CN103232152A - Production process of microcrystalline glass curved plate - Google Patents

Production process of microcrystalline glass curved plate Download PDF

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Publication number
CN103232152A
CN103232152A CN2013101513170A CN201310151317A CN103232152A CN 103232152 A CN103232152 A CN 103232152A CN 2013101513170 A CN2013101513170 A CN 2013101513170A CN 201310151317 A CN201310151317 A CN 201310151317A CN 103232152 A CN103232152 A CN 103232152A
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CN
China
Prior art keywords
hot bending
microcrystalline glass
sheet material
crystallization
crystallizing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101513170A
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Chinese (zh)
Inventor
秦小平
秦刚
姜小元
王刚琳
石章辉
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SICHUAN YIMING MICROCRYSTALLINE TECHNOLOGY Co Ltd
Original Assignee
SICHUAN YIMING MICROCRYSTALLINE TECHNOLOGY Co Ltd
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Application filed by SICHUAN YIMING MICROCRYSTALLINE TECHNOLOGY Co Ltd filed Critical SICHUAN YIMING MICROCRYSTALLINE TECHNOLOGY Co Ltd
Priority to CN2013101513170A priority Critical patent/CN103232152A/en
Publication of CN103232152A publication Critical patent/CN103232152A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

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  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
  • Glass Compositions (AREA)

Abstract

The invention discloses a production process of a microcrystalline glass curved plate. The production process comprises the steps of burdening, melting, rolling and annealing to obtain a microcrystalline glass plate, firstly carrying out hot bending treatment on the first microcrystalline glass plate and then crystallizing the microcrystalline glass plate, cooling and polishing after crystallizing. The hot bending treatment comprises the step of placing the microcrystalline glass plate in a hot bending kiln for raising the temperature to 760-850 DEG C and insulating for 2-4h. The crystallizing comprises the step of rapidly raising the temperature to 880-950 DEG C after the hot bending is completed and insulating-crystallizing the microcrystalline glass plate. According to the production process of carrying out hot bending on the microcrystalline glass curved plate and then crystallizing, the microcrystalline glass plate is only subjected to temperature raising treatment, a two-step method of cooling after the microcrystalline glass plate is crystallized at a high temperature and raising the temperature again for carrying out hot bending treatment is saved, thus energy consumption of 50 percent is saved, the production time of the microcrystalline glass curved plate is shortened, and the working efficiency is increased; and because the temperature for hot-bending of the un-crystallized plate is lower, fracture or cracks of the microcrystalline glass plate during hot bending can be reduced, and the quality and the yield are increased.

Description

The production technique of CURVE DECORATIVE SHEET OF CERAMIC GLASS
Technical field
The present invention relates to a kind of production technique of building and ornament materials, be specifically related to a kind of production technique of CURVE DECORATIVE SHEET OF CERAMIC GLASS.
Background technology
Crystallizing glass sheet material belongs to new decorative material for building, and its performance is better than building and ornament materials such as marble, granite, is described as " the green building material of 21st century ".And microcrystalline glass decorative plate is easy to by hot bending process for producing arc sheet material, is used for decorating the cylindric buildings of various different sizes.
The production technique of tradition devitrified glass is mainly rolling process and sintering process, patent name is to utilize granite waste to produce the method for the devitrified glass building decorative plates (patent No.: ZL200910216248.0) adopt the all-electric melting calendering technology to produce crystallizing glass sheet material, all adopt hot bending production technique after the first crystallization when producing the crystallite arc then.Need when producing with this technology sheet material is carried out twice thermal treatment, energy consumption is higher, and production efficiency is lower, therefore the CURVE DECORATIVE SHEET OF CERAMIC GLASS production technique is improved very important.
Find in the production process of research CURVE DECORATIVE SHEET OF CERAMIC GLASS: the sheet material of non-crystallized sheet material softening temperature after than crystallization is low, softening temperature also is lower than crystallization temperature simultaneously, therefore adopt first hot bending, the production technique of crystallization then, only need sheet material is carried out a hyperthermic treatment, just can reach the requirement of hot bending and crystallization, reduce energy consumption, improve production efficiency.
Summary of the invention
In order to need in the production that solves CURVE DECORATIVE SHEET OF CERAMIC GLASS in the prior art sheet material is carried out twice thermal treatment (carrying out hot bending after the crystallization), cause the problem that energy consumption is excessive, production efficiency is low, the invention provides a kind of production technique of CURVE DECORATIVE SHEET OF CERAMIC GLASS, this production technique is carried out crystallization after adopting and earlier the crystallizing glass sheet material hot bending being handled again, only need sheet material is carried out a hyperthermic treatment, both save energy consumption, improved working efficiency again.
In order to reach above-mentioned technique effect, the present invention takes following technical scheme:
A kind of production technique of CURVE DECORATIVE SHEET OF CERAMIC GLASS, comprise after batching, fusing, calendering, the annealing crystallizing glass sheet material, it is characterized in that crystallizing glass sheet material is carried out hot bending earlier to be handled, crystallization is carried out to sheet material in the back, cooling after the crystallization, polishing.
In the production technique of above-mentioned CURVE DECORATIVE SHEET OF CERAMIC GLASS, the step of described hot bending processing and crystallization is specific as follows: hot bending is handled: place the hot bending kiln to be warming up to 760~850 ℃ crystallizing glass sheet material, insulation 2~4h carries out hot bending and coring and handles; Crystallization: after hot bending is finished, be warming up to 880~950 ℃ rapidly, sheet material is incubated crystallization.
As the preferred embodiments of the present invention, preferably: the time of described insulation crystallization is 40~60min.
As embodiments of the invention, described be cooled to adopt blower fan to sheet material cooling handle, be down to room temperature after, open the hot bending kiln.
The present invention compared with prior art has following beneficial effect:
(1) CURVE DECORATIVE SHEET OF CERAMIC GLASS adopts first hot bending, the production technique of crystallization then, only need sheet material is carried out a hyperthermic treatment, having saved high temperature carries out lowering the temperature after the crystallization to sheet material, again the two-step approach that the hot bending that heats up is again handled, not only save 50% energy consumption, shortened the production time of CURVE DECORATIVE SHEET OF CERAMIC GLASS simultaneously, improved working efficiency.
(2) softening temperature of non-crystallized crystallizing glass sheet material is lower than the sheet material after the crystallization, reduced the energy consumption in the hot bending treating processes, and because the temperature that non-crystallized sheet material hot bending is handled is lower, can reduces sheet material and burst or crackle in the hot bending processing, improve quality and the yield rate of product; Hot bending also is the process of crystallization when handling, and can improve the quality of product.
(3) adopt blower fan to the sheet material processing of lowering the temperature, be down to room temperature after, open the hot bending kiln, to the sheet material processing of progressively lowering the temperature, can reduce sheet material crackle takes place in temperature-fall period.
Embodiment
The invention will be further elaborated and explanation below in conjunction with embodiments of the invention.
Embodiment:
The crystallizing glass sheet material that the present invention adopts is through the crystallizing glass sheet material after batching, fusing, calendering, the annealing, does not pass through crystallization.Can be " utilizing granite waste to produce the method for devitrified glass building decorative plates " (ZL200910216248.0) step a)-d) make crystallizing glass sheet material according to patent name, concrete steps are as follows: a) the grouan waste is pulverized and be 50-350 purpose fine powder; B) above-mentioned grouan fine powder and component thereof are mixed by following weight ratio: granite fine powder 75-90, fluorite powder 2-5, dicalcium powder 6-12, soda ash 1-4, water 1-4; C) above-mentioned compound is sent into the all-electric melting kiln, be fused into glass metal under 1550-1650 ℃ temperature condition, enter clarification, homogenization material road through dog-hole, uptake, clarification, the homogenizing glass metal after good enters to be shaped expects the road; D) above-mentioned glass metal is delivered to the rolling press calendering formation by the material road that is shaped, mold temperature is 1050-1150 ℃, afterwards in type glass temperature is reduced to 850-950 ℃, is delivered to annealing furnace through crossing the roller platform, carries out anneal.Also can adopt the crystallizing glass sheet material that does not pass through crystallization of the method production that utilizes other as the starting material of production CURVE DECORATIVE SHEET OF CERAMIC GLASS of the present invention.
With the crystallizing glass sheet material of annealing, according to the arc specification, cut then.The sheet material that cuts is put into stainless steel mould, send into the hot bending kiln and handle.Set the heating temperature curve of hot bending kiln, carry out hot bending and crystallization, concrete steps are as follows: 1. earlier sheet material at the uniform velocity is warming up to 760 ℃-850 ℃, softening temperature according to different varieties sheet material is selected, heating-up time 40min-60min is incubated 2-4h again under this temperature, carry out hot bending and coring and handle.2. treat sheet material on request hot bending good after, be warming up to 880 ℃-950 ℃ rapidly, sheet material is incubated crystallization, soaking time 40min-80min.3. by blower fan to the sheet material processing of lowering the temperature, when temperature is down to the room temperature left and right sides, open the hot bending kiln, take out sheet material.4. with the circular arc grinding machine sheet material is polished and cuts, become CURVE DECORATIVE SHEET OF CERAMIC GLASS.
The production method that crystallizing glass sheet material production CURVE DECORATIVE SHEET OF CERAMIC GLASS adopts first hot bending of the present invention to handle the back crystallization needs about 7h, and the production method of hot bending needs 12h after the first crystallization and adopt.
Although invention has been described with reference to explanatory embodiment of the present invention here, above-described embodiment only is preferred implementation of the present invention, embodiments of the present invention are not restricted to the described embodiments, should be appreciated that, those skilled in the art can design a lot of other modification and embodiments, and these are revised and embodiment will drop within the disclosed principle scope and spirit of the application.

Claims (4)

1. the production technique of a CURVE DECORATIVE SHEET OF CERAMIC GLASS, comprise after batching, fusing, calendering, the annealing crystallizing glass sheet material, it is characterized in that crystallizing glass sheet material is carried out hot bending earlier to be handled, crystallization is carried out to sheet material in the back, cooling after the crystallization, polishing.
2. the production technique of CURVE DECORATIVE SHEET OF CERAMIC GLASS according to claim 1, it is characterized in that described hot bending is handled and the step of crystallization is specific as follows: hot bending is handled: place the hot bending kiln to be warming up to 760~850 ℃ crystallizing glass sheet material, insulation 2~4h carries out hot bending and coring and handles; Crystallization: after hot bending is finished, be warming up to 880~950 ℃ rapidly, sheet material is incubated crystallization.
3. the production technique of CURVE DECORATIVE SHEET OF CERAMIC GLASS according to claim 2, the time that it is characterized in that described insulation crystallization is 40~60min.
4. according to the production technique of each described CURVE DECORATIVE SHEET OF CERAMIC GLASS of claim 1-3, it is characterized in that described be cooled to adopt blower fan to sheet material cooling handle, be down to room temperature after, open the hot bending kiln.
CN2013101513170A 2013-04-27 2013-04-27 Production process of microcrystalline glass curved plate Pending CN103232152A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107713776A (en) * 2017-09-29 2018-02-23 佛山市曼凯盛科技有限公司 The method for producing devitrified glass baking tray
CN108328910A (en) * 2018-04-11 2018-07-27 四川名微晶科技股份有限公司 Microwave thermal bend kiln and the method for preparing hot bending devitrified glass using microwave heating
CN109369021A (en) * 2018-10-15 2019-02-22 基智精密科技(深圳)有限公司 Glass manufacturing apparatus and method for glass preparation
CN110894137A (en) * 2018-09-13 2020-03-20 深圳市东丽华科技有限公司 Toughened glass, 3D glass ceramic and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1180671A (en) * 1997-11-21 1998-05-06 清华大学 Manufacturing technology for sintering glass ceramics
CN1919764A (en) * 2006-10-09 2007-02-28 雷恒孚 Manufacture method of large-size glass-ceramic decoration plate
CN101462820A (en) * 2009-01-08 2009-06-24 广东科迪微晶玻璃实业有限公司 Low-expansion glass-ceramics moulding method for lithium-aluminum-silicon system
CN101475300A (en) * 2008-11-20 2009-07-08 广州兴华玻璃工业有限公司 Hot bending process for big step glass
CN102583971A (en) * 2012-02-28 2012-07-18 徐日宏 Hot-melting glass with bowlder effect and manufacturing method of hot-melting glass

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1180671A (en) * 1997-11-21 1998-05-06 清华大学 Manufacturing technology for sintering glass ceramics
CN1919764A (en) * 2006-10-09 2007-02-28 雷恒孚 Manufacture method of large-size glass-ceramic decoration plate
CN101475300A (en) * 2008-11-20 2009-07-08 广州兴华玻璃工业有限公司 Hot bending process for big step glass
CN101462820A (en) * 2009-01-08 2009-06-24 广东科迪微晶玻璃实业有限公司 Low-expansion glass-ceramics moulding method for lithium-aluminum-silicon system
CN102583971A (en) * 2012-02-28 2012-07-18 徐日宏 Hot-melting glass with bowlder effect and manufacturing method of hot-melting glass

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107713776A (en) * 2017-09-29 2018-02-23 佛山市曼凯盛科技有限公司 The method for producing devitrified glass baking tray
CN108328910A (en) * 2018-04-11 2018-07-27 四川名微晶科技股份有限公司 Microwave thermal bend kiln and the method for preparing hot bending devitrified glass using microwave heating
CN108328910B (en) * 2018-04-11 2023-10-10 四川一名微晶科技股份有限公司 Microwave hot bending kiln and method for preparing hot bending microcrystalline glass by utilizing microwave heating
CN110894137A (en) * 2018-09-13 2020-03-20 深圳市东丽华科技有限公司 Toughened glass, 3D glass ceramic and preparation method thereof
CN109369021A (en) * 2018-10-15 2019-02-22 基智精密科技(深圳)有限公司 Glass manufacturing apparatus and method for glass preparation
US11192816B2 (en) 2018-10-15 2021-12-07 Shenzhen Jingjiang Yunchuang Technology Co., Ltd. Glass production apparatus and method for manufacturing glass

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Application publication date: 20130807