CN103263873A - Solubiliser composition and preparation method thereof - Google Patents
Solubiliser composition and preparation method thereof Download PDFInfo
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- CN103263873A CN103263873A CN2013101490446A CN201310149044A CN103263873A CN 103263873 A CN103263873 A CN 103263873A CN 2013101490446 A CN2013101490446 A CN 2013101490446A CN 201310149044 A CN201310149044 A CN 201310149044A CN 103263873 A CN103263873 A CN 103263873A
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Abstract
The invention discloses a solubiliser composition and a preparation method thereof. The solubiliser composition comprises, by weight, 1 part of a polyoxyethylene-polyoxypropylene segmented copolymer, 1 to 3 parts of sorbitol and 1 to 3 parts of water. The preparation method comprises the following steps of mixing sorbitol and water according to the above weight part ratio, dipping the polyoxyethylene-polyoxypropylene segmented copolymer into the mixed solution of sorbitol and water for at least 10min, and carrying out stirring to obtain a transparent liquid. The solubiliser composition obtained by the preparation method is colorless and odorless, can be dissolved water or ethanol easily, does not agglomerate or cake, can promote dissolution of a plurality of perfumes, essence and bactericides in water and has a wide application range.
Description
Technical field
The present invention relates to a kind of solubilizer, relate in particular to a kind of solubilizer composition and method of making the same.
Background technology
Polyox-yethylene-polyoxypropylene block copolymer, it is poloxamer, be that block copolymerization under condition is heated in catalysis makes by expoxy propane and oxirane, can be used as solubilizer, emulsifying agent, defoamer, dispersant and accelerant, be widely used in metal processing, cleaning, papermaking, fiber, oil and medical industry.
This block copolymer is pulverulent solids, water-soluble or ethanol, but the dissolution velocity in water or ethanol is extremely slow, the time that for example often needs to place more than 12 hours in water just can dissolve fully, and can not be in hot environment when placing, various condition restriction are brought great inconvenience with regard to the use of giving this solubilizer; In addition, after this polyox-yethylene-polyoxypropylene block copolymer dissolves in water or ethanol, tend to agglomerating or caking, also be difficult for its effect as solubilizer of performance.
Summary of the invention
Slow at existing solubilizer polyox-yethylene-polyoxypropylene block copolymer dissolution velocity in water or ethanol, and problem easy agglomerating or caking, the invention provides a kind of solubilizer composition that contains polyox-yethylene-polyoxypropylene block copolymer that has solved the problems referred to above.
In order to achieve the above object, the present invention has adopted following technical scheme:
A kind of solubilizer composition, this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1～3 part of sorbierite, 1～3 part in water.
Sorbierite and this ratio are combined in and all play crucial effects in the said composition, if sorbierite is changed into other alcohols such as glycerine, propane diols, ethanol, perhaps change the combination outside this ratio into, agglomerating, difficult dissolving that the solubilizer composition that obtains then can lump, make troubles to production, perhaps the solubilizer content molten weak effect that reduces.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1 part of sorbierite, 1 part in water.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 2 parts of sorbierites, 2 parts in water.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 3 parts of sorbierites, 3 parts in water.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1.5 parts of sorbierites, 1.5 parts in water.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 2.5 parts of sorbierites, 2.5 parts in water.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 3 parts of sorbierites, 1 part in water.
Preferably, the solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1 part of sorbierite, 3 parts in water.
The present invention discloses solubilizer preparation of compositions method, according to the quality share of each component as mentioned above, sorbierite is mixed with water, polyox-yethylene-polyoxypropylene block copolymer is soaked in the mixed solution of sorbierite and water, soak time at least 10 minutes stirs and forms transparence liquid.
Preferably, when polyox-yethylene-polyoxypropylene block copolymer was soaked in the mixed solution of sorbierite and water, temperature remained on normal temperature or 2～8 ° of C.
The composition that obtains after mixing according to each component of this quality share and this mixed method is liquid, colorless and odorless, and very easily water-soluble or ethanol can add water-pure system easily to or not have pure system, and can agglomerating or caking after dissolving; Simultaneously, this solubilizer composition has solubilization to spices and essences such as aromatic oil, Thymol, menthol, freshener and bactericide (as DP-300 triclosan, CPC Cetylpyridinium Chloride, PCMX parachlorometaxylenol, TCC triclocarban etc.), and these water-fast materials can be dissolved in the water after being added with this solubilizer composition preferably; Simultaneously, this solubilizer composition has been avoided grease smell, the astringent taste of other solubilizer such as tween, hydrogenation castor oil, can be widely used in oral cleaning nursing articles such as toothpaste, mouthwash, oral cavity fresh and cool spray, denfifrice, artificial tooth nursing cleaning agent, and products such as other cleaning agents, disinfectant, toner.
The invention discloses a kind of solubilizer composition and method of making the same, each component of mixing this ratio according to this preparation method, the said composition colorless and odorless that obtains, very easily be dissolved in water or ethanol, can be not agglomerating or caking, can promote the dissolvings in water such as multiple spices and essence and bactericide, the appropriate products scope is wide.
The specific embodiment
Below in conjunction with specific embodiment technical scheme of the present invention is done further explanation clearly and completely.
Embodiment one
Embodiment one discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1 part of sorbierite, 1 part in water.
Polyox-yethylene-polyoxypropylene block copolymer is soaked in the mixed solution of sorb alcohol and water, soak at room temperature is more than 10 minutes, make that polyox-yethylene-polyoxypropylene block copolymer is fully wetting, complete swelling, then stir fast, can form transparent solubilizer composition.
In other embodiments, when polyox-yethylene-polyoxypropylene block copolymer being soaked in the mixed solution of sorb alcohol and water, soaking temperature is controlled at normal temperature, or control is at 2～8 ℃.
Embodiment two
Embodiment two discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 2 parts of sorbierites, 2 parts in water.
The preparation method is with embodiment one.
Embodiment three
Embodiment three discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 3 parts of sorbierites, 3 parts in water.
The preparation method is with embodiment one.
Embodiment four
Embodiment four discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1.5 parts of sorbierites, 1.5 parts in water.
The preparation method is with embodiment one.
Embodiment five
Embodiment five discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 2.5 parts of sorbierites, 2.5 parts in water.
The preparation method is with embodiment one.
Embodiment six
Embodiment six discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 3 parts of sorbierites, 1 part in water.
The preparation method is with embodiment one.
Embodiment seven
Embodiment seven discloses a kind of solubilizer composition, and this solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1 part of sorbierite, 3 parts in water.
The preparation method is with embodiment one.
By above-described embodiment as can be known, solubilizer composition and method of making the same disclosed by the invention, each component of mixing this ratio according to this preparation method, the said composition colorless and odorless that obtains, very easily be dissolved in water or ethanol, can be not agglomerating or caking, can promote the dissolvings in water such as multiple spices and essence and bactericide, the appropriate products scope is wide.
It should be noted that above-described embodiment only is to the specifying of technical scheme of the present invention, and be not used in restriction the present invention, everyly the present invention is done being equal to of same design replace or conversion, all belong to protection scope of the present invention.
Claims (10)
1. solubilizer composition, it is characterized in that: described solubilizer composition comprises each component of following quality share: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1～3 part of sorbierite, 1～3 part in water.
2. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1 part of sorbierite, 1 part in water.
3. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 2 parts of sorbierites, 2 parts in water.
4. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 3 parts of sorbierites, 3 parts in water.
5. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1.5 parts of sorbierites, 1.5 parts in water.
6. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 2.5 parts of sorbierites, 2.5 parts in water.
7. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 3 parts of sorbierites, 1 part in water.
8. solubilizer composition as claimed in claim 1, it is characterized in that: described solubilizer composition comprises each component of following mass ratio: 1 part of polyox-yethylene-polyoxypropylene block copolymer, 1 part of sorbierite, 3 parts in water.
9. solubilizer preparation of compositions method, it is characterized in that: according to the quality share of each component as described in arbitrary as claim 1-8, sorbierite is mixed with water, polyox-yethylene-polyoxypropylene block copolymer is soaked in the mixed solution of sorbierite and water, soak time at least 10 minutes stirs and forms transparence liquid.
10. solubilizer preparation of compositions method as claimed in claim 9 is characterized in that: when described polyox-yethylene-polyoxypropylene block copolymer is soaked in the mixed solution of sorbierite and water, and temperature remains on normal temperature or 2～8 ° of C.
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| CN2013101490446A CN103263873A (en) | 2013-04-25 | 2013-04-25 | Solubiliser composition and preparation method thereof |
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| CN2013101490446A CN103263873A (en) | 2013-04-25 | 2013-04-25 | Solubiliser composition and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109730059A (en) * | 2019-01-22 | 2019-05-10 | 宁波翔神生化有限公司 | It is a kind of efficiently to wash shield bacteriostatic agent and preparation method thereof |
| CN111632021A (en) * | 2020-07-27 | 2020-09-08 | 浙江爱尚日用品有限公司 | Probiotics toothpaste for preventing gingival atrophy |
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| CN1050499A (en) * | 1989-09-25 | 1991-04-10 | 新时代株式会社 | Dentifrice composition |
| WO1999051716A1 (en) * | 1998-04-03 | 1999-10-14 | Unilever Plc | Detergent compositions |
| CN101190182A (en) * | 2006-12-01 | 2008-06-04 | 北京大学 | Self-emulsifying composition |
| CN101906295A (en) * | 2010-04-21 | 2010-12-08 | 四川海盾石油新技术开发有限公司 | Water-soluble thick oil viscosity reducer |
| CN102670435A (en) * | 2012-01-04 | 2012-09-19 | 河南科技大学 | Degreasing liquid soap and preparation method thereof |
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2013
- 2013-04-25 CN CN2013101490446A patent/CN103263873A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1050499A (en) * | 1989-09-25 | 1991-04-10 | 新时代株式会社 | Dentifrice composition |
| US5035880A (en) * | 1989-09-25 | 1991-07-30 | Sunstar Kabushiki Kaisha | Dentifrice composition |
| WO1999051716A1 (en) * | 1998-04-03 | 1999-10-14 | Unilever Plc | Detergent compositions |
| CN101190182A (en) * | 2006-12-01 | 2008-06-04 | 北京大学 | Self-emulsifying composition |
| CN101906295A (en) * | 2010-04-21 | 2010-12-08 | 四川海盾石油新技术开发有限公司 | Water-soluble thick oil viscosity reducer |
| CN102670435A (en) * | 2012-01-04 | 2012-09-19 | 河南科技大学 | Degreasing liquid soap and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109730059A (en) * | 2019-01-22 | 2019-05-10 | 宁波翔神生化有限公司 | It is a kind of efficiently to wash shield bacteriostatic agent and preparation method thereof |
| CN111632021A (en) * | 2020-07-27 | 2020-09-08 | 浙江爱尚日用品有限公司 | Probiotics toothpaste for preventing gingival atrophy |
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Application publication date: 20130828 |