CN103222942A

CN103222942A - Chinese herbal medicine foot bath solution added with bamboo vinegar and preparation method thereof

Info

Publication number: CN103222942A
Application number: CN2013101827924A
Authority: CN
Inventors: 王友升; 崔宇; 刘永国; 张燕
Original assignee: JIANGYIN ZHONGLI BIOLOGICAL TECHNOLOGY Co Ltd; Beijing Technology and Business University
Current assignee: JIANGYIN ZHONGLI BIOLOGICAL TECHNOLOGY Co Ltd; Beijing Technology and Business University
Priority date: 2013-05-17
Filing date: 2013-05-17
Publication date: 2013-07-31

Abstract

The invention aims at providing a hand sanitizer realizing continuous bacteriostasis and lasting fragrance and rich in natural moisture preserving components and nutrition factors and a preparation method thereof. The main components of the hand sanitizer include fatty alcohol-polyoxyethylene ether sodium sulfate, cocamidopropyl betaine, coconutt diethanol amide, clove essence, bamboo vinegar, NaCl and LGP. The preparation method comprises the following steps of: firstly preparing the bamboo vinegar; placing the fatty alcohol-polyoxyethylene ether sodium sulfate and deionized water in a reaction kettle, and standing until the fatty alcohol-polyoxyethylene ether sodium sulfate is completely dissolved at room temperature; sequentially adding the cocamidopropyl betaine, coconutt diethanol amide, clove essence 1#, clove essence 2# and bamboo vinegar at a stirring speed of 80rpm, and stirring uniformly; adding the NaCl at a stirring speed of 50rpm, and stirring at 50rpm until the NaCl is completely dissolved; adding the michelia essence and LGP, and stirring uniformly at the stirring speed of 50rpm; and then vacuumizing to remove bubbles to obtain the bamboo vinegar hand sanitizer. The bamboo vinegar hand sanitizer provided by the invention is rich in bamboo vinegar essence, and can promote blood circulation of hands and delay cell aging while reducing bacterium invasion, infection risk and disease occurrence and transmission.

Description

A kind of Chinese herbal medicine foot bath liquid that adds Bamboo vinegar and preparation method thereof

Technical field

The invention belongs to daily articles for washing field, concrete is a kind of contain the Bamboo vinegar composition, have antibacterial, as to nourish an effect handwashing liquid.

Background technology

Existing handwashing liquid generally only has simple cleaning action, and often fungistatic effect is not enough, and some sterilizing compositions that add, and easily the hand skin is damaged, and makes both hands slowly become coarse, stiff.Therefore, it is antibacterial to need a kind of handwashing liquid to continue, again the handwashing liquid that can not damage hand.

Summary of the invention

The object of the present invention is to provide a kind of continue antibacterial, lasting is lasting, is rich in the handwashing liquid of natural moisture preserving composition and trophic factors.

The main component of this handwashing liquid is: polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine, cocoanut fatty acid diethanolamide, Flos Caryophylli essence, Bamboo vinegar, NaCl, LGP.

Its preparation method is: get the polyoxyethylenated alcohol sodium sulfate of percentage by weight 6% and 70.12% deionized water and place reactor, at room temperature dissolve fully to polyoxyethylenated alcohol sodium sulfate.With the mixing speed of 80rpm, add 4.5% cocamido propyl betaine, 1% cocoanut fatty acid diethanolamide, 4% Flos Caryophylli elite 1#, 2% Flos Caryophylli elite 2# and 10% Bamboo vinegar successively, subsequently to stirring.Mixing speed with 50rpm adds 1.8%NaCl then, keeps 50rpm to be stirred to NaCl and dissolves fully, adds 0.08% michelia essence and 0.5%LGP, keeps the 50rpm mixing speed to stirring.Evacuation just obtains the Bamboo vinegar handwashing liquid to remove bubble afterwards.

Wherein the preparation method of Flos Caryophylli elite is: get Flos Caryophylli 50g, wrap with filter cloth and place the 1L beaker, add 500ml, 70% ethanol, after the soaked overnight, extract 2h down at 55 ℃; Cross leaching filtrate; Add 500ml, 70% ethanol in filtering residue, 55 ℃ are extracted 2h down, cross leaching filtrate; Add 500ml, 70% ethanol once more in filtering residue, 55 ℃ are extracted 2h down, cross leaching filtrate.Mix three times filtrate, steam to 150ml, get wherein half, be the glycerol that 75ml adds 75ml, obtain Flos Caryophylli elite 1# at 55 ℃ of backspins; Get second half and add the 75ml propylene glycol, obtain Flos Caryophylli elite 2#.

Wherein the preparation method of Bamboo vinegar is: bamboo chip is made in the bamboo wood fragmentation, dry distilling and carbonization then, carry out condensed in two stages, and leave standstill after the liquid of condensed in two stages gained mixed in blending tank, obtain the elementary Bamboo vinegar solution of pH2.5-3.0, and under 40-100 ℃ of temperature range, condition more than the vacuum 0.08Mpa, carry out the one-level distillation, when distillation yield is the 80-90% of stock solution volume, carry out condensation and collect and obtain the one-level distillate.The one-level distillate placed under 40-100 ℃ of temperature range, the condition more than the vacuum 0.085Mpa carry out secondary distillation, when distillation yield is the 80-90% of original volume, obtain required Bamboo vinegar.

Bamboo vinegar handwashing liquid of the present invention contains the Bamboo vinegar elite, can promote the hand blood circulation, and delaying cell aging reduces the antibacterial infringement simultaneously, reduces infection risk, reduces the generation and the propagation of disease.

The specific embodiment

At first, carry out the preparation of Flos Caryophylli elite: get Flos Caryophylli 50g, wrap with filter cloth and place the 1L beaker, add 500ml, 70% ethanol, after the soaked overnight, extract 2h down at 55 ℃; Cross leaching filtrate; Add 500ml, 70% ethanol in filtering residue, 55 ℃ are extracted 2h down, cross leaching filtrate; Add 500ml, 70% ethanol once more in filtering residue, 55 ℃ are extracted 2h down, cross leaching filtrate.Mix three times filtrate, steam to 150ml, get wherein half, be the glycerol that 75ml adds 75ml, obtain Flos Caryophylli elite 1# at 55 ℃ of backspins; Get second half and add the 75ml propylene glycol, obtain Flos Caryophylli elite 2#.

Then, carry out the preparation of Bamboo vinegar: bamboo chip is made in the bamboo wood fragmentation, dry distilling and carbonization then, carry out condensed in two stages, and leave standstill after the liquid of condensed in two stages gained mixed in blending tank, obtain the elementary Bamboo vinegar solution of pH2.5-3.0, and under 40-100 ℃ of temperature range, condition more than the vacuum 0.08Mpa, carry out the one-level distillation, when distillation yield is the 80-90% of stock solution volume, carry out condensation and collect and obtain the one-level distillate.The one-level distillate placed under 40-100 ℃ of temperature range, the condition more than the vacuum 0.085Mpa carry out secondary distillation, when distillation yield is the 80-90% of original volume, obtain required Bamboo vinegar.

The polyoxyethylenated alcohol sodium sulfate of percentage by weight 6% and 70.12% deionized water place reactor, at room temperature dissolve fully to polyoxyethylenated alcohol sodium sulfate.With the mixing speed of 80rpm, add 4.5% cocamido propyl betaine, 1% cocoanut fatty acid diethanolamide, 4% Flos Caryophylli elite 1#, 2% Flos Caryophylli elite 2# and 10% Bamboo vinegar successively, subsequently to stirring.Mixing speed with 50rpm adds 1.8%NaCl then, keeps 50rpm to be stirred to NaCl and dissolves fully, adds 0.08% michelia essence and 0.5%LGP, keeps the 50rpm mixing speed to stirring.Evacuation just obtains the Bamboo vinegar handwashing liquid to remove bubble afterwards.

Performance test:

Get Bamboo vinegar handwashing liquid sample at the nutrient agar flat board, place 37 ℃, cultivate 48h, 5 flat boards all do not have colony growth, so total number of bacteria is 0cfu/ml.

Get Bamboo vinegar handwashing liquid sample at the sabouraud culture medium flat board, place 28 ℃, the result who cultivated 7 days shows that when cultivating 3d, 5d, 5 flat boards all do not have bacteria growing, have only 1 block of plate that a bacterium colony is arranged during 7d, so the mycete yeast adds up to 0.2cfu/ml.The testing result of comprehensive total number of bacteria and mycete, yeast sum is learnt the total plate count＜200cfu/ml of Bamboo vinegar handwashing liquid sample to meet GB19877.1-2005.

Claims

1. the preparation method of a Bamboo vinegar handwashing liquid, the main component of this handwashing liquid is: polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine, cocoanut fatty acid diethanolamide, Flos Caryophylli essence, Bamboo vinegar, NaCl, LGP; It is characterized in that: at first carry out the preparation of Bamboo vinegar; Then polyoxyethylenated alcohol sodium sulfate and deionized water are placed reactor, at room temperature dissolve fully to polyoxyethylenated alcohol sodium sulfate; With the mixing speed of 80rpm, add cocamido propyl betaine, cocoanut fatty acid diethanolamide, Flos Caryophylli elite 1#, Flos Caryophylli elite 2# and Bamboo vinegar successively, subsequently to stirring; Mixing speed with 50rpm adds NaCl then, keeps 50rpm to be stirred to NaCl and dissolves fully, adds michelia essence and LGP, keeps the 50rpm mixing speed to stirring; Evacuation obtains the Bamboo vinegar handwashing liquid to remove bubble afterwards.

2. the described preparation method of claim 1, wherein the preparation method of Flos Caryophylli elite is as follows: get Flos Caryophylli 50g, wrap with filter cloth and place the 1L beaker, add 500ml, 70% ethanol, after the soaked overnight, extract 2h down at 55 ℃; Cross leaching filtrate; Add 500ml, 70% ethanol in filtering residue, 55 ℃ are extracted 2h down, cross leaching filtrate; Add 500ml, 70% ethanol once more in filtering residue, 55 ℃ are extracted 2h down, cross leaching filtrate; Mix three times filtrate, steam to 150ml, get wherein half, be the glycerol that 75ml adds 75ml, obtain Flos Caryophylli elite 1# at 55 ℃ of backspins; Get second half and add the 75ml propylene glycol, obtain Flos Caryophylli elite 2#.

3. the described preparation method of claim 1, wherein the preparation method of Bamboo vinegar is as follows: bamboo chip is made in the bamboo wood fragmentation, dry distilling and carbonization then, carry out condensed in two stages, and leave standstill after the liquid of condensed in two stages gained mixed in blending tank, obtain the elementary Bamboo vinegar solution of pH2.5-3.0, and under 40-100 ℃ of temperature range, condition more than the vacuum 0.08Mpa, carry out the one-level distillation, when distillation yield is the 80-90% of stock solution volume, carry out condensation and collect and obtain the one-level distillate; The one-level distillate placed under 40-100 ℃ of temperature range, the condition more than the vacuum 0.085Mpa carry out secondary distillation, when distillation yield is the 80-90% of original volume, obtain required Bamboo vinegar.

4. the described preparation method of one of claim 1-3, wherein the weight percent content of handwashing liquid composition is: 6% polyoxyethylenated alcohol sodium sulfate, 4.5 cocamido propyl betaine, 1% cocoanut fatty acid diethanolamide, 4% Flos Caryophylli elite 1#, 2% Flos Caryophylli elite 2# and 10% Bamboo vinegar, 0.08% michelia essence, 0.5LGP, 1.8%NaCl and 70.12 deionized waters.

5. the Bamboo vinegar handwashing liquid that obtains of the described preparation method of one of claim 1-4.