CN103175754A - Physical detection method for quality of lime and light calcined dolomite - Google Patents
Physical detection method for quality of lime and light calcined dolomite Download PDFInfo
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- CN103175754A CN103175754A CN2013100970253A CN201310097025A CN103175754A CN 103175754 A CN103175754 A CN 103175754A CN 2013100970253 A CN2013100970253 A CN 2013100970253A CN 201310097025 A CN201310097025 A CN 201310097025A CN 103175754 A CN103175754 A CN 103175754A
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- light dolomite
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Abstract
The invention provides a physical detection method for the quality of lime and light calcined dolomite, which is implemented through calculating the physical and chemical indexes of igloss, CaO, and activity of clinkers according to the corresponding relation between the volume density of clinkers after raw stones in lime and light calcined dolomite are completely decomposed and the igloss, CaO and MgO contents thereof, so that the physical detection of quality indexes of lime and light calcined dolomite is rapidly implemented, thereby timely providing the physical detection data of the quality of lime and light calcined dolomite for production sites, providing reliable basis for the quality control of production teams and the guidance of on-site production process parameter adjustment, and guaranteeing the stable control of product quality. Meanwhile, the phenomena of manually-operated sampling and nonstandard detection are avoided, the production scheduling procedure is simplified, the working efficiency and management control level are improved, and the efficient operation of production is ensured.
Description
Technical field
The invention belongs to inspection technology field relates in particular to the on-the-spot rapid physical detection method of a kind of lime or light dolomite quality.
Background technology
Traditional lime or light dolomite quality testing are mainly the methods of employingization check analysis, this off-line quality analysis control model, analytical equipment used is away from the production scene, its quality testing technique, means and equipment are serious to lag behind, detect data feedback oversize to the time cycle of production scene, can't satisfy the actual production technological equipment to the requirement of the online real-time measure and control of product quality at all.Especially catastrophic fluctuation appears when abnormal when product quality, the foundation of relevant quality testing data as Scientific Regulation can not be provided in time, exactly, in time instruct and adjust the produced on-site technological parameter, can only conjesture to adjust with subjectivity blindly, thereby cause the out of control of product quality, have a strong impact on the stability of product quality, restricted the rapidly and efficiently operation of rhythm of production, even caused serious economic loss because of product quality problem.
Summary of the invention
The present invention aims to provide the physical detection methods of a kind of lime or light dolomite quality, thereby provide the quality testing data for the scene quickly and accurately, in time instruct and adjust the produced on-site technological parameter, guarantee the stable control of product quality and the efficient operation of production.
For this reason, the technical solution taked of the present invention is:
The physical detection methods of a kind of lime, light dolomite quality, it is characterized in that, according to the corresponding relation of giving birth to stone in lime or light dolomite and decompose fully the size of rear grog volume density and its igloss, CaO, MgO content, extrapolate igloss, the CaO of grog, the physical and chemical index of activity degree, realize that the rapid physical of lime or light dolomite quality detects; Its concrete grammar and step are:
1, randomly draw lime or the light dolomite sample that a certain amount of particle size range is evenly distributed in each grade of 30-70mm, and guarantee that lime or light dolomite sample have certain representativeness on grade;
2, with balance, lime or light dolomite sample are weighed, obtain the weight of lime or light dolomite sample;
3, the lime after weighing or light dolomite sample are packed in thin plastic packaging bag, seal after evacuation of air, again lime or the light dolomite sample plastic packaging bag of sealing are put into respectively measuring tank after being filled with water, measure one by one the volume of lime or light dolomite sample;
4, according to the weight and volume of step (2), (3) detection, calculate respectively the volume density of each lime or light dolomite sample;
5, use fluorescence detection to detect the CaO content of each lime or light dolomite sample, detect at least 2 points at every turn;
6, in on-the-spot a period of time of intercepting, lime or the light dolomite of actual production is in kind, the intercepting number of times repeats more than 100 times, lime or light dolomite to each grade detect respectively according to step (1)-(5), use MINITAB software to carry out data regression, obtain the corresponding relation of each sample CaO content and volume density, and make corresponding table;
7, the weight, volume and the volume density that step (1)-(4) are detected are applied to commercial production as foundation.
Beneficial effect of the present invention is:
The present invention is according to the corresponding relation of giving birth to stone in lime or light dolomite and decompose fully the size of rear grog volume density and its igloss, CaO, MgO content, extrapolate fast igloss, the CaO of grog, the physical and chemical index of activity degree, thereby the physical detection data of lime or light dolomite quality are provided for the production scene, for the quality control of production team provides reliable basis with in time instructing and adjusting the produced on-site technological parameter, guaranteed the stable control of product quality.Simultaneously, can avoid the manually-operated sampling and detect non-standard phenomena, simplifying the production scheduling program, increase work efficiency and manage the control level, guaranteeing the efficient operation of producing.
Embodiment
The physical detection methods of lime of the present invention, light dolomite quality, mainly according to the corresponding relation of giving birth to stone in lime or light dolomite and decompose fully the size of rear grog volume density and its igloss, CaO, MgO content, extrapolate igloss, the CaO of grog, the physical and chemical index of activity degree, realize that the rapid physical of lime or light dolomite quality detects.The invention will be further described below in conjunction with embodiment.
Embodiment 1:
The concrete steps of lime physical detection methods are:
1, randomly draw a certain amount of particle size range at each grade lime sample of 30-70mm, and guarantee that the lime sample has certain representativeness on grade.
2, with balance, each grade lime sample is weighed, obtain the weight of each lime sample.
3, in the lime sample after weighing is packed thin plastic packaging bag into, seal after evacuation of air, then the lime sample plastic packaging bag of sealing is put into respectively measuring tank after being filled with water, measure one by one the volume of lime sample.
4, according to step 2,3 weight and volumes that detect, calculate respectively the volume density of each lime sample.
5, use fluorescence detection to detect the CaO content of each lime sample, detect 3 points at every turn.
6, the lime of actual production in on-the-spot a period of time of intercepting, the intercepting number of times repeats 110 times, and the lime of each grade is detected respectively according to step 1-5, uses MINITAB software to carry out data regression, obtain the corresponding relation of each sample CaO content and volume density, and make corresponding table.
7, the weight, volume and the volume density that step 1-4 are detected are applied in on-the-spot actual production control as lime quality control foundation.
Embodiment 2:
The concrete steps of light dolomite physical detection methods are:
1, randomly draw a certain amount of particle size range at each grade light dolomite sample of 30-70mm, and guarantee that the light dolomite sample has certain representativeness on grade.
2, with balance, each grade light dolomite sample is weighed, obtain the weight of each light dolomite sample.
3, in the light dolomite sample after weighing is packed thin plastic packaging bag into, seal after evacuation of air, then the light dolomite sample plastic packaging bag of sealing is put into respectively measuring tank after being filled with water, measure one by one the volume of light dolomite sample.
4, according to step 2,3 weight and volumes that detect, calculate respectively the volume density of each light dolomite sample.
5, use fluorescence detection to detect the CaO content of each light dolomite sample, detect 5 points at every turn.
6, the light dolomite of actual production in on-the-spot a period of time of intercepting, the intercepting number of times repeats 105 times, light dolomite to each grade detects respectively according to step 1-5, use MINITAB software to carry out data regression, obtain the corresponding relation of each sample CaO content and volume density, and make corresponding table.
7, the weight, volume and the volume density that step 1-4 are detected, as the quality of light dolomite according to being applied to during on-the-spot actual production controls.
Claims (1)
1. the physical detection methods of a lime, light dolomite quality, it is characterized in that, according to the corresponding relation of giving birth to stone in lime or light dolomite and decompose fully the size of rear grog volume density and its igloss, CaO, MgO content, extrapolate igloss, the CaO of grog, the physical and chemical index of activity degree, realize that the rapid physical of lime or light dolomite quality detects; Its concrete grammar and step are:
(1), randomly draw lime or light dolomite sample that a certain amount of particle size range is evenly distributed in each grade of 30-70mm, and guarantee that lime or light dolomite sample have certain representativeness on grade;
(2), with balance, lime or light dolomite sample are weighed, obtain the weight of lime or light dolomite sample;
(3), the lime after weighing or light dolomite sample are packed in thin plastic packaging bag, seal after evacuation of air, again lime or the light dolomite sample plastic packaging bag of sealing are put into respectively measuring tank after being filled with water, measure one by one the volume of lime or light dolomite sample;
(4), according to the weight and volume that step (2), (3) detect, calculate respectively the volume density of each lime or light dolomite sample;
(5), use fluorescence detection to detect the CaO content of each lime or light dolomite sample, detect at least 2 points at every turn;
(6), in on-the-spot a period of time of intercepting, lime or the light dolomite of actual production is in kind, the intercepting number of times repeats more than 100 times, lime or light dolomite to each grade detect respectively according to step (1)-(5), use MINITAB software to carry out data regression, obtain the corresponding relation of each sample CaO content and volume density, and make corresponding table;
(7), weight, volume and volume density that step (1)-(4) are detected, as according to being applied to commercial production.
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101639449A (en) * | 2009-08-27 | 2010-02-03 | 武汉钢铁(集团)公司 | Method for rapidly detecting main component in active lime and passivated lime |
CN101710110A (en) * | 2009-12-17 | 2010-05-19 | 北京博奇电力科技有限公司 | Method for determining contents of active CaO and MgO in limestone for wet-method flue gas desulphurization |
CN102735820A (en) * | 2012-07-06 | 2012-10-17 | 武汉钢铁(集团)公司 | Method for analyzing limestone and dolomite samples at low cost |
CN102809517A (en) * | 2011-05-30 | 2012-12-05 | 上海宝钢工业检测公司 | Application of barrate strength test method in detection of barrate performance of dolomite or limestone |
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2013
- 2013-03-26 CN CN2013100970253A patent/CN103175754A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101639449A (en) * | 2009-08-27 | 2010-02-03 | 武汉钢铁(集团)公司 | Method for rapidly detecting main component in active lime and passivated lime |
CN101710110A (en) * | 2009-12-17 | 2010-05-19 | 北京博奇电力科技有限公司 | Method for determining contents of active CaO and MgO in limestone for wet-method flue gas desulphurization |
CN102809517A (en) * | 2011-05-30 | 2012-12-05 | 上海宝钢工业检测公司 | Application of barrate strength test method in detection of barrate performance of dolomite or limestone |
CN102735820A (en) * | 2012-07-06 | 2012-10-17 | 武汉钢铁(集团)公司 | Method for analyzing limestone and dolomite samples at low cost |
Non-Patent Citations (1)
Title |
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张会兵等: "回转窑轻烧白云石质量的在线检测与控制", 《冶金分析》, vol. 24, 31 October 2004 (2004-10-31), pages 767 - 769 * |
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Application publication date: 20130626 |