CN103250845B - Inflammation relieving herbal tea buccal tablet and preparation method thereof - Google Patents
Inflammation relieving herbal tea buccal tablet and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the technical field of tea products, in particular to an inflammation relieving herbal tea buccal tablet and a preparation method thereof. The inflammation relieving herbal tea buccal tablet is characterized by comprising the following compound raw materials: 10-13 parts of fructus arctii, 24-28 parts of radix scrophulariae, 24-30 parts of cassia seeds, 24-28 parts of fructus cannabis, 3-5 parts of green tea and 0-5 parts of mint. The preparation method of the tablet comprises the steps of compound raw material smashing, extraction, purification, concentration, compounding, boiled granulation, dryness, screening and tabletting. According to the buccal tablet and the method, the processing techniques of the traditional herb tea and the buccal tablet are combined, the operation is simple, the control is easy, and the buccal tablet has broad-spectrum sterilization, lung heat clearing, heat clearing and toxicity removing functions, and has a better effect on preventing halitosis.
Description
Technical field
The present invention relates to health food technology field, particularly a kind of cool tea buccal tablets and method for making thereof of relieving inflammation or internal heat.
Background technology
Cold tea is mainly decocted by the cold and cool Chinese herbal medicine of the property of medicine that water constituent forms, the effects such as having dries promotes the production of body fluid, relieve inflammation or internal heat, improving eyesight, dissipating bind, detumescence, also can be used for controlling hot eyes headache, dizziness and tinnitus, furuncle swelling toxin and hypertension etc., especially can be clearing heat and detoxicating, be the first-selection of cold drink in summer.
Modern pharmacology research shows, Coumarins, saponins etc. are to inhibited apoptosis, reduce the activity of lipids contents and some metabolic enzymes, strengthen scheming shrinkage factor, increase CF etc., and organic acid (Chlorogenic acid), polyphenol and flavonoids have broad-spectrum sterilization effectiveness, in some Chinese herbal medicines of the existence that these compositions are all extensively sent out.
Buccal tablet is to be contained in oral cavity, the compressed tablets that can slowly dissolve under the effect of saliva, its advantage is that the time of functional component is controlled and the persistence of site of action (being mainly oral cavity and pharynx), use and carry convenient etc.Due to its special using method and manufacture craft; mouthfeel and stability are the problems that buccal tablet exploitation must be captured; the collocation of the composition and engineering attribute that relates generally to functional component and auxiliary material to buccal tablet stripping mouthfeel, auxiliary material is to the protection of main component in buccal tablet with containing the maintenance of tablet quality.
Along with social progress, it is particularly important that interpersonal communication exchange seems, and the halitosis causing due to lung heat and oral cavity germ etc. will directly reduce the quality of communication, therefore need to slow down halitosis phenomenon containing taking buccal tablet.On market, buccal tablet mainly belongs to medicine or bread and cheese candy class now, has some defects.As the buccal tablet of medicine, generally comparatively lay particular stress on drug effect and mouthfeel is poor, even there will be some side effects; Lozenge as candy class is too focused on mouthfeel and outward appearance.
Therefore, it is good that a kind of mouthfeel is badly in need of in health food technology field, has a kind of cool tea buccal tablets and method for making thereof of relieving inflammation or internal heat of relieving inflammation or internal heat, preventing and alleviating halitosis effect.
Summary of the invention
The invention provides a kind of cool tea buccal tablets and method for making thereof of relieving inflammation or internal heat, technical scheme is as follows:
The cool tea buccal tablets that relieves inflammation or internal heat, is characterized in that, by following compound raw material, is made:
Great burdock achene, radix scrophulariae, cassia seed, fructus cannabis, green tea, peppermint, formulated according to 10-13 part, 24-28 part, 24-30 part, 24-28 part, 3-5 part, 0-5 part quality proportioning.
The cool tea buccal tablets method for making of relieving inflammation or internal heat, is characterized in that, comprises the steps: the pulverizing of compound raw material, extraction, purifying, concentrated, composite, fluidized granulating dry, screening, compressing tablet.
A kind of cool tea buccal tablets method for making of relieving inflammation or internal heat as mentioned above, wherein, in described composite step: one or more of xylitol and sweet mellow wine, Aspartame and citric acid and sodium carboxymethylcellulose, according to being respectively 30-60% with the mass volume ratio of concentrated solution, 8-15%, 10-15% is formulated.
The cool tea buccal tablets method for making of relieving inflammation or internal heat as mentioned above, wherein, in described extraction step: distilled water and ethanol and ethyl acetate mixed liquor, formulated according to 60-70 part, 30-40 part quality proportioning.
The cool tea buccal tablets method for making of relieving inflammation or internal heat as mentioned above, wherein, described screening step is: cross the screening of 30-40 eye mesh screen.
Advantage of the present invention: the effect of three kinds of compound raw materials is complemented each other, contains water soluble ingredient and micro-liposoluble constituent, thereby is kept original local flavor of cold tea.The present invention combines traditional cold tea with the processing technology of buccal tablet, simple to operate, is easy to control, and has broad-spectrum sterilization, removes lung heat and clearing heat and detoxicating effect, for pre-anti-halitosis, has a good effect.
The specific embodiment
For technological means, creation characteristic that the present invention is realized, reach object and effect is easy to understand, below further set forth the present invention.
A kind of cool tea buccal tablets that relieves inflammation or internal heat of the present invention, comprises three kinds of compound raw materials: radix glehniae, the tuber of dwarf lilyturf, radix polygonati officinalis, Radix Glycyrrhizae, green tea, peppermint, and formulated according to 10-20 part, 20-40 part 15-20 part, 20-25 part, 5-10 part, 0-5 part quality proportioning;
Chinese olive, balloonflower root, honeysuckle, mulberry leaf, peppermint, green tea, formulated according to 30-35 part, 15-18 part, 16-20 part, 12-18 part, 5-8 part, 1-3 part quality proportioning;
Great burdock achene, radix scrophulariae, cassia seed, fructus cannabis, green tea, peppermint, formulated according to 10-13 part, 24-28 part, 24-30 part, 24-28 part, 3-5 part, 0-5 part quality proportioning.
The method for making of a kind of cool tea buccal tablets that relieves inflammation or internal heat of the present invention, comprises following steps:
Step 1: adopt superfine communication technique that compound raw meal is broken to 100-200 order.
Step 2: first, feed particles and extractant that step 1 is pulverized are infiltrated in extractant with the mass ratio of 3-6 part according to 1 part, at temperature 45-70 ℃, extract 15-20 minute under the condition of microwave power 300W, repeat this process 1-2 time; Then add edible ethanol in the mixed extract obtaining, when alcoholic strength reaches 80-90 and spends, normal temperature is cooling, stirs 1h.
Extractant is formulated according to 60-70 part and 30-40 part mass ratio by distilled water and ethanol and ethyl acetate mixed liquor, and the mixed liquor of ethanol and ethyl acetate is formulated according to 85-100 part and 0-15 part mass ratio.
Step 3: the mixed extract being obtained with 2000-6000 rev/min of centrifugation step 2, centrifugal 15 minutes, collect centrifugate.
Step 4: the centrifugate of obtaining in step 3 is carried out to Vacuum Concentration, at vacuum 0.01MPa, at temperature 40-50 ℃, according to fraction collection speed, reclaim ethanol, until ethanol evaporation is complete, till solution pol is 5-20brix.
Step 5: take xylitol as filler, one or more of sweet mellow wine, Aspartame and citric acid are flavouring, and sodium carboxymethylcellulose is disintegrant, is dissolved in by the concentrated solution obtaining of step 4.Filler, the addition of flavouring and disintegrant and the mass volume ratio of concentrated solution are respectively 30-60%, 8-15%, 10-15%.
Step 6: by composite the obtained mixed solution input boiling granulating drying equipment of step 5, carry out drying and granulating.
Step 7: the granulation product that step 6 is obtained is crossed 30-40 eye mesh screen, what screening obtained is compressing tablet softwood.
Step 8: compressing tablet softwood is mixed with adhesive, dolomol, and compressing tablet obtains lozenge.
Embodiment 1
Get 15 parts of radix glehniaes, 35 parts of the tubers of dwarf lilyturf, 18 parts of radix polygonati officinalis, 23 parts, Radix Glycyrrhizae, 9 parts of roasted green teas.
First, by compound raw material ultramicro grinding, cross 100 eye mesh screens; 95 parts of ethanol and 5 parts of ethyl acetate are mixed with mixed solution, and 30 parts of ethanol and ethyl acetate mixed liquor are poured in 70 parts of distilled water and be mixed with extractant.According to the mass ratio of pulverized particles and extractant, be that 1:5 is mixed with solution, 55 ℃ of temperature, under the condition of microwave power 300W, extract 15 minutes, repeat once this leaching process.Then, ethanol is added in this extract, until alcoholic strength reaches 90 degree, stir alcohol precipitation, and with 3000rpm, carry out centrifugally, the centrifugate obtaining being concentrated at 45 ℃ to pol is 12brix, 30% xylitol is dissolved in stirring, 10% sweet mellow wine and 12% sodium carboxymethylcellulose.Finally, in mixed liquor input fluidized drying facility for granulating after this is composite, at EAT, be 170 ℃, leaving air temp is 110 ℃, under the condition that flow velocity is 0.6L/min, granulates, the particle making is crossed 40 mesh sieves, screening obtains compressing tablet softwood, adds the dolomol that accounts for compressing tablet softwood 1% as lubricant, adjusts angle of repose, carry out compressing tablet, obtain lozenge.
Embodiment 2
Get 35 parts of Chinese olives, 16 parts of balloonflower roots, 18 parts of honeysuckles, 15 parts, mulberry leaf, 7 parts of peppermints, 9 parts of roasted green teas.
First, by compound raw material ultramicro grinding, cross 100 eye mesh screens; 92.5 parts of ethanol and 7.5 parts of ethyl acetate are mixed with mixed solution, and 30 parts of ethanol and ethyl acetate mixed liquor are poured in 70 parts of distilled water and be mixed with extractant.According to the mass ratio of pulverized particles and extractant, be that 1:6 is mixed with solution, at temperature 50 C, under the condition of microwave power 300W, extract 20 minutes, repeat once this leaching process.Then, ethanol is added in this extract, until alcoholic strength reaches 90 degree, stir alcohol precipitation, and with 3000rpm, carry out centrifugally, the centrifugate obtaining being concentrated at 45 ℃ to pol is 10brix, stirs the xylitol that dissolves in 35%, 10% sweet mellow wine and 8% citric acid, 12% sodium carboxymethylcellulose.Finally, in mixed liquor input fluidized drying facility for granulating after this is composite, at EAT, be 170 ℃, leaving air temp is 110 ℃, under the condition that flow velocity is 0.6L/min, granulates, the particle making is crossed 40 mesh sieves, screening obtains compressing tablet softwood, adds the dolomol that accounts for compressing tablet softwood 1% as lubricant, adjusts angle of repose, carry out compressing tablet, obtain lozenge.
Embodiment 3
12 parts of great burdock achenes, 25 parts of radix scrophulariaes, 27 parts of cassia seeds, 25 parts of fructus cannabis, 7 parts of peppermints, 9 parts of roasted green teas.
First, by compound raw material ultramicro grinding, cross 100 eye mesh screens; 100 parts of ethanol and 15 parts of ethyl acetate are mixed with mixed solution, and 35 parts of ethanol and ethyl acetate mixed liquor are poured in 65 parts of distilled water and be mixed with extractant.According to the mass ratio of pulverized particles and extractant, be that 1:6 is mixed with solution, at temperature 50 C, under the condition of microwave power 300W, extract 20 minutes, repeat once this leaching process.Then, ethanol is added in this extract, until alcoholic strength reaches 90 degree, stir alcohol precipitation, and with 3000rpm, carry out centrifugally, the centrifugate obtaining being concentrated at 45 ℃ to pol is 12brix, stirs the xylitol that dissolves in 45%, 10% sweet mellow wine and 3.5% citric acid, 10% sodium carboxymethylcellulose.Finally, in mixed liquor input fluidized drying facility for granulating after this is composite, at EAT, be 170 ℃, leaving air temp is 110 ℃, under the condition that flow velocity is 0.6L/min, granulates, the particle making is crossed 40 mesh sieves, screening obtains compressing tablet softwood, adds the dolomol that accounts for compressing tablet softwood 1% as lubricant, adjusts angle of repose, carry out compressing tablet, obtain lozenge.
More than show and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (1)
1. the method for making of the cool tea buccal tablets that relieves inflammation or internal heat, it is characterized in that, by great burdock achene, radix scrophulariae, cassia seed, fructus cannabis, green tea, peppermint, formulated according to 10-13 part, 24-28 part, 24-30 part, 24-28 part, 3-5 part, 0-5 part quality proportioning, comprise following steps:
Step 1, pulverizes: adopt superfine communication technique that described compound raw meal is broken to 100-200 order;
Step 2, extracts: feed particles and extractant that step 1 is pulverized are infiltrated in extractant with the mass ratio of 3-6 part according to 1 part, at temperature 45-70 ℃, under the condition of microwave power 300W, extract 15-20 minute, repeat this process 1-2 time; Then add edible ethanol in the mixed extract obtaining, when alcoholic strength reaches 80-90 and spends, normal temperature is cooling, stirs 1 hour;
This extractant is by 35 parts of ethanol and ethyl acetate mixed liquor, to be poured in 65 parts of distilled water formulatedly, and the mixed liquor of ethanol and ethyl acetate is formulated according to 100 parts of ethanol and 15 parts of ethyl acetate mass ratios;
Step 3, purifying: the extract being obtained with 2000-6000 rev/min of centrifugation step 2, centrifugal 15 minutes, collect centrifugate;
Step 4, concentrated: the centrifugate of obtaining in step 3 to be carried out to Vacuum Concentration, at vacuum 0.01MPa, at temperature 40-50 ℃, according to fraction collection speed, reclaim ethanol, until ethanol evaporation is complete, till solution pol is 5-20brix;
Step 5, composite: take xylitol as filler, one or more of sweet mellow wine, Aspartame and citric acid are flavouring, and sodium carboxymethylcellulose is disintegrant, be dissolved in by the concentrated solution obtaining of step 4; The addition of filler, flavouring and disintegrant and the mass volume ratio of concentrated solution are respectively 30-60%, 8-15%, 10-15%;
Step 6, fluidized granulating is dry: by composite the obtained mixed solution input boiling granulating drying equipment of step 5, carry out drying and granulating;
Step 7, screening: the granulation product that step 6 is obtained is crossed 30-40 eye mesh screen, what screening obtained is compressing tablet softwood; Step 8, compressing tablet: compressing tablet softwood is mixed with adhesive, dolomol, and compressing tablet obtains lozenge.
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