CN103190789B - Manufacturing method of antibacterial and deodorant duvet - Google Patents

Manufacturing method of antibacterial and deodorant duvet Download PDF

Info

Publication number
CN103190789B
CN103190789B CN201310079785.1A CN201310079785A CN103190789B CN 103190789 B CN103190789 B CN 103190789B CN 201310079785 A CN201310079785 A CN 201310079785A CN 103190789 B CN103190789 B CN 103190789B
Authority
CN
China
Prior art keywords
antibacterial
deodouring
preparation
eiderdown quilt
fiber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201310079785.1A
Other languages
Chinese (zh)
Other versions
CN103190789A (en
Inventor
沈守兵
宋春常
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Shuixing Home Textile Co Ltd
Original Assignee
Shanghai Shuixing Home Textile Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Shuixing Home Textile Co Ltd filed Critical Shanghai Shuixing Home Textile Co Ltd
Priority to CN201310079785.1A priority Critical patent/CN103190789B/en
Publication of CN103190789A publication Critical patent/CN103190789A/en
Application granted granted Critical
Publication of CN103190789B publication Critical patent/CN103190789B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention aims to disclose a manufacturing method of an antibacterial and deodorant duvet. The manufacturing method comprises the following steps: (1) pretreating down; (2) manufacturing antibacterial and deodorant down fiber; (3) drying and sterilizing by ultraviolet; and (4) manufacturing the antibacterial and deodorant duvet. Compared with the prior art, by compounding a silver-based inorganic antibacterial agent RHA-T1 of NAFUR and a chitin antibacterial finishing agent SA-50DS of Japanese TK, the down fiber has a lasting antibacterial and deodorant function under the condition that a bonding agent is not added; and by a method of filling antibacterial fiber and the antibacterial and deodorant down fiber in a mixed way, the duvet has a more lasting antibacterial and deodorant effect, therefore, the aim of the invention is achieved.

Description

A kind of preparation method of antibacterial deodourizing eiderdown quilt
Technical field
The present invention relates to a kind of preparation method of eiderdown quilt, particularly a kind of preparation method of antibacterial deodourizing eiderdown quilt.
Background technology
Eider down is good natural heat insulating material formed, has light weight, and soft, the advantages such as good heat preservation performance, eiderdown quilt is also the preferably selection of consumer's insulated bed Bed linens.But the chemical composition of eider down is a kind of protein, and with animal fat, through degreasing repeatedly, cleaning in processing procedure, still impurity and bacterium can not be eliminated completely.
In recent years, the antibacterial deodourizing research of down feather material is also constantly increased, as the China Patent Publication No. patent of invention that is CN1327079C discloses a kind of processing method of eider down of anti-bacteria and anti-virus mildew-resistant deodorization health function, use chitin is solvent impregnated or spray into down fiber, but this method chitin and down fiber binding strength poor, antibacterial deodourizing effect is also not obvious; In addition also have and adopt organic antibacterial agent to carry out the method for antimicrobial treatment, but the method poor safety performance, effect persistence is undesirable.
The chemical composition of eider down is a kind of protein, and with animal fat, through degreasing repeatedly, cleaning in processing procedure, still impurity and bacterium can not be eliminated completely, solve the problem of breed bacteria in its use procedure, a kind of antibacterial finishing agent of high-efficient and lasting must be adopted.
Therefore, the special preparation method needing a kind of antibacterial deodourizing eiderdown quilt, to solve above-mentioned existing Problems existing.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of antibacterial deodourizing eiderdown quilt, for the deficiencies in the prior art, its antibacterial effect is obvious, more than 98% is reached to the staphylococcic bacteriostasis rate in candida albicans, Escherichia coli and Kingsoft, and have long-lasting, in use breed bacteria can not produce stink, also can improve consumer and use eiderdown quilt allergic phenomena, considerably increase the use crowd of eiderdown quilt.
Technical problem solved by the invention can realize by the following technical solutions:
A preparation method for antibacterial deodourizing eiderdown quilt, is characterized in that, it comprises the steps:
(1) eider down pre-treatment: raw material goes stalk → dedust husky → smart point → previous cleaning → washing → dehydration;
(2) preparation of antibacterial and deodouring down fiber: adopt the silver-based inorganic antibacterial agent RHA-T1 of NAFUR and the chitin antibacterial finishing agent SA-50DS of Japanese TK to carry out composite, the obtained antibacterial and deodouring down fiber that can wash;
(3) drying and processing: the antibacterial and deodouring down fiber prepared is carried out drying and processing;
(4) ultraviolet-sterilization process: adopt ultraviolet sterilization device to carry out sterilization processing to the eider down of drying;
(5) preparation of antibacterial and deodouring eiderdown quilt: adopt anti-bacterial fibre and antibacterial and deodouring down fiber jointly to mix and fill suede, obtained antibacterial and deodouring eiderdown quilt.
In one embodiment of the invention, described previous cleaning is cold wash, and the wash time of described previous cleaning is 4-15 minute.
In one embodiment of the invention, described washing is adopt the high down suede cleaning agent Riel ECO of Zhejiang riel chemical industry to carry out carrying out washing treatment, and consumption is 10-30g/L, and pH value is 6.5-7.5, and temperature is 40-60 DEG C, and the processing time is 30-40min.
In one embodiment of the invention, in the preparation of described antibacterial and deodouring down fiber, adjusted to ph, to 6-7.5, is warmed up to 70-80 DEG C, is then incubated 10-200min.
In one embodiment of the invention, the temperature of described oven dry is 100-120 DEG C, and the time is 10-20 min.
In one embodiment of the invention, described anti-bacterial fibre is the one in chitin fiber or Kang Tesi (Chitcel) fiber.
In one embodiment of the invention, described antibacterial and deodouring down fiber is >=98% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
In one embodiment of the invention, the antibacterial and deodouring eiderdown quilt of preparation, in use after 1 year, is >=95% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
The preparation method of antibacterial deodourizing eiderdown quilt of the present invention, compared with prior art, the silver-based inorganic antibacterial agent RHA-T1 of NAFUR and the chitin antibacterial finishing agent SA-50DS of Japanese TK is adopted to carry out composite, under making not add the condition of adhesive, down fiber has long-acting antibacterial and deodouring function, adopt anti-bacterial fibre to mix the way of filling suede with antibacterial and deodouring down fiber simultaneously, make eiderdown quilt have more lasting antibiosis and deodorization effects, realize object of the present invention.
The detailed description and obtaining that feature of the present invention can consult the better embodiment of below this case is well understood to.
Detailed description of the invention
The technological means realized to make the present invention, creation characteristic, reach object and effect is easy to understand, below in conjunction with specifically setting forth the present invention further.
The preparation method of antibacterial deodourizing eiderdown quilt of the present invention, it comprises the steps:
(1) eider down pre-treatment: raw material goes stalk → dedust husky → smart point → previous cleaning → washing → dehydration;
(2) preparation of antibacterial and deodouring down fiber: adopt the silver-based inorganic antibacterial agent RHA-T1 of NAFUR and the chitin antibacterial finishing agent SA-50DS of Japanese TK to carry out composite, the obtained antibacterial and deodouring down fiber that can wash;
(3) drying and processing: the antibacterial and deodouring down fiber prepared is carried out drying and processing;
(4) ultraviolet-sterilization process: adopt ultraviolet sterilization device to carry out sterilization processing to the eider down of drying;
(5) preparation of antibacterial and deodouring eiderdown quilt: adopt anti-bacterial fibre and antibacterial and deodouring down fiber jointly to mix and fill suede, obtained antibacterial and deodouring eiderdown quilt.
In the present invention, described previous cleaning is cold wash, and the wash time of described previous cleaning is 4-15 minute.
In the present invention, described washing is adopt the high down suede cleaning agent Riel ECO of Zhejiang riel chemical industry to carry out carrying out washing treatment, and consumption is 10-30g/L, and pH value is 6.5-7.5, and temperature is 40-60 DEG C, and the processing time is 30-40min.
In the present invention, in the preparation of described antibacterial and deodouring down fiber, adjusted to ph, to 6-7.5, is warmed up to 70-80 DEG C, is then incubated 10-200min.
In the present invention, the temperature of described oven dry is 100-120 DEG C, and the time is 10-20 min.
In the present invention, described anti-bacterial fibre is the one in chitin fiber or Kang Tesi (Chitcel) fiber.
In the present invention, described antibacterial and deodouring down fiber is >=98% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
In the present invention, the antibacterial and deodouring eiderdown quilt of preparation, in use after 1 year, is >=95% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
Embodiment 1
Processing step:
(1) eider down pre-treatment: raw material goes stalk → dedust husky → smart point → previous cleaning → washing → dehydration;
(2) preparation of antibacterial and deodouring down fiber: adopt the silver-based inorganic antibacterial agent RHA-T1 of NAFUR and the chitin antibacterial finishing agent SA-50DS of Japanese TK to carry out composite, the obtained antibacterial and deodouring down fiber that can wash;
(3) drying and processing: the antibacterial and deodouring down fiber prepared is carried out drying and processing;
(4) ultraviolet-sterilization process: adopt ultraviolet sterilization device to carry out sterilization processing to the eider down of drying;
(5) preparation of antibacterial and deodouring eiderdown quilt: adopt anti-bacterial fibre and antibacterial and deodouring down fiber jointly to mix and fill suede, obtained antibacterial and deodouring eiderdown quilt.
Described previous cleaning is cold wash, and the wash time of described previous cleaning is 4 minutes.
Described washing is adopt the high down suede cleaning agent Riel ECO of Zhejiang riel chemical industry to carry out carrying out washing treatment, and consumption is 10g/L, and pH value is 6.5, and temperature is 40 DEG C, and the processing time is 30min.
In the preparation of described antibacterial and deodouring down fiber, adjusted to ph to 6, is warmed up to 70 DEG C, is then incubated 10min.
The temperature of described oven dry is 100 DEG C, and the time is 20 min.
Described anti-bacterial fibre is chitin fiber.
Described antibacterial and deodouring down fiber is >=98% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate; The antibacterial and deodouring eiderdown quilt of preparation, in use after 1 year, is >=95% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
Embodiment 2
Processing step:
(1) eider down pre-treatment: raw material goes stalk → dedust husky → smart point → previous cleaning → washing → dehydration;
(2) preparation of antibacterial and deodouring down fiber: adopt the silver-based inorganic antibacterial agent RHA-T1 of NAFUR and the chitin antibacterial finishing agent SA-50DS of Japanese TK to carry out composite, the obtained antibacterial and deodouring down fiber that can wash;
(3) drying and processing: the antibacterial and deodouring down fiber prepared is carried out drying and processing;
(4) ultraviolet-sterilization process: adopt ultraviolet sterilization device to carry out sterilization processing to the eider down of drying;
(5) preparation of antibacterial and deodouring eiderdown quilt: adopt anti-bacterial fibre and antibacterial and deodouring down fiber jointly to mix and fill suede, obtained antibacterial and deodouring eiderdown quilt.
Described previous cleaning is cold wash, and the wash time of described previous cleaning is 15 minutes.
Described washing is adopt the high down suede cleaning agent Riel ECO of Zhejiang riel chemical industry to carry out carrying out washing treatment, and consumption is 30g/L, and pH value is 7.5, and temperature is 60 DEG C, and the processing time is 40min.
In the preparation of described antibacterial and deodouring down fiber, adjusted to ph to 7.5, is warmed up to 80 DEG C, is then incubated 200min.
The temperature of described oven dry is 120 DEG C, and the time is 10 min.
Described anti-bacterial fibre is Kang Tesi (Chitcel) fiber.
Described antibacterial and deodouring down fiber is >=98% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate; The antibacterial and deodouring eiderdown quilt of preparation, in use after 1 year, is >=95% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
Embodiment 3
Processing step:
(1) eider down pre-treatment: raw material goes stalk → dedust husky → smart point → previous cleaning → washing → dehydration;
(2) preparation of antibacterial and deodouring down fiber: adopt the silver-based inorganic antibacterial agent RHA-T1 of NAFUR and the chitin antibacterial finishing agent SA-50DS of Japanese TK to carry out composite, the obtained antibacterial and deodouring down fiber that can wash;
(3) drying and processing: the antibacterial and deodouring down fiber prepared is carried out drying and processing;
(4) ultraviolet-sterilization process: adopt ultraviolet sterilization device to carry out sterilization processing to the eider down of drying;
(5) preparation of antibacterial and deodouring eiderdown quilt: adopt anti-bacterial fibre and antibacterial and deodouring down fiber jointly to mix and fill suede, obtained antibacterial and deodouring eiderdown quilt.
Described previous cleaning is cold wash, and the wash time of described previous cleaning is 9 minutes.
Described washing is adopt the high down suede cleaning agent Riel ECO of Zhejiang riel chemical industry to carry out carrying out washing treatment, and consumption is 20g/L, and pH value is 7, and temperature is 50 DEG C, and the processing time is 35min.
In the preparation of described antibacterial and deodouring down fiber, adjusted to ph to 6.5, is warmed up to 75 DEG C, is then incubated 100min.
The temperature of described oven dry is 110 DEG C, and the time is 15 min.
Described anti-bacterial fibre is chitin fiber.
Described antibacterial and deodouring down fiber is >=98% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate; The antibacterial and deodouring eiderdown quilt of preparation, in use after 1 year, is >=95% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
More than show and describe general principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications; these changes and improvements all fall in the claimed scope of the invention, and application claims protection domain is defined by appending claims and equivalent thereof.

Claims (8)

1. a preparation method for antibacterial deodourizing eiderdown quilt, is characterized in that, it comprises the steps:
(1) eider down pre-treatment: raw material goes stalk → dedust husky → smart point → previous cleaning → washing → dehydration;
(2) preparation of antibacterial and deodouring down fiber: adopt silver-based inorganic antibacterial agent RHA-T1 and chitin antibacterial finishing agent SA-50DS to carry out composite, the obtained antibacterial and deodouring down fiber that can wash;
(3) drying and processing: the antibacterial and deodouring down fiber prepared is carried out drying and processing;
(4) ultraviolet-sterilization process: adopt ultraviolet sterilization device to carry out sterilization processing to the eider down of drying;
(5) preparation of antibacterial and deodouring eiderdown quilt: adopt anti-bacterial fibre and antibacterial and deodouring down fiber jointly to mix and fill suede, obtained antibacterial and deodouring eiderdown quilt.
2. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, it is characterized in that, described previous cleaning is cold wash, and the wash time of described previous cleaning is 4-15 minute.
3. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, is characterized in that, described washing carries out carrying out washing treatment for adopting high down suede cleaning agent Riel ECO, consumption is 10-30g/L, pH value is 6.5-7.5, and temperature is 40-60 DEG C, and the processing time is 30-40min.
4. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, it is characterized in that, in the preparation of described antibacterial and deodouring down fiber, adjusted to ph, to 6-7.5, is warmed up to 70-80 DEG C, is then incubated 10-200min.
5. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, it is characterized in that, the temperature of described oven dry is 100-120 DEG C, and the time is 10-20 min.
6. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, is characterized in that, described anti-bacterial fibre is the one in chitin fiber or Kang Tesi (Chitcel) fiber.
7. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, it is characterized in that, described antibacterial and deodouring down fiber is >=98% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
8. the preparation method of antibacterial deodourizing eiderdown quilt as claimed in claim 1, it is characterized in that, the antibacterial and deodouring eiderdown quilt of preparation, in use after 1 year, is >=95% to gold-coloured staphylococci, candida albicans and colibacillary bacteriostasis rate.
CN201310079785.1A 2013-03-13 2013-03-13 Manufacturing method of antibacterial and deodorant duvet Active CN103190789B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310079785.1A CN103190789B (en) 2013-03-13 2013-03-13 Manufacturing method of antibacterial and deodorant duvet

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310079785.1A CN103190789B (en) 2013-03-13 2013-03-13 Manufacturing method of antibacterial and deodorant duvet

Publications (2)

Publication Number Publication Date
CN103190789A CN103190789A (en) 2013-07-10
CN103190789B true CN103190789B (en) 2014-12-31

Family

ID=48713747

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310079785.1A Active CN103190789B (en) 2013-03-13 2013-03-13 Manufacturing method of antibacterial and deodorant duvet

Country Status (1)

Country Link
CN (1) CN103190789B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114224143A (en) * 2021-11-05 2022-03-25 仪征龙兴塑胶有限公司 Highly-waterproof antibacterial breathable sleeping bag and preparation method thereof

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103451957B (en) * 2013-08-09 2016-01-27 安徽华强羽绒有限公司 Fungus and mildew resistance eider down care agent and preparation method thereof
CN105369639B (en) * 2014-08-25 2018-07-24 江苏欣隆羽绒有限公司 A kind of bactericidal deodorant and its method of removal natural feather and chemical fiber plus material peculiar smell
CN105803801A (en) * 2014-12-30 2016-07-27 上海水星家用纺织品股份有限公司 Preparation method of composite long-acting antibacterial and anti-mite down fibers
CN104783587A (en) * 2015-04-30 2015-07-22 南通那芙尔服饰有限公司 Method for producing antibacterial and deodorized down quilt
CN104970629B (en) * 2015-06-29 2016-08-24 界首市贝特纺织有限公司 Aloe silk flosssilk wadding health comforter batt preparation method
CN105386131B (en) * 2015-10-15 2017-11-17 莫文油 Eider down goes to obstruct decontamination system
CN107022825A (en) * 2016-01-29 2017-08-08 上海水星家用纺织品股份有限公司 A kind of preparation method of eider down and tencel mixture
CN106724483A (en) * 2017-01-24 2017-05-31 安徽省宇鸿纺织工艺制品有限公司 health-care down quilt
CN107663772A (en) * 2017-09-25 2018-02-06 舒城县玉龙羽绒有限公司 A kind of feather cleaning method
CN108100984A (en) * 2018-01-31 2018-06-01 海宁市锦涤化纤有限公司 A kind of manufacturing method of antibacterial thermal insulating eiderdown quilt
CN110004728B (en) * 2019-04-12 2021-11-02 宁波博洋家纺集团有限公司 Preparation process of fluffy warm-keeping mildew-proof down quilt
CN115233459B (en) * 2022-08-24 2023-04-25 扬州骏翔羽绒制品有限公司 Degreasing and degerming process for white duck velvet

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1492092A (en) * 2003-09-02 2004-04-28 邯郸市雪驰集团有限公司 Antibiotic down and its making method
CN1514056A (en) * 2003-06-30 2004-07-21 良 陈 Processing method for down with antibacterid, antivirus, mould proof, off odour eliminating and health care functions and use
CN2669724Y (en) * 2003-08-07 2005-01-12 邯郸市雪驰集团有限公司 Antibacterial down quilt
CN101611938A (en) * 2008-06-27 2009-12-30 凌颖 A kind of antibacterial down feather and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1514056A (en) * 2003-06-30 2004-07-21 良 陈 Processing method for down with antibacterid, antivirus, mould proof, off odour eliminating and health care functions and use
CN2669724Y (en) * 2003-08-07 2005-01-12 邯郸市雪驰集团有限公司 Antibacterial down quilt
CN1492092A (en) * 2003-09-02 2004-04-28 邯郸市雪驰集团有限公司 Antibiotic down and its making method
CN101611938A (en) * 2008-06-27 2009-12-30 凌颖 A kind of antibacterial down feather and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114224143A (en) * 2021-11-05 2022-03-25 仪征龙兴塑胶有限公司 Highly-waterproof antibacterial breathable sleeping bag and preparation method thereof

Also Published As

Publication number Publication date
CN103190789A (en) 2013-07-10

Similar Documents

Publication Publication Date Title
CN103190789B (en) Manufacturing method of antibacterial and deodorant duvet
CN104783587A (en) Method for producing antibacterial and deodorized down quilt
CN104441158A (en) Processing method of Chinese redwood barks
CN104336252A (en) Preparation method of gardenia tea
CN103046318A (en) Antibiotic finishing process for knitted fabric
CN104746349A (en) Preparation method of negative-ion down feather material and negative-ion down feather quilt
CN109137532A (en) A kind of processing technology of plant odor type antibacterial down feather
KR20130078082A (en) Method of making chrysanthemum tea containing siberian chrysanthemum and chrysanthemumtea thereof
CN103382638A (en) Preparation method of anion down feather material and applications thereof in home-textile products
CN104336200A (en) Preparation method of gardenia black tea
CN104947222A (en) Light and fluffy ecological bacteriostatic down fiber and making method thereof
CN103931800B (en) A kind of processing method of three tealeaves that complete
CN104308926A (en) Wicker treating agent
CN105862434A (en) Production method of antibacterial down fibers
CN106490696A (en) A kind of healthy Chinese herbal medicine socks
CN104947233A (en) Antistatic ecological bacteriostatic down fiber and making method thereof
CN104910815A (en) Method for extracting gelatin from rabbit skin
CN104476640A (en) Rice straw health-care aroma-enhancing anticorrosion modified soaking liquid and use method thereof
CN104674544A (en) Tussah silk fabric functional finishing agent, finishing method and finished tussah silk fabric
CN105803801A (en) Preparation method of composite long-acting antibacterial and anti-mite down fibers
CN103422343B (en) Woolen sweater treating liquid with potassium myristate
KR101535110B1 (en) Padding for keeping warmth using kapok fiber being antifungal-finishing and wool
JP2007138343A (en) Method for treatment of natural antimicrobial agent and antimicrobial fiber material
CN107125384A (en) The preparation method of olive tea
CN103668514B (en) A kind of method of electrostatic spinning prepares the method for nano Ag antibacterial fiber

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant