CN103274687A - Preparation method of low-temperature co-firing ceramic material with high dielectric constant - Google Patents
Preparation method of low-temperature co-firing ceramic material with high dielectric constant Download PDFInfo
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- CN103274687A CN103274687A CN2013101719671A CN201310171967A CN103274687A CN 103274687 A CN103274687 A CN 103274687A CN 2013101719671 A CN2013101719671 A CN 2013101719671A CN 201310171967 A CN201310171967 A CN 201310171967A CN 103274687 A CN103274687 A CN 103274687A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 229910010293 ceramic material Inorganic materials 0.000 title claims abstract description 19
- 238000010344 co-firing Methods 0.000 title abstract 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims abstract description 86
- 239000000843 powder Substances 0.000 claims abstract description 76
- 239000011521 glass Substances 0.000 claims abstract description 38
- 238000000227 grinding Methods 0.000 claims abstract description 31
- 238000000498 ball milling Methods 0.000 claims abstract description 29
- 239000002243 precursor Substances 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000002245 particle Substances 0.000 claims abstract description 19
- 238000005245 sintering Methods 0.000 claims abstract description 19
- 239000000919 ceramic Substances 0.000 claims abstract description 15
- 238000010791 quenching Methods 0.000 claims abstract description 8
- 230000000171 quenching effect Effects 0.000 claims abstract description 8
- 238000007599 discharging Methods 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 30
- 238000009413 insulation Methods 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 23
- 239000002904 solvent Substances 0.000 claims description 21
- 239000008367 deionised water Substances 0.000 claims description 13
- 229910021641 deionized water Inorganic materials 0.000 claims description 13
- 239000007864 aqueous solution Substances 0.000 claims description 11
- 238000005469 granulation Methods 0.000 claims description 11
- 230000003179 granulation Effects 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 229920005596 polymer binder Polymers 0.000 claims description 11
- 239000002491 polymer binding agent Substances 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 8
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 8
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 claims description 8
- 239000011230 binding agent Substances 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 4
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 3
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 claims description 3
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 claims description 3
- 239000011812 mixed powder Substances 0.000 claims description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
- 229910052573 porcelain Inorganic materials 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 3
- 230000004927 fusion Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 230000005540 biological transmission Effects 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 3
- 239000003990 capacitor Substances 0.000 abstract 1
- 238000013329 compounding Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000005303 weighing Methods 0.000 description 15
- 229910010413 TiO 2 Inorganic materials 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 238000000748 compression moulding Methods 0.000 description 5
- 239000003989 dielectric material Substances 0.000 description 5
- 238000005498 polishing Methods 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 238000004891 communication Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910000906 Bronze Inorganic materials 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000010974 bronze Substances 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000011982 device technology Methods 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical group C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical class C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 1
- 230000005672 electromagnetic field Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000002241 glass-ceramic Substances 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000010532 solid phase synthesis reaction Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201310171967.1A CN103274687B (en) | 2013-04-23 | 2013-04-23 | Preparation method of low-temperature co-firing ceramic material with high dielectric constant |
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CN201310171967.1A CN103274687B (en) | 2013-04-23 | 2013-04-23 | Preparation method of low-temperature co-firing ceramic material with high dielectric constant |
Publications (2)
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CN103274687A true CN103274687A (en) | 2013-09-04 |
CN103274687B CN103274687B (en) | 2014-12-03 |
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CN201310171967.1A Active CN103274687B (en) | 2013-04-23 | 2013-04-23 | Preparation method of low-temperature co-firing ceramic material with high dielectric constant |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106505248A (en) * | 2016-10-26 | 2017-03-15 | 中国地质大学(武汉) | A kind of glass ceramics type method for preparing solid electrolyte |
CN109940752A (en) * | 2019-04-02 | 2019-06-28 | 东莞市琅菱机械有限公司 | A kind of electron ceramic material production system and technique |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6316376B1 (en) * | 2000-11-17 | 2001-11-13 | Kug Sun Hong | Dielectric ceramic compositions and method of preparation therefor |
CN1915904A (en) * | 2006-08-29 | 2007-02-21 | 中国科学院上海硅酸盐研究所 | Low temperature sintered composite microwave medium ceramic in series of lithium, niobium and titanium, and prepartion method |
CN1974479A (en) * | 2006-12-07 | 2007-06-06 | 华南理工大学 | Low temperature sintered high frequency heat stable dielectric ceramic and its prepn process |
CN101215159A (en) * | 2007-12-28 | 2008-07-09 | 天津大学 | Low-temperature sintering low-loss high frequency medium ceramic and preparing method thereof |
CN101613200A (en) * | 2009-07-21 | 2009-12-30 | 西安交通大学 | A kind of low-temperature sintered microwave dielectric ceramic material and preparation method thereof |
-
2013
- 2013-04-23 CN CN201310171967.1A patent/CN103274687B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6316376B1 (en) * | 2000-11-17 | 2001-11-13 | Kug Sun Hong | Dielectric ceramic compositions and method of preparation therefor |
CN1915904A (en) * | 2006-08-29 | 2007-02-21 | 中国科学院上海硅酸盐研究所 | Low temperature sintered composite microwave medium ceramic in series of lithium, niobium and titanium, and prepartion method |
CN1974479A (en) * | 2006-12-07 | 2007-06-06 | 华南理工大学 | Low temperature sintered high frequency heat stable dielectric ceramic and its prepn process |
CN101215159A (en) * | 2007-12-28 | 2008-07-09 | 天津大学 | Low-temperature sintering low-loss high frequency medium ceramic and preparing method thereof |
CN101613200A (en) * | 2009-07-21 | 2009-12-30 | 西安交通大学 | A kind of low-temperature sintered microwave dielectric ceramic material and preparation method thereof |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106505248A (en) * | 2016-10-26 | 2017-03-15 | 中国地质大学(武汉) | A kind of glass ceramics type method for preparing solid electrolyte |
CN109940752A (en) * | 2019-04-02 | 2019-06-28 | 东莞市琅菱机械有限公司 | A kind of electron ceramic material production system and technique |
CN109940752B (en) * | 2019-04-02 | 2024-04-19 | 东莞市琅菱机械有限公司 | Electronic ceramic material production system and process |
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CN103274687B (en) | 2014-12-03 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Preparation Method for High Dielectric Constant Low Temperature Co fired Ceramic Materials Effective date of registration: 20230421 Granted publication date: 20141203 Pledgee: Huaxia Bank Limited by Share Ltd. Kunming Chenggong Pledgor: YUNNAN INFINE NEO-MATERIAL Co.,Ltd. Registration number: Y2023530000024 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20141203 Pledgee: Huaxia Bank Limited by Share Ltd. Kunming Chenggong Pledgor: YUNNAN INFINE NEO-MATERIAL Co.,Ltd. Registration number: Y2023530000024 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method for high dielectric constant low-temperature co fired ceramic materials Granted publication date: 20141203 Pledgee: Bank of China Limited Kunming Xishan sub branch Pledgor: YUNNAN INFINE NEO-MATERIAL Co.,Ltd. Registration number: Y2024530000012 |