CN103192024A - Preparation method of mixed binder of water glass and silicasol - Google Patents

Preparation method of mixed binder of water glass and silicasol Download PDF

Info

Publication number
CN103192024A
CN103192024A CN201310108471XA CN201310108471A CN103192024A CN 103192024 A CN103192024 A CN 103192024A CN 201310108471X A CN201310108471X A CN 201310108471XA CN 201310108471 A CN201310108471 A CN 201310108471A CN 103192024 A CN103192024 A CN 103192024A
Authority
CN
China
Prior art keywords
waterglass
parts
ludox
preparation
defoamer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201310108471XA
Other languages
Chinese (zh)
Inventor
邵建栋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUXI UNIVERSAL PRECISION CASTING CO Ltd
Original Assignee
WUXI UNIVERSAL PRECISION CASTING CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WUXI UNIVERSAL PRECISION CASTING CO Ltd filed Critical WUXI UNIVERSAL PRECISION CASTING CO Ltd
Priority to CN201310108471XA priority Critical patent/CN103192024A/en
Publication of CN103192024A publication Critical patent/CN103192024A/en
Pending legal-status Critical Current

Links

Landscapes

  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention relates to a preparation method of a mixed binder of water glass and silicasol. The preparation method comprises the steps of uniformly mixing water glass, a silicasol solution, fireproof powder and a penetrating agent in a certain weight proportion at the temperature of 15-30 DEG C, adding a defoamer into a mixture to carry out defoaming, and standing for more than 8h finally to obtain the mixed binder of water glass and silicasol. With the adoption of the binder prepared by the method, the powder-liquid ratio of a surface layer coating is high, the back surface of a mold shell is smooth so that the surface finish of a casting is improved, and the strength of the mold shell is also uniform.

Description

Waterglass and Ludox hybrid adhesive preparation method
Technical field
The present invention relates to a kind of preparation method of binding agent, is in the casting industry specifically, for the manufacture of the preparation method of waterglass and the Ludox hybrid adhesive of shell.
Background technology
As everyone knows, in casting industry, for the manufacture of main three kinds of the binding agent of shell, they are respectively sodium silicate binder, silica sol binder, waterglass and Ludox compound binding agent.Problems such as behind the sodium silicate binder shell, its surface exists that sodium salt gathers, worm hole and surface layer come off make that the fineness of cast(ing) surface is relatively poor, need polish to wait toward contact and process operation.The investment precoat powder liquor ratio of silica sol binder is often lower, and it has corrosiveness to wax-pattern, and behind its shell, the surface is also more coarse, and unevenness is excessive, also can cause the fineness of cast(ing) surface poor.And the principle of waterglass and Ludox compound binding agent shell is, elder generation is at wax-pattern surface-coated Ludox and carry out drying, applies waterglass again, dry shell.But, because the elevated temperature strength of waterglass and Ludox is different, thereby cause the interlaminar strength of this shell inhomogeneous.
Summary of the invention
The problem to be solved in the present invention provides a kind of waterglass and Ludox hybrid adhesive preparation method, adopts the binding agent of this method preparation, investment precoat powder liquor ratio height, and the shell rear surface is comparatively smooth, make cast(ing) surface fineness improve, and investment shell intensity is even.
For addressing the above problem, take following scheme:
Waterglass of the present invention and Ludox hybrid adhesive preparation method's characteristics are may further comprise the steps:
The first step is chosen the raw material of following parts by weight: 88~92 parts of waterglass, 8~12 parts of silicon sol solutions, 125~135 parts of refractory powders, 0.4~0.6 part of bleeding agent, 0.04~0.06 part of defoamer;
Second one, under 15~30 ℃ temperature, waterglass, silicon sol solution, refractory powder and bleeding agent are put into agitator together, stir, obtain mixed liquor;
The 3rd one, under 15~30 ℃ temperature, add defoamer in the mixed liquor and stir;
The 4th one, under 15~30 ℃ temperature, the mixed liquor that will have defoamer was placed more than 8 hours, obtained waterglass and Ludox hybrid adhesive.
Wherein, described refractory powder is silica flour.
Take such scheme, have the following advantages:
Because waterglass of the present invention and Ludox hybrid adhesive preparation method mix waterglass and Ludox, and added a large amount of refractory powders therein, therefore, the powder liquor ratio of its investment precoat is higher, mobile, spreadability is better, the shell rear surface is comparatively smooth, can improve the fineness of cast(ing) surface.And behind waterglass and the Ludox mixed-forming, there is not interlayer structure in its shell, and the elevated temperature strength of shell integral body is comparatively even.
The specific embodiment
Be described in further details below in conjunction with the present invention of embodiment:
Embodiment one
Under 15 ℃ room temperature condition, implement following steps:
The first step is chosen 88 parts of waterglass, 12 parts of silicon sol solutions, 125 parts of silica flours, 0.4 part of bleeding agent, 0.04 part of defoamer.Above-mentioned umber is parts by weight.
Second one, waterglass, silicon sol solution, refractory powder and bleeding agent are put into agitator together, stir, obtain mixed liquor.
The 3rd one, add defoamer in the mixed liquor and stir.
The 4th one, the mixed liquor that will have defoamer was placed more than 8 hours, obtained waterglass and Ludox hybrid adhesive.
Embodiment two
Under 20 ℃ room temperature condition, implement following steps:
The first step is chosen 90 parts of waterglass, 10 parts of silicon sol solutions, 130 parts of silica flours, 0.5 part of bleeding agent, 0.05 part of defoamer.Above-mentioned umber is parts by weight.
Second one, waterglass, silicon sol solution, refractory powder and bleeding agent are put into agitator together, stir, obtain mixed liquor.
The 3rd one, add defoamer in the mixed liquor and stir.
The 4th one, the mixed liquor that will have defoamer was placed more than 8 hours, obtained waterglass and Ludox hybrid adhesive.
Embodiment three
Under 30 ℃ room temperature condition, implement following steps:
The first step is chosen 92 parts of waterglass, 8 parts of silicon sol solutions, 135 parts of silica flours, 0.6 part of bleeding agent, 0.06 part of defoamer.Above-mentioned umber is parts by weight.
Second one, waterglass, silicon sol solution, refractory powder and bleeding agent are put into agitator together, stir, obtain mixed liquor.
The 3rd one, add defoamer in the mixed liquor and stir.
The 4th one, the mixed liquor that will have defoamer was placed more than 8 hours, obtained waterglass and Ludox hybrid adhesive.

Claims (2)

1. waterglass and Ludox hybrid adhesive preparation method is characterized in that may further comprise the steps:
Choose the raw material of following parts by weight earlier:
88~92 parts of waterglass,
8~12 parts of silicon sol solutions,
125~135 parts of refractory powders,
0.4~0.6 part of bleeding agent,
0.04~0.06 part of defoamer;
Then, under 15~30 ℃ temperature, waterglass, silicon sol solution, refractory powder and bleeding agent are put into agitator together, stir, obtain mixed liquor;
Afterwards, under 15~30 ℃ temperature, add defoamer in the mixed liquor and stir;
At last, under 15~30 ℃ temperature, the mixed liquor that will have defoamer was placed more than 8 hours, obtained waterglass and Ludox hybrid adhesive.
2. waterglass as claimed in claim 1 and Ludox hybrid adhesive preparation method is characterized in that described refractory powder is silica flour.
CN201310108471XA 2013-04-01 2013-04-01 Preparation method of mixed binder of water glass and silicasol Pending CN103192024A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310108471XA CN103192024A (en) 2013-04-01 2013-04-01 Preparation method of mixed binder of water glass and silicasol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310108471XA CN103192024A (en) 2013-04-01 2013-04-01 Preparation method of mixed binder of water glass and silicasol

Publications (1)

Publication Number Publication Date
CN103192024A true CN103192024A (en) 2013-07-10

Family

ID=48714942

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310108471XA Pending CN103192024A (en) 2013-04-01 2013-04-01 Preparation method of mixed binder of water glass and silicasol

Country Status (1)

Country Link
CN (1) CN103192024A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106141073A (en) * 2016-08-22 2016-11-23 浙江遂金特种铸造有限公司 Ludox component is used in a kind of casting

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86102002A (en) * 1986-03-20 1986-09-10 沈阳工业学院 Ludox, water glass composite shell
CN1032503A (en) * 1987-10-12 1989-04-26 国家机械工业委员会沈阳铸造研究所 Compound shell-producing technology using silica-sol wash
US20040244943A1 (en) * 2003-06-04 2004-12-09 American Colloid Company Acid activated clay for use in foundry sand
CN1827256A (en) * 2006-04-14 2006-09-06 清华大学 Method for direct production of core in narrow groove and blind hole of wax mould

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86102002A (en) * 1986-03-20 1986-09-10 沈阳工业学院 Ludox, water glass composite shell
CN1032503A (en) * 1987-10-12 1989-04-26 国家机械工业委员会沈阳铸造研究所 Compound shell-producing technology using silica-sol wash
US20040244943A1 (en) * 2003-06-04 2004-12-09 American Colloid Company Acid activated clay for use in foundry sand
CN1827256A (en) * 2006-04-14 2006-09-06 清华大学 Method for direct production of core in narrow groove and blind hole of wax mould

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106141073A (en) * 2016-08-22 2016-11-23 浙江遂金特种铸造有限公司 Ludox component is used in a kind of casting

Similar Documents

Publication Publication Date Title
CN104402009B (en) Calcium silicate hydrate gel solution early strength agent and suction filtration preparation method thereof
CN103058623B (en) Foamed water glass expanded perlite thermal insulating board
CN107311560A (en) A kind of inorganic heat insulation mortar and preparation method thereof
CN104014719B (en) A kind of high-performance alcohol base casting coatings and preparation method thereof
CN105294134B (en) A kind of preparation method of the iron runner castable containing graphene oxide
CN101838433A (en) Method for preparing polycarboxylic compound ceramic water reducing agent
CN106220096A (en) A kind of have the excellent durable and concrete of water resistance
CN103182514B (en) Method for preparing neodymium iron boron magnetic powder by self-propagating combustion
CN102838379B (en) Lightweight foamed ceramics and preparation method thereof
CN102875157A (en) Preparation method of aluminum oxide ceramics
CN103357814A (en) Lost foam casting-use paint formula and technology method thereof
CN108299001A (en) A kind of silicon-base ceramic core forming method
CN103626510B (en) Method for preparing magnesium borate whisker porous ceramic by employing in-situ growth
CN102357648A (en) Chill coating for casting
CN105798225A (en) Anti-crack enhanced complexing agent for fired mold precision casting paint and application thereof
CN104525064B (en) A kind of alkaline silica sol and preparation method thereof
CN104371703A (en) Method for preparing oil fracturing proppant from high-aluminum fly ash
CN101941046B (en) Composite sodium silicate binder for sand mold and preparing method thereof
CN105218108A (en) A kind of cement kiln external system high-strength sprayed material and preparation using method thereof
CN108296428A (en) A kind of dry powder lost foam casting coating
CN103551496B (en) Anhydrous water-base forsterite powder paint
CN103192024A (en) Preparation method of mixed binder of water glass and silicasol
CN102515796B (en) High-temperature composite environment-friendly paint used in glass kiln
CN107417160A (en) The synthetic method of silane-modified ammonium polyacrylate water reducer under a kind of microwave action
CN102557579A (en) Silica-based porous composite heat insulation material and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C05 Deemed withdrawal (patent law before 1993)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20130710