CN103183998A - Directional reflective material and preparation method thereof - Google Patents
Directional reflective material and preparation method thereof Download PDFInfo
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- CN103183998A CN103183998A CN2013101058039A CN201310105803A CN103183998A CN 103183998 A CN103183998 A CN 103183998A CN 2013101058039 A CN2013101058039 A CN 2013101058039A CN 201310105803 A CN201310105803 A CN 201310105803A CN 103183998 A CN103183998 A CN 103183998A
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Abstract
The invention provides a directional reflective material and a preparation method thereof, and relates to the technical field of reflective materials. The directional reflective material is prepared by compressing a protective layer comprising the components of titanium dioxide, pearl powder, methyl methacrylate, butyl methacrylate, hydroxyl-propyl acrylate and di-tert-pentyl peroxide with a glass bead layer, a support layer and anti-sticking layer through a compacting machine. The reflective material provided by the invention is stronger in reflective degree, wider in reflected visibility, and better in corrosion resistance, can be little affected by climate change, and is suitable for more areas and use in various environments.
Description
Technical field
The present invention relates to the technical field of light reflecting material, relate in particular to a kind of retroreflecting material and preparation method thereof.
Background technology
The various reflecting sign labels that light reflecting material is mainly used in making, number plate of vehicle, safety features etc., play tangible warning function with its bright colour by day, under the situation of night or insufficient light, its bright reflecting effect can strengthen people's recognition capability effectively, sees target clearly, arouse vigilance, thereby avoid accident to take place, reduce loss of life and personal injury, reduce financial loss, become the indispensable security guard of road traffic, tangible social benefit is arranged.Use range relates generally to departments such as public security traffic, traffic superintendance, fire-fighting, railway, colliery, and civilian light reflecting material mainly is reflective cloth, reflective lattice sheet, reflective spray painting cloth etc.
Closely during the last ten years, the production technology develop rapidly of China's tapetum lucidum, economy, engineering level, high-strength reflecting film have formed product line, and automotive number plate is also produced in enormous quantities with tapetum lucidum and truck reflecting marking tapetum lucidum; Not only substituted import, also exported to foreign countries.
Oriented reflection film often is applied to abominable outdoor environment, requires to have better weather and higher directional reflective performance, requires reflective visibility range wide, also can play good reflection action in rugged environment.But the reflective visibility range of light reflecting material of the prior art is narrow.
Summary of the invention
Technical problem to be solved by this invention provides wide retroreflecting material of strong, the reflective visibility range of a kind of weathering resistance and preparation method thereof.
Technical problem to be solved by this invention realizes by the following technical solutions:
A kind of retroreflecting material, matcoveredn, soot layer, reflecting layer, supporting layer and adherent layer is characterized in that, described reflecting layer is made up of the starting material of following weight proportioning:
The composition material optimum weight proportioning in reflecting layer is:
Prepare a kind of method of retroreflecting material, it is characterized in that, described preparation method is as follows:
A, proportion takes by weighing each raw material by weight;
B, the titanium dioxide that weighs up and the pearl powder back that stirs is placed on one side, stand-by;
C, elder generation put into reactor mixing stirring with methyl methacrylate, butyl methacrylate, Propylene glycol monoacrylate, mix to stir after 3 minutes to drip two t-amyl peroxy things and continual the stirring again in reactor;
C, the titanium dioxide and the pearl powder that stir are put in the reactor after dripping two t-amyl peroxy things again, fully stirred, the back insulation that stirs was taken out after 2 hours;
D, the mixture that takes out namely be can be made into the reflecting layer behind the coating machine coating film forming;
E, protective layer, soot layer, reflecting layer, supporting layer and adherent layer press together by press and make light reflecting material.
The described dropping time that drips two t-amyl peroxy things in the reactor is 2 hours.
Beneficial effect of the present invention is: the light reflecting material that the present invention makes, and reflectance is stronger, and the visibility range of reflection is wider, and antiseptic property is good, is subjected to the influence of climate change little, is fit to use under the more regional various environment.
Embodiment
For technique means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below in conjunction with the example of embodiment the present invention is described in further details.
A, proportion takes by weighing each raw material by weight, titanium dioxide 15g, pearl powder 10g, methyl methacrylate 35g, butyl methacrylate 10g, Propylene glycol monoacrylate 15g, two t-amyl peroxy thing 15g;
B, the titanium dioxide that weighs up and the pearl powder back that stirs is placed on one side, stand-by;
C, elder generation put into reactor mixing stirring with methyl methacrylate, butyl methacrylate, Propylene glycol monoacrylate, mix to stir after 3 minutes to drip two t-amyl peroxy things and continual the stirring again in reactor, and the dropping time is 2 hours;
C, the titanium dioxide and the pearl powder that stir are put in the reactor after dripping two t-amyl peroxy things again, fully stirred, the back insulation that stirs was taken out after 2 hours;
D, the mixture that takes out namely be can be made into the reflecting layer behind the coating machine coating film forming;
E, protective layer, soot layer, reflecting layer, supporting layer and adherent layer press together by press and make light reflecting material.
More than show and described ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that describes in above-described embodiment and the specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (3)
3. prepare the method for a kind of retroreflecting material as claimed in claim 1 or 2, it is characterized in that, described preparation method is as follows:
A, proportion takes by weighing each raw material by weight;
B, the titanium dioxide that weighs up and the pearl powder back that stirs is placed on one side, stand-by;
C, elder generation put into reactor mixing stirring with methyl methacrylate, butyl methacrylate, Propylene glycol monoacrylate, mix to stir after 3 minutes to drip two t-amyl peroxy things and continual the stirring again in reactor;
C, the titanium dioxide and the pearl powder that stir are put in the reactor after dripping two t-amyl peroxy things again, fully stirred, the back insulation that stirs was taken out after 2 hours;
D, the mixture that takes out namely be can be made into the reflecting layer behind the coating machine coating film forming;
E, protective layer, soot layer, reflecting layer, supporting layer and adherent layer press together by press and make light reflecting material.
3, the preparation method of a kind of retroreflecting material according to claim 3 is characterized in that: the described dropping time that drips two t-amyl peroxy things in the reactor is 2 hours.
Priority Applications (1)
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CN2013101058039A CN103183998A (en) | 2013-03-28 | 2013-03-28 | Directional reflective material and preparation method thereof |
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CN2013101058039A CN103183998A (en) | 2013-03-28 | 2013-03-28 | Directional reflective material and preparation method thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106019437A (en) * | 2016-08-08 | 2016-10-12 | 浙江万基光学有限公司 | Corrosion-resistant novel reflecting material and preparation method thereof |
CN106019438A (en) * | 2016-08-08 | 2016-10-12 | 浙江万基光学有限公司 | Reflecting material based on modified titanium dioxide and preparation method of reflecting material |
CN107286374A (en) * | 2017-08-02 | 2017-10-24 | 合肥市大卓电力有限责任公司 | A kind of preparation method of reflectorized material on power equipment |
CN109164522A (en) * | 2018-09-04 | 2019-01-08 | 安徽新恒辉反光材料有限公司 | A kind of wide cut permeability type reflectorized material and preparation method thereof |
CN109181192A (en) * | 2018-09-03 | 2019-01-11 | 安徽新恒辉反光材料有限公司 | A kind of roads reflecting material and preparation method thereof |
CN109880415A (en) * | 2019-03-25 | 2019-06-14 | 国网河南省电力公司社旗县供电公司 | A kind of electric power mark reflectorized material |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4104102A (en) * | 1975-02-24 | 1978-08-01 | Morgan Adhesives Company | Method of making a retroreflective laminate |
CN101819291A (en) * | 2010-04-20 | 2010-09-01 | 王默文 | Reflective material, reflective membrane, reflective board and preparation method thereof |
CN102417325A (en) * | 2011-08-09 | 2012-04-18 | 重庆市智翔铺道技术工程有限公司 | Tunnel bituminous pavement clearing functional layer |
CN102879843A (en) * | 2012-10-11 | 2013-01-16 | 常州市日月反光材料有限公司 | Reflecting film |
-
2013
- 2013-03-28 CN CN2013101058039A patent/CN103183998A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4104102A (en) * | 1975-02-24 | 1978-08-01 | Morgan Adhesives Company | Method of making a retroreflective laminate |
CN101819291A (en) * | 2010-04-20 | 2010-09-01 | 王默文 | Reflective material, reflective membrane, reflective board and preparation method thereof |
CN102417325A (en) * | 2011-08-09 | 2012-04-18 | 重庆市智翔铺道技术工程有限公司 | Tunnel bituminous pavement clearing functional layer |
CN102879843A (en) * | 2012-10-11 | 2013-01-16 | 常州市日月反光材料有限公司 | Reflecting film |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106019437A (en) * | 2016-08-08 | 2016-10-12 | 浙江万基光学有限公司 | Corrosion-resistant novel reflecting material and preparation method thereof |
CN106019438A (en) * | 2016-08-08 | 2016-10-12 | 浙江万基光学有限公司 | Reflecting material based on modified titanium dioxide and preparation method of reflecting material |
CN106019438B (en) * | 2016-08-08 | 2019-03-12 | 浙江万基光学有限公司 | A kind of reflectorized material and preparation method thereof based on modified titanium |
CN106019437B (en) * | 2016-08-08 | 2019-06-07 | 浙江万基光学有限公司 | A kind of corrosion resistant Novel light-reflecting material and preparation method thereof |
CN107286374A (en) * | 2017-08-02 | 2017-10-24 | 合肥市大卓电力有限责任公司 | A kind of preparation method of reflectorized material on power equipment |
CN109181192A (en) * | 2018-09-03 | 2019-01-11 | 安徽新恒辉反光材料有限公司 | A kind of roads reflecting material and preparation method thereof |
CN109164522A (en) * | 2018-09-04 | 2019-01-08 | 安徽新恒辉反光材料有限公司 | A kind of wide cut permeability type reflectorized material and preparation method thereof |
CN109880415A (en) * | 2019-03-25 | 2019-06-14 | 国网河南省电力公司社旗县供电公司 | A kind of electric power mark reflectorized material |
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Application publication date: 20130703 |