively distinguishes temperature, and each is distinguished Temperature Setting and sees Table 1.To often make an inspection tour in the production process, guarantee that temperature does not have large fluctuation, the fluctuation be controlled at ± 0.5 ℃.
Melt is incubated by biphenyl in flow process, and the biphenyl temperature is controlled at 293 ℃, adds static mixer in pipeline, so that melt temperature is even.
Adopted the down-mounting type manifold at spinning manifold, manifold is divided into dress formula manifold and down-mounting type manifold according to the mounting means of spinning pack at present.Upper dress formula manifold exists " stack effect " in process of production, and being looped around spinning pack ambient air absorption heat can get rid of from the top insulation, cause thermal loss, can make the assembly melt temperature inhomogeneous.And adopt the down-mounting type manifold to overcome the harmful effect that " stack effect " causes spinning.
By two pairs of hot-rollings, and set the purpose that the rational temperature of height reaches drafting forming, the first heat roller temperature is set as between 92 ℃, the second heat roller temperature is higher than the first hot-rolling, and temperature is controlled at 132 ℃, and the hot-rolling surface is the temperature uniformity everywhere, thereby tow is heated evenly, each hot-rolling is opened during repiece with incubator, closes when normally moving.
Table 1 is produced the heating process parameter of 44dtex/144f super fine denier artificial real silk
Figure BDA0000141105600000031
Figure BDA0000141105600000041
Producing specification by this heating process is 44dtex/144f super fine denier artificial real silk, and production process is normal, and the lousiness broken end reduces 15 percentage points at original base, and spinnability significantly improves, excellence rate 〉=92%, and the physical index of gained silk is as follows:
Line density dtex 44
The line density deviation ratio 0.8
The fineness-unevenness rate 0.55
Fracture strength cN/dtex 3.8
The fracture strength irregularity 3.2
Elongation at break 24.9
The extension at break irregularity 8.1
Oil content 0.91
Boiling water shrinkage 6.7
Yarn unevenness 0.56
The network degree Individual/rice 27
Dye equal and property Level ≥4.0
Cylinder is heavy kg Fixed heavy

Claims (3)

1. the heat-treatment processing process of a super fine denier artificial real silk, it is characterized in that described super fine denier artificial real silk spins production line according to the FDY section and makes, do section and become melt through the screw extruder melt extruded, behind the impurity in the melt process prefilter removal melt, be transported to through piping and respectively spin the position, each spins the position and by measuring pump melt quantitative is delivered to each filament spinning component, melt is extruded the spray silk from the spinneret orifice of spinnerets in filament spinning component, then successively through encircling quenching, being frozen into strand, boundling oils, drafting forming, adds network and is wound into spinning cake again; Wherein screw extruder is divided into six districts, and the Temperature Setting in each district is: the first district is 270~276 ℃, and Second Region increases by 8~10 ℃ than the first district, and each district increases by 1~3 ℃ than last district temperature backward.
2. the heat-treatment processing process of super fine denier artificial real silk according to claim 1, it is characterized in that in the drafting forming process, the temperature of the first hot-rolling is 88~95 ℃, the temperature of the second hot-rolling is 130~135 ℃, each hot-rolling to guarantee hot-rolling surface temperature uniformity, is heated evenly tow with incubator.
3. the heat-treatment processing process of super fine denier artificial real silk according to claim 1, it is characterized in that melt is in the process that piping is carried, by the biphenyl insulation, the biphenyl temperature is controlled between 292~295 ℃, and the adding static mixer is even to guarantee melt temperature in pipeline.
CN2012100574558A 2012-03-06 2012-03-06 Heat treatment processing process for superfine denier imitated yarns Pending CN103305928A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104451916A (en) * 2014-12-01 2015-03-25 烟台华润锦纶有限公司 Production process for black nylon stretch yarns
CN105755568A (en) * 2015-11-19 2016-07-13 厦门翔鹭化纤股份有限公司 Alkali-dissolution polyester fibers and preparation method thereof
CN109112650A (en) * 2017-06-23 2019-01-01 江苏天地化纤有限公司 A kind of Silk heat-treatment processing process

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
杜荣江等: ""纺拉一步法(FDY)超细旦涤纶长丝的工艺探讨"", 《合成纤维》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104451916A (en) * 2014-12-01 2015-03-25 烟台华润锦纶有限公司 Production process for black nylon stretch yarns
CN105755568A (en) * 2015-11-19 2016-07-13 厦门翔鹭化纤股份有限公司 Alkali-dissolution polyester fibers and preparation method thereof
CN109112650A (en) * 2017-06-23 2019-01-01 江苏天地化纤有限公司 A kind of Silk heat-treatment processing process

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Application publication date: 20130918