CN103111087A - Extraction device of plant active ingredient - Google Patents
Extraction device of plant active ingredient Download PDFInfo
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- CN103111087A CN103111087A CN2013100805716A CN201310080571A CN103111087A CN 103111087 A CN103111087 A CN 103111087A CN 2013100805716 A CN2013100805716 A CN 2013100805716A CN 201310080571 A CN201310080571 A CN 201310080571A CN 103111087 A CN103111087 A CN 103111087A
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Abstract
The invention discloses an extraction device of a plant active ingredient. The device comprises a homogenate equipment tank body (1) and an end cover arranged at the upper end, wherein the end cover (13) and the homogenate equipment tank body (1) are sealed through a C-shaped clamp and a gasket; a feed funnel (12), an anchor agitator (6), a high-speed shearing agitator (9) and an ultrasonic generator (8) are mounted on the end cover (13); an agitating paddle of the anchor agitator (6), the high-speed shearing agitator (9) and a probe (10) of the ultrasonic generator all extend into a working cavity of the homogenate equipment tank body (1) from the end cover (13); the anchor agitator (6) comprises a motor (7) providing power, a rotation shaft and an agitating paddle; the high-speed shearing agitator (9) and the probe (10) of the ultrasonic generator are located between the agitating paddle and the rotation shaft; and a detachable blade (11) is mounted on the rotation shaft. The device disclosed by the invention has a simple structure and is easy to clean; and the working efficiency is high, and the operation range is wide.
Description
Technical field
The present invention relates to a kind of chemical extraction device, be specifically related to a kind of extraction element of effective ingredients in plant.
Background technology
The extract of effective ingredients in plant has larger economic worth, orange peel essential oil for example, and little algae oil, Rosa Damascana, and the effective effective component in rare Chinese herbal medicine, they are widely used in the industries such as medicine, cosmetics, food.Effective ingredients in plant is mainly the saturated and unrighted acid (also referred to as thick grease) of C14-18, is to be completed by extraction element for the extraction of effective ingredients in plant, and the quality of the performance of extraction element is vital factor in producing.
Yet the operating efficiency of the extraction element of prior art is all lower, produces length consuming time, has increased production cost.Simultaneously, the extraction element of prior art usually can only be used for certain specific raw material and extract specific extract, and in process of production, the difference of the active ingredient that usually will extract according to raw material and wish adopts different extraction elements.
Summary of the invention
In order to solve the problem of above-mentioned existence, the object of the present invention is to provide a kind of extraction element of effective ingredients in plant, this device adopts the fixedly tactic pattern of end cap, is beneficial to replacing, cleaning and the raw-material interpolation of parts; At end cap welding liquid make-up charging aperture, be convenient to add solvent in leaching process; The ultrasonic extraction technology is combined in extraction element, is conducive to the simplification of separating step; Adopt circulation, to accelerate leaching process, raise the efficiency, fall its property of medicine of better maintenance for rare Chinese herbal medicine.This device jet strengthened and ultrasonic cavitation reinforcement coupling with high speed shear simultaneously, apply in the extraction of plant active principle, adopt stirring at low speed and low velocity shear effect, structure refinement is delivered in the useful effect zone, utilize ultrasonic technology and high speed shear, destroy rapidly eucaryotic cell structure, active ingredient is discharged.
The present invention is achieved by the following technical solutions:
The extraction element of effective ingredients in plant provided by the invention comprises the end cap 13 that homogenate equipment tank body 1 and its upper end arrange, and described end cap 13, is characterized in that by C type folder and gasket seal with homogenate equipment tank body 1:
Described loading hopper 12, anchor agitator 6, high speed shear agitator 9 and the supersonic generator 8 of being equipped with on end cap 13; The probe 10 of the paddle of described anchor agitator 6, high speed shear agitator 9 and supersonic generator all stretches in the working chamber of homogenate equipment tank body 1 from described end cap 13; Described anchor agitator 6 is included as its motor that power is provided 7, turning cylinder and paddle, and the paddle of described anchor agitator 6 is fixedly connected with motor 7 by turning cylinder; Described paddle is " U " shape paddle, and described high speed shear agitator 9 and supersonic generator probe 10 are between described paddle and power transmission shaft; Dismountable blade 11 is installed on described turning cylinder.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described loading hopper 12 is welded on end cap 13; Its lower end diameter is 10-25mm, the middle globe valve that connects; Described loading hopper 12 materials are stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the lower end of described motor 7 is welded on end cap 13 centers.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described high speed shear agitator 9 and supersonic generator 8 are connected on end cap 13 by end face seal.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the diameter of described high speed shear agitator 9 outer shaft stators is 20mm, and there are 6 rectangular teeths the end, and long is 3.4mm, wide 2.0mm, high 7.1mm; Interior axle rotor is 3 teeth, the long 2.51mm of the upper section of tooth, and the long 6.1mm of lower section, width 2.5mm, height 8.2mm, the gap of rotor is 0.4mm; The material of described fast shearing stirrer 9 is selected from stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described supersonic generator probe 10 diameters are 18-24mm, and material is selected from stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the length of described blade 11 is 1/3 of homogenate equipment tank body radius, and the width of blade is 1-2.5cm; Described blade is positioned at 1/2-2/3 tank body total height at the bottom of homogenate equipment tank body 1 tank; Described blade material is selected from stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described high speed shear agitator 9 and ultrasonic disperser probe 10 symmetries are fixedly installed in apart from end cap 13 center 1/7-6/7 end cap radius; Described high speed shear stirs 9 and the 10 oblique installations of ultrasonic disperser probe, with the counterclockwise angle of tank body center line be the 5-15 degree; It is 1/8 distance of the total height of tank body at the bottom of tank that described high speed shear stirs 9 bottoms, and described ultrasonic disperser probe 10 bottoms are 3/8 distance of the total height of tank body apart from pot bottom.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the tank skin of described homogenate equipment tank body 1 is provided with insulation jacket 3; Described insulation jacket 3 is provided with water inlet 4 and discharge outlet 5; The lower end of described homogenate equipment tank body 1 is provided with the discharging opening 2 with its internal communication, and described discharging opening 2 is provided with discharge valve.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described homogenate equipment tank body 1 is dismountable tank body, and it is connected with lowering or hoisting gear; Described tank diameter and aspect ratio are 0.6:1-0.8:1.
The invention provides a kind of using method of extraction element of effective ingredients in plant, step is as follows:
The plant that 1) will need to extract cleans up, after the pretreatment size (concrete much scopes), with deionized water mixing match mass ratio be 1:3～1:10, open extraction element C type folder, start lowering or hoisting gear mixture is poured in tank body, rising tank body and sealing;
2) start anchor agitator, rotating speed is 50-250r/min, starts simultaneously circulator bath, and the temperature of controlling mixed material in agitator tank is 0-60 ° of C, opens rotating blade after 1-5min, and it is 50-500r/min that rotating speed is set, and stirs 2-8min;
3) open the high speed shear agitator, open simultaneously supersonic generator, ultrasonic power is set;
4) after the high speed shear agitator stirs 15-30min, stop high speed shear agitator and rotating blade, open charging aperture, add 1/8～2/8 benzinum of tank body cumulative volume, then close charging aperture;
5) after 10-20min is stirred in continuation, stop stirring and ultrasonic generator, extract the upper strata benzinum, lower floor's mixture is discharged by discharging opening;
6) can obtain required active ingredient with the extract decompression distillation is concentrated, described active ingredient is the saturated and unrighted acid of C14-18.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, in step (1), the mixture addition will surpass the height of rotating blade.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, after step (5) continues to stir 10-20min, stop stirring and ultrasonic generator, extract the upper strata benzinum, lower floor's mixture is passed through to start lowering or hoisting gear, take off tank body, pour out mixture.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, active ingredient is water-soluble substances, and extraction step is described step (1) (2) (3) (5) (6).
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, the high speed shear agitator speed is 10000-28000r/min.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, further preferably, the high speed shear agitator speed is 10000-20000r/min.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, supersonic generator power is 50-500w, and frequency is 50-25khz,
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, supersonic generator power is 100-150W.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, the anchor agitator rotating speed is 80-150r/min.
According to the using method of the extraction element that the invention provides a kind of effective ingredients in plant, preferably, the rotating blade rotating speed is 200-350r/min.
According to the extraction element of effective ingredients in plant provided by the invention, mainly comprise a homogenate equipment that is used for destroying plant cell, a circulation that is connected with homogenate equipment, the position lowering or hoisting gear that can adjust tank body.
According to homogenate equipment tank body of the present invention, diameter and aspect ratio are 0.6-0.8, and a lowering or hoisting gear is connected with tank body, tank body can disassemble, and be convenient to it and clean, and the interpolation of material, the tank body material is fiberglass, is beneficial to observe its internal-response state, and the interpolation of material.Tank body lower part is offered a discharging opening, is beneficial to the discharging of its inner material
According to chuck layer of the present invention, its material is fiberglass, wherein walks circulation, is convenient to arrange temperature environment in tank body according to reaction needed, is beneficial to the efficient of extraction.And extract is fresh-keeping, its external circulation.
According to anchor agitator of the present invention, be two paddle, the width of blade is 5-15mm, preferred 10mm is fixed in the upper cover center, bottom 3-7mm at the bottom of the tank, the agitator radius is slightly less than the tank body radius, design benefit: 1) prevent from occurring in whipping process the dead angle; 2) prevent that extract is bonded on tank wall, during work, agitator speed is 50-100r/min, mixes in the destructive power zone of action in order to material is delivered to, and the material of whole agitator is 304 stainless steels.Miniature motor of the present invention is for parts anchor agitator and blade provide power source.
According to high speed shear agitator of the present invention, the diameter of outer shaft stator is 20mm, there are 6 rectangular teeths the end, size: long is the high 7.1mm of the wide 2.0mm of 3.4mm, and interior axle rotor is 3 teeth, the long 2.51mm of the upper section of tooth, the long 6.1mm of lower section, width 2.5mm, height 8.2mm, the gap of rotor is 0.4mm, material 304 stainless steels.
According to supersonic generator probe of the present invention, be the preferred 20mm of 18-24mm, material 304 stainless steels.
Be 4 on chip according to blade of the present invention, the length of blade is that the width of 1/3. blade of tank body radius is 1-2.5cm, and material is 304 stainless steels, is loaded at the bottom of the tank approximately 2/3 left and right of tank body total height, blade adopts Quick-disassembling device to install, and is convenient to it and changes and safeguard.
According to liquid make-up charging aperture of the present invention, as required extract is diluted in leaching process, and the additional charging aperture that extracts solvent, these parts are welded on end cap, lower end diameter is 10-25mm, and the middle globe valve that connects comes gauge tap, and the upper end is connected to a funnel, be convenient to charging, material is 304 stainless steels.
According to end cap of the present invention, material is 304 stainless steels, the high speed shear agitator is connected with supersonic generator and is adopted the end face seal technology to be connected with end cap, charging aperture is welded on end cap, end cap and motor bottom cabinet are welded into an integral body, make whole mechanical damage functional component place close structure.
according to the present invention, anchor agitator is fixed in the upper cover center, bottom 3-7mm high speed shear agitator and ultrasonic disperser probe symmetry at the bottom of the tank are fixedly installed in apart from upper cover vertical center line 1/7-6/7d place, d is the internal diameter of tank body, high speed shear stirs and the oblique installation of ultrasonic disperser probe, setting angle is identical, with the counterclockwise angle of tank body center line be the 5-15 degree, high speed shear agitator bottom is 1/8h at the bottom of tank, supersonic generator probe bottom is 3/8h apart from pot bottom, h is the total height of tank body, blade is installed on apart from pot bottom 1/2h place, wherein upper cover and tank body are by C type folder and gasket seal, symmetrical 6 the C types folder of periphery.
According to the present invention, the adjustable rotating speed of high speed shear agitator is at 10000-28000r/min, preferred rotating speed is 10000r/min, and grade-adjustable has A-G7 grade, and ultrasonic disperser power is 50-500w, frequency is 50-25khz, preferred power is 150W, and the rotating speed of anchor agitator 6 is at 50-250r/min, preferred 80r/min, the rotating speed of blade 11 is at 50-500r/min, preferred rotating speed 200r/min.
The using method of the extraction element of effective ingredients in plant provided by the invention, step is as follows:
The plant that 1) will need to extract cleans up, particle diameter≤6mm after pretreatment, allow desired concn come mixing match 1:3～1:10(mass ratio with deionized water), open C type folder, starting lowering or hoisting gear imports mixture in tank body, cumulative volume will surpass the height of parts 11, rising tank body and sealed shell of tank at least.
2) starting the anchor agitator rotating speed is 50-100r/min, starts simultaneously the temperature 0-60 ° of C that circulator bath is controlled mixed material in agitator tank, opens blade 11 after 3min, and rotating speed is 100-250r/min, stirs 3-15min.
3) open the high speed shear agitator, rotating speed is set to 10000-28000r/min, opens simultaneously supersonic generator, and ultrasonic power is 50-500W.
4) after stirring 15-30min, stop high speed shear agitator 9 and open 12 ball valve with rotating blade 11, add the benzinum (V is the cumulative volume of tank body) of 1/8～2/8V from charging aperture, then close ball valve.
5) after stirring 10-20min, stop, extracting the upper strata benzinum, lower floor's mixture is discharged by 2, or directly start lowering or hoisting gear, tank body is taken off, pour out mixture.
6) if required active ingredient is water-soluble substances, need not to use step 4.
7) the extract decompression distillation can be obtained required concentrated active ingredient, described active ingredient is the saturated and unrighted acid of C14-18.
According to device provided by the invention in the mechanism process, after anchor agitator mixes integral body, the blind spot that has occurred in having avoided stirring, and with the each several part mixture be delivered to the effect effective coverage in, rotating blade adds the disturbance of strong center stirring region on the one hand, with floating or be suspended in the large particle diameter material cutting on top, accelerate the frequency that it is sent to the active region on the other hand.Anchor agitator and blade help out.In the high speed shear zone of action, the fluid rotating speed is high, the mutual friction of iuntercellular phase, or directly impinge upon on the stator and rotor end face, caused by larger extruding and collision, cyto-architectural destruction.The violent change of bubble in ultrasonic cavitation process on the other hand, producing additive effect has turbulence effect, perturbation effect, interfacial effect, the comprehensive effects such as Mohaupt effect make cell be subject to serious damage so that destroy.Synergy and Main Function that both form, thus the chemical composition in cell is released, and directly dissolving, shortened extraction time widely, improves extraction efficiency.The booster action of anchor agitator and blade, the effect of the main destruction cell of high speed shear agitator and ultrasonic disperser probe, consist of this device energy rapid damage eucaryotic cell structure, make chemical composition be released dissolving, the latter extracts under ultrasound environments, utilize the ultrasonic extraction technology also greatly to improve, extraction efficiency, shortening time.
The present invention combines existing ultrasonic technology and high speed shear technology, utilize puddler and supersonic generator to destroy rapidly cell membrane, active ingredient in release cells, the low speed rotation of recycling stirring at low speed oar, make that cell in container obtains fully, effective break process, the method for employing mechanical damage is obtained active ingredient efficiently, rapidly from cell; Insulation jacket can guarantee the temperature of the extract in the fiberglass retort, and the operator can regulate according to the difference of extract the temperature of recirculated water, this makes utilization scope of the present invention wider, can be used for grease and protein extraction, orange peel extraction of essential oil, rose ethereal oil extraction, the extraction of natural plant pigment and the extraction of some Chinese herbal medicine active ingredient of little algae.In sum, the present invention has advantages of that high efficiency, utilization scope are wide.
Beneficial effect of the present invention:
The extraction element of effective ingredients in plant provided by the invention, this device adopts the fixedly tactic pattern of end cap, is beneficial to replacing, cleaning and the raw-material interpolation of parts; At end cap welding liquid make-up charging aperture, be convenient to add solvent in leaching process; The ultrasonic extraction technology is combined in extraction element, is conducive to the simplification of separating step; Adopt circulation, during the rising temperature, can accelerate leaching process, raise the efficiency, reduce temperature for rare Chinese herbal medicine, can keep more fully its property of medicine.This device jet strengthened and ultrasonic cavitation reinforcement coupling with high speed shear simultaneously, apply in the extraction of plant active principle, adopt stirring at low speed and low velocity shear effect, structure refinement is delivered in the useful effect zone, utilizes ultrasonic technology and high speed shear, destroy rapidly eucaryotic cell structure, active ingredient is discharged, dissolving is controlled by circulation in whole process, and in tank body, temperature guarantees the activity of extract.
Description of drawings
Fig. 1 is the structural representation of the extraction element of effective ingredients in plant provided by the invention.
In the drawings: 1-homogenate equipment tank body, 2-discharging opening, 3-insulation jacket, 4-water inlet, 5-discharge outlet, the 6-anchor agitator, 7-motor, 8-supersonic generator, 9-high speed shear agitator, 10-supersonic generator probe, the 11-blade, 12-charging aperture, 13-end cap, 14-lowering or hoisting gear.
The specific embodiment
The present invention is described in detail below in conjunction with accompanying drawing.
As shown in Figure 1, a kind of extraction element of effective ingredients in plant, comprise the end cap 13 that homogenate equipment tank body 1 and its upper end arrange, described end cap 13 by C type folder and gasket seal, is equipped with loading hopper 12, anchor agitator 6, high speed shear agitator 9 and supersonic generator 8 with homogenate equipment tank body 1 on end cap 13; The probe 10 of the paddle of described anchor agitator 6, high speed shear agitator 9 and supersonic generator all stretches in the working chamber of homogenate equipment tank body 1 from described end cap 13; Described anchor agitator 6 is included as its motor that power is provided 7, turning cylinder and paddle, and the paddle of described anchor agitator 6 is fixedly connected with motor 7 by turning cylinder; Described paddle is " U " shape paddle, and described high speed shear agitator 9 and supersonic generator probe 10 are between described paddle and power transmission shaft; Dismountable blade 11 is installed on described turning cylinder.
Embodiment 1: the extraction of grease in chlorella
1) chlorella after concentrating (transferring to corresponding proportioning by reality is required) 1:10(quality is than algae: water) open C type folder, start lowering or hoisting gear, mixture is poured in tank body, cumulative volume is the 2/3V of tank body, then rise tank body and sealed shell of tank.
2) starting the anchor agitator rotating speed is 80r/min, starts simultaneously circulator bath, and the temperature of controlling mixed material in agitator tank is about 60 ° of C, opens rotating blade 11 after 3 minutes, and rotating speed is 150r/min, stirs 5 minutes.
3) open the high speed shear agitator, rotating speed is set to 15000r/min, opens simultaneously supersonic generator, and ultrasonic power is 150W, and frequency is 20KHZ.
4) after work 25min, stop high speed shear agitator 9 and rotating blade 11, the circulation temperature is arranged on about 25 ° of C of room temperature range, open 12 ball valve, add the benzinum (V is the cumulative volume of tank body) of 3/16V from charging aperture, then close ball valve.
5) stir 15min after, stop, extracting the upper strata benzinum, lower floor's mixture is discharged by 2, then benzinum is mixed phase, decompression distillation can obtain required algae oil, then lower floor's mixture washing can be obtained the water soluble protein composition.
Destroy the contrast effect of chlorella structure apparatus of the present invention and other method, wherein be extracted out the aliphatic acid that thick grease is C14-18, after first carrying out esterification, again by chromatography, detect the content of its fatty acid methyl ester, calculate again the total content of grease, and with plant in total content compare, calculate extraction efficiency.
Comparing result:
Embodiment 2: the extraction of orange peel essential oil
1) the orange skin 1:15(quality after concentrating is than orange peel: deionized water) open C type folder, start lowering or hoisting gear, mixture is poured in tank body, cumulative volume is the 3/4V of tank body, then rise tank body and sealed shell of tank.
2) starting the anchor agitator rotating speed is 100r/min, starts simultaneously circulator bath and controls, and in agitator tank, the temperature of mixed material is about 60 ° of C, opens blade 11 after 3 minutes, and rotating speed is 200r/min, stirs 5 minutes.
3) open the high speed shear agitator, rotating speed is set to 15000r/min, opens simultaneously supersonic generator, and ultrasonic power is 200W, and frequency is 20KHZ.
4) after work 30min, stop all parts, at first stop high speed shear agitator 9 and rotating blade 11, then stop high speed shear and ultrasonication, open C type folder, start lowering or hoisting gear, mixture is poured out, or directly got rid of from the bottom, go back at last rotary device, mixture is all carried out isolated by filtration, and then the liquid phase decompression distillation is got final product to get thick tangerine peel essential oil.
The present invention can be used for grease and protein extraction, orange peel extraction of essential oil, rose ethereal oil extraction, the extraction of natural plant pigment and the extraction of some Chinese herbal medicine active ingredient of little algae.
The extraction element of effective ingredients in plant provided by the invention, this device adopts the fixedly tactic pattern of end cap, is beneficial to replacing, cleaning and the raw-material interpolation of parts; At end cap welding liquid make-up charging aperture, be convenient to add solvent in leaching process; The ultrasonic extraction technology is combined in extraction element, is conducive to the simplification of separating step; Adopt circulation, during the rising temperature, can accelerate leaching process, raise the efficiency, reduce temperature for rare Chinese herbal medicine, can keep more fully its property of medicine.This device jet strengthened and ultrasonic cavitation reinforcement coupling with high speed shear simultaneously, apply in the extraction of plant active principle, adopt stirring at low speed and low velocity shear effect, structure refinement is delivered in the useful effect zone, utilizes ultrasonic technology and high speed shear, destroy rapidly eucaryotic cell structure, active ingredient is discharged, dissolving is controlled by circulation in whole process, and in tank body, temperature guarantees the activity of extract.
Claims (10)
1. the extraction element of an effective ingredients in plant, comprise the end cap (13) that homogenate equipment tank body (1) and its upper end arrange, and described end cap (13), is characterized in that by C type folder and gasket seal with homogenate equipment tank body (1):
Described loading hopper (12), anchor agitator (6), high speed shear agitator (9) and the supersonic generator (8) of being equipped with on end cap (13); The probe (10) of the paddle of described anchor agitator (6), high speed shear agitator (9) and supersonic generator all stretches in the working chamber of homogenate equipment tank body (1) from described end cap (13); Described anchor agitator (6) is included as its motor that power is provided (7), turning cylinder and paddle, and the paddle of described anchor agitator (6) is fixedly connected with motor (7) by turning cylinder; Described paddle is " U " shape paddle, and described high speed shear agitator (9) and supersonic generator probe (10) are between described paddle and power transmission shaft; Dismountable blade (11) is installed on described turning cylinder.
2. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described loading hopper (12) is welded on end cap (13); Its lower end diameter is 10-25mm, the middle globe valve that connects; Described loading hopper (12) material is stainless steel.
3. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, the lower end of described motor (7) is welded on end cap (13) center.
4. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described high speed shear agitator (9) and supersonic generator (8) are connected on end cap (13) by end face seal.
5. the extraction element of effective ingredients in plant according to claim 4, is characterized in that, the diameter of described high speed shear agitator (9) outer shaft stator is 20mm, and there are 6 rectangular teeths the end, and long is 3.4mm, wide 2.0mm, high 7.1mm; Interior axle rotor is 3 teeth, the long 2.51mm of the upper section of tooth, and the long 6.1mm of lower section, width 2.5mm, height 8.2mm, the gap of rotor is 0.4mm; The material of described fast shearing stirrer (9) is selected from stainless steel.
6. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described supersonic generator probe (10) diameter is 18-24mm, and material is selected from stainless steel.
7. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, the length of described blade (11) is 1/3 of homogenate equipment tank body radius, and the width of blade is 1-2.5cm; Described blade is positioned at 1/2-2/3 tank body total height at the bottom of homogenate equipment tank body (1) tank; Described blade material is selected from stainless steel.
8. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described high speed shear agitator (9) and ultrasonic disperser probe (10) symmetry is fixedly installed in apart from end cap (13) center 1/7-6/7 end cap radius; Described high speed shear stirs (10) the oblique installation of popping one's head in of (9) and ultrasonic disperser, with the counterclockwise angle of tank body center line be the 5-15 degree; It is 1/8 distance of the total height of tank body at the bottom of tank that described high speed shear stirs (9) bottom, and described ultrasonic disperser probe (10) bottom is 3/8 distance of the total height of tank body apart from pot bottom.
9. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, the tank skin of described homogenate equipment tank body (1) is provided with insulation jacket (3); Described insulation jacket (3) is provided with water inlet (4) and discharge outlet (5); The lower end of described homogenate equipment tank body (1) is provided with the discharging opening (2) with its internal communication, and described discharging opening (2) is provided with discharge valve.
10. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described homogenate equipment tank body (1) is dismountable tank body, and it is connected with lowering or hoisting gear; Described tank diameter and aspect ratio are 0.6:1-0.8:1.
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| CN201310080571.6A CN103111087B (en) | 2013-03-13 | 2013-03-13 | Extraction device of plant active ingredient |
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| CN201310080571.6A CN103111087B (en) | 2013-03-13 | 2013-03-13 | Extraction device of plant active ingredient |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103265645A (en) * | 2013-06-03 | 2013-08-28 | 浙江宇翔生物科技有限公司 | Device and method for extracting algal polysaccharide by ultrasonic-assisted extraction |
| CN108421271A (en) * | 2018-03-22 | 2018-08-21 | 安徽睿知信信息科技有限公司 | A kind of pharmacy extraction inspissator |
| TWI671107B (en) * | 2018-12-20 | 2019-09-11 | 黃長義 | Oscillating device of extraction system |
| CN110559685A (en) * | 2019-09-29 | 2019-12-13 | 贾小军 | High-efficient separation and purification equipment of plant active ingredient |
| CN110605085A (en) * | 2019-09-11 | 2019-12-24 | 陕西羊老大服饰股份有限公司 | Purification equipment for wool and soybean protein fibers |
| CN114949913A (en) * | 2021-06-07 | 2022-08-30 | 台湾嘉义大学 | Ultrasonic extraction system and equipment thereof |
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| CN202044951U (en) * | 2011-03-22 | 2011-11-23 | 湖北中烟工业有限责任公司 | Efficient extracting device for extracting active ingredients of plants |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103265645A (en) * | 2013-06-03 | 2013-08-28 | 浙江宇翔生物科技有限公司 | Device and method for extracting algal polysaccharide by ultrasonic-assisted extraction |
| CN103265645B (en) * | 2013-06-03 | 2016-01-20 | 浙江宇翔生物科技有限公司 | A kind of device and method of ultrasonic-assisted extraction Sargassum polysaccharides |
| CN108421271A (en) * | 2018-03-22 | 2018-08-21 | 安徽睿知信信息科技有限公司 | A kind of pharmacy extraction inspissator |
| TWI671107B (en) * | 2018-12-20 | 2019-09-11 | 黃長義 | Oscillating device of extraction system |
| CN110605085A (en) * | 2019-09-11 | 2019-12-24 | 陕西羊老大服饰股份有限公司 | Purification equipment for wool and soybean protein fibers |
| CN110559685A (en) * | 2019-09-29 | 2019-12-13 | 贾小军 | High-efficient separation and purification equipment of plant active ingredient |
| CN114949913A (en) * | 2021-06-07 | 2022-08-30 | 台湾嘉义大学 | Ultrasonic extraction system and equipment thereof |
| TWI783508B (en) * | 2021-06-07 | 2022-11-11 | 國立嘉義大學 | Ultrasonic extraction system and its equipment |
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