CN202044951U - Efficient extracting device for extracting active ingredients of plants - Google Patents

Efficient extracting device for extracting active ingredients of plants Download PDF

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Publication number
CN202044951U
CN202044951U CN2011200762628U CN201120076262U CN202044951U CN 202044951 U CN202044951 U CN 202044951U CN 2011200762628 U CN2011200762628 U CN 2011200762628U CN 201120076262 U CN201120076262 U CN 201120076262U CN 202044951 U CN202044951 U CN 202044951U
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reaction tank
active ingredients
bottom cover
extraction
extraction device
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肜霖
黄龙
张敦铁
吴昭
邵兴伟
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China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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Abstract

本实用新型公开了一种提取植物有效成分的高效提取装置,属于化学提取设备领域。提取植物有效成分的高效提取装置的反应罐的罐体四周设置有用蒸汽加热的夹层,所述反应罐内壁上设置有超声波发生器,所述反应罐的中央设置有搅拌器,搅拌器的下端设置有搅拌刀片,所述反应罐的顶盖上设置有进料口和排气孔,所述反应罐的底部设置有过滤网和底盖,底盖中央设置出料管。所述的过滤网是20~40目的。所述的底盖是与罐体活动连接的。所述的出料管直径为10cm~20cm。本实用新型设计合理,结构简单,进出料快速方便,提取效率高,生产周期短,可单批次多次提取,且适合大规模生产。

Figure 201120076262

The utility model discloses a high-efficiency extraction device for extracting plant effective components, which belongs to the field of chemical extraction equipment. The reaction tank of the high-efficiency extraction device for extracting plant active ingredients is equipped with an interlayer heated by steam around the tank body, the inner wall of the reaction tank is provided with an ultrasonic generator, the center of the reaction tank is provided with an agitator, and the lower end of the agitator is provided There is a stirring blade, the top cover of the reaction tank is provided with a feed port and an exhaust hole, the bottom of the reaction tank is provided with a filter screen and a bottom cover, and a discharge pipe is provided in the center of the bottom cover. The filter screen is 20-40 mesh. The bottom cover is movably connected with the tank body. The diameter of the discharge pipe is 10cm-20cm. The utility model has the advantages of reasonable design, simple structure, fast and convenient feeding and discharging, high extraction efficiency, short production cycle, multiple extractions in a single batch, and is suitable for large-scale production.

Figure 201120076262

Description

提取植物有效成分的高效提取装置High-efficiency extraction device for extracting active ingredients of plants

技术领域 technical field

本实用新型属于化学提取设备领域,具体涉及提高天然植物原料有效成分提取效率的提取设备。The utility model belongs to the field of chemical extraction equipment, in particular to extraction equipment for improving the extraction efficiency of natural plant raw material active ingredients.

背景技术 Background technique

现有技术中,天然植物及中草药被越来越多的用于医药、食品、香料等各种领域,对天然植物原料有效成分的提取是其重要的方式和环节。目前对天然植物的提取主要是采用有机溶剂加热浸提,这种方式提取效率不高,时间、能源消耗大,往往不仅造成植物原料中热敏性成分的破坏,还带出很多杂质,增加了后续分离纯化的处理过程,增加了消耗和生产成本。超声波提取技术是利用超声波特殊的强纵向振动,高速冲击破碎、空化效应搅拌及加热等物理性能,加速有效成分的溶解,提高有效成分的提取率,具有提取时间短、产率高、不破坏有效成分、无污染等优点,在提取天然植物及中草药有效成分方面的应用越来越广泛。超声波的工业化设备目前正处于发展阶段,虽然已有商业化的设备,还有很多相关的专利成果,但总体来说还有许多不完善的地方。如专利CN244839Y和专利CN2015585669U将超声波发生器放置在设备的底端,原料容易沉淀在底端而影响超声波工作效果,出料口大小受局限,排渣困难。专利CN201333400Y则较好的解决了这个问题,但该设备仅仅是具有超声提取功能的设备,原料需进行粉碎前处理。In the prior art, natural plants and Chinese herbal medicines are increasingly used in various fields such as medicine, food, and spices, and the extraction of active ingredients from natural plant materials is an important method and link. At present, natural plants are mainly extracted by heating with organic solvents. This method is not efficient, consumes a lot of time and energy, and often not only causes damage to heat-sensitive components in plant materials, but also brings out many impurities, which increases the subsequent separation. The purification process increases consumption and production costs. Ultrasonic extraction technology is the use of ultrasonic special strong longitudinal vibration, high-speed impact crushing, cavitation effect stirring and heating and other physical properties to accelerate the dissolution of active ingredients, improve the extraction rate of active ingredients, with short extraction time, high yield, non-destructive The advantages of active ingredients, no pollution, etc., are more and more widely used in extracting active ingredients of natural plants and Chinese herbal medicines. Ultrasonic industrial equipment is currently in the development stage. Although there are already commercial equipment and many related patent achievements, there are still many imperfections in general. For example, in patent CN244839Y and patent CN2015585669U, the ultrasonic generator is placed at the bottom of the equipment. The raw materials are easy to settle at the bottom and affect the working effect of the ultrasonic wave. The size of the discharge port is limited and the slag discharge is difficult. Patent CN201333400Y solves this problem better, but this equipment is only equipment with ultrasonic extraction function, and the raw materials need to be pulverized before treatment.

实用新型内容 Utility model content

针对现有技术的上述不足,本实用新型要解决的技术问题是提供一种提取植物有效成分的高效提取装置,将原料的破碎、浸提和超声波提取融为一体,减少了中间环节,节约提取时间,降低生产成本,提高了原料有效成分的提取效率。Aiming at the above-mentioned deficiencies of the prior art, the technical problem to be solved by the utility model is to provide a high-efficiency extraction device for extracting active ingredients of plants, which integrates the crushing, extraction and ultrasonic extraction of raw materials, reduces intermediate links, and saves extraction time, reduce production costs, and improve the extraction efficiency of active ingredients in raw materials.

本实用新型的技术方案是:提取植物有效成分的高效提取装置的反应罐的罐体四周设置有用蒸汽加热的夹层,所述反应罐内壁上设置有超声波发生器,所述反应罐的中央设置有搅拌器,搅拌器的下端设置有搅拌刀片,所述反应罐的顶盖上设置有进料口和排气孔,所述反应罐的底部设置有过滤网和底盖,底盖中央设置出料管。所述的过滤网是20~40目的。所述的底盖是与罐体活动连接的。所述的出料管直径为10cm~20cm。The technical scheme of the utility model is: an interlayer heated by steam is arranged around the tank body of the reaction tank of the high-efficiency extraction device for extracting active ingredients of plants, the inner wall of the reaction tank is provided with an ultrasonic generator, and the center of the reaction tank is provided with Stirrer, the lower end of the stirrer is provided with a stirring blade, the top cover of the reaction tank is provided with a feed port and an exhaust hole, the bottom of the reaction tank is provided with a filter screen and a bottom cover, and the center of the bottom cover is provided with a discharge Tube. The filter screen is 20-40 mesh. The bottom cover is movably connected with the tank body. The diameter of the discharge pipe is 10cm-20cm.

本实用新型设计合理,结构简单,进出料快速方便,提取效率高,生产周期短,可单批次多次提取,且适合大规模生产。The utility model has the advantages of reasonable design, simple structure, fast and convenient feeding and discharging, high extraction efficiency, short production cycle, multiple extractions in a single batch, and is suitable for large-scale production.

附图说明 Description of drawings

附图1是本实用新型一实施例结构示意图。Accompanying drawing 1 is the structural representation of an embodiment of the utility model.

附图中标记分述如下:1-搅拌器;2-排气孔;3-搅拌刀片;4-进料口;5-夹层;6-超声波发生器;7-反应罐;8-过滤网;9-底盖;10-出料管;11-阀门。The marks in the accompanying drawings are described as follows: 1-stirrer; 2-venting hole; 3-stirring blade; 4-feeding port; 5-interlayer; 9-bottom cover; 10-discharging pipe; 11-valve.

具体实施方式 Detailed ways

下面结合附图对本实用新型的具体实施方式作进一步详细的描述。请参见附图1,将天然植物原料通过进料口4加入反应罐7内,加入浸提溶剂,关闭进料口,夹层5通蒸汽进行加热,开启搅拌器1,转速为30~100转/min,3~10min后,关闭搅拌器1,开启超声波发生装置6,浸提时间1~30min,罐内压力通过排气口2进行调节。提取完毕,打开阀门11,将经初滤提取液通过出料管10收集进入下一道工序,打开底盖9,打开过滤器8,出渣。机械搅拌采用变频调速,根据原料的坚硬程度来选择调节;搅拌头采用刀片,用于打碎物料;超声波发生器安装在罐体壁上,便于超声波充分发挥作用;采用打开底盖排渣,不易堵塞。Below in conjunction with accompanying drawing, the specific embodiment of the present utility model is described in further detail. Please refer to accompanying drawing 1, add natural plant raw material in reaction tank 7 through feed inlet 4, add leaching solvent, close feed inlet, interlayer 5 passes steam to heat, open agitator 1, and rotating speed is 30~100 rpm min, after 3 to 10 minutes, turn off the agitator 1, turn on the ultrasonic generator 6, the extraction time is 1 to 30 minutes, and the pressure in the tank is adjusted through the exhaust port 2. After the extraction is completed, the valve 11 is opened, and the primary filtered extract is collected through the discharge pipe 10 to enter the next process, the bottom cover 9 is opened, the filter 8 is opened, and the slag is discharged. The mechanical stirring adopts frequency conversion speed regulation, which is selected and adjusted according to the hardness of the raw materials; the stirring head uses blades to break the materials; the ultrasonic generator is installed on the tank wall to facilitate the full use of ultrasonic waves; the slag is discharged by opening the bottom cover, Not easy to clog.

本实用新型与现有技术相比有以下优点:Compared with the prior art, the utility model has the following advantages:

1、将原料破碎、加热浸提、超声提取融合成为一个整体,减少了中间环节,节约提取时间,降低生产成本,提高了原料有效成分的提取效率;1. Combining raw material crushing, heating extraction, and ultrasonic extraction into a whole, reducing intermediate links, saving extraction time, reducing production costs, and improving the extraction efficiency of active ingredients of raw materials;

2、搅拌刀片在旋转过程中,涡流带动原料,经过刀片,被切割研磨粉碎,免去了干燥粉碎步骤,减少生产区粉尘污染,提高工作效率;2. During the rotation process of the mixing blade, the eddy current drives the raw material, passes through the blade, is cut, ground and crushed, eliminating the need for drying and crushing steps, reducing dust pollution in the production area, and improving work efficiency;

3、加热搅拌提取和超声提取既可同时使用,也可分别使用,扩大了原料使用范围;3. Heating and stirring extraction and ultrasonic extraction can be used at the same time or separately, which expands the scope of use of raw materials;

4、增大出料管口径,有效防止管道堵塞,且设备清洗方便。4. Increase the caliber of the discharge pipe to effectively prevent pipe blockage, and the equipment is easy to clean.

5、设备结构简单,操作方便,原料应用广泛,进出料快速方便,提取效率高,生产周期短,单批次多次提取,适合大规模生产。5. The equipment has simple structure, convenient operation, wide application of raw materials, fast and convenient feeding and discharging, high extraction efficiency, short production cycle, multiple extractions in a single batch, and is suitable for large-scale production.

Claims (4)

1.一种提取植物有效成分的高效提取装置,其特征在于:本装置的反应罐(7)的罐体四周设置有用蒸汽加热的夹层(5),所述反应罐(7)内壁上设置有超声波发生器(6),所述反应罐(7)的中央设置有搅拌器(1),搅拌器(1)的下端设置有搅拌刀片(3),所述反应罐(7)的顶盖上设置有进料口(4)和排气孔(2),所述反应罐(7)的底部设置有过滤网(8)和底盖(9),底盖(9)中央设置出料管(10)。1. a high-efficiency extraction device for extracting plant active ingredients is characterized in that: the tank body of the reaction tank (7) of the device is provided with an interlayer (5) heated by steam, and the inner wall of the reaction tank (7) is provided with Ultrasonic generator (6), the center of described reaction tank (7) is provided with stirrer (1), and the lower end of stirrer (1) is provided with stirring blade (3), on the top cover of described reaction tank (7) A feed inlet (4) and an air vent (2) are provided, a filter screen (8) and a bottom cover (9) are provided at the bottom of the reaction tank (7), and a discharge pipe ( 10). 2.根据权利要求1所述的提取植物有效成分的高效提取装置,其特征在于:所述的过滤网(8)是20~40目的。2. The high-efficiency extraction device for extracting plant active ingredients according to claim 1, characterized in that: the filter screen (8) is 20-40 mesh. 3.根据权利要求1所述的提取植物有效成分的高效提取装置,其特征在于:所述的底盖(9)是与罐体活动连接的。3. The high-efficiency extraction device for extracting plant active ingredients according to claim 1, characterized in that: the bottom cover (9) is movably connected with the tank body. 4.根据权利要求1所述的提取植物有效成分的高效提取装置,其特征在于:所述的出料管(10)直径为10cm~20cm。4. The high-efficiency extraction device for extracting plant active ingredients according to claim 1, characterized in that: the diameter of the discharge pipe (10) is 10cm-20cm.
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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103111087A (en) * 2013-03-13 2013-05-22 华东理工大学 Extraction device of plant active ingredient
CN103182196A (en) * 2011-12-31 2013-07-03 上海金皮宝制药有限公司 High pressure drug extraction system
CN103665191A (en) * 2013-12-25 2014-03-26 嘉兴职业技术学院 Preparation method of chitosan and immersion device for preparing chitosan
CN104307202A (en) * 2014-11-11 2015-01-28 成都彼斯特生物科技有限公司 Traditional Chinese medicine extraction pot capable of preventing dregs from being mixed with medicament
CN104524810A (en) * 2014-12-31 2015-04-22 江苏天琦生物科技有限公司 Ultrasonic extraction pot
CN104941245A (en) * 2015-07-01 2015-09-30 马鞍山市润启新材料科技有限公司 Natural pigment extraction device
CN105597644A (en) * 2014-11-24 2016-05-25 丹阳恒安化学科技研究所有限公司 Reaction vessel
CN107597330A (en) * 2017-10-13 2018-01-19 海南大学 Tropical plants biological effective components extraction reducing mechanism and extraction element
CN108744584A (en) * 2018-07-10 2018-11-06 山东端信堂大禹药业有限公司 A kind of device and its extracting method extracting scutelloside from radix scutellariae
WO2019032448A1 (en) 2017-08-08 2019-02-14 Kultevat, Inc. System and method for continuous stirred tank solvent extraction using feedstock
CN110721496A (en) * 2019-11-05 2020-01-24 邳州富通生物制品有限公司 Plant extraction element
CN111604020A (en) * 2020-05-23 2020-09-01 江西思派思香料化工有限公司 Multistage filtration reation kettle of natural spices production usefulness

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103182196B (en) * 2011-12-31 2016-04-20 上海金皮宝制药有限公司 A kind of High pressure drug extraction system
CN103182196A (en) * 2011-12-31 2013-07-03 上海金皮宝制药有限公司 High pressure drug extraction system
CN103111087B (en) * 2013-03-13 2015-04-22 华东理工大学 Extraction device of plant active ingredient
CN103111087A (en) * 2013-03-13 2013-05-22 华东理工大学 Extraction device of plant active ingredient
CN103665191A (en) * 2013-12-25 2014-03-26 嘉兴职业技术学院 Preparation method of chitosan and immersion device for preparing chitosan
CN103665191B (en) * 2013-12-25 2016-06-01 嘉兴职业技术学院 The preparation method of a kind of chitosan and prepare the liquid-immersion device of chitosan
CN104307202A (en) * 2014-11-11 2015-01-28 成都彼斯特生物科技有限公司 Traditional Chinese medicine extraction pot capable of preventing dregs from being mixed with medicament
CN105597644A (en) * 2014-11-24 2016-05-25 丹阳恒安化学科技研究所有限公司 Reaction vessel
CN104524810A (en) * 2014-12-31 2015-04-22 江苏天琦生物科技有限公司 Ultrasonic extraction pot
CN104941245A (en) * 2015-07-01 2015-09-30 马鞍山市润启新材料科技有限公司 Natural pigment extraction device
WO2019032448A1 (en) 2017-08-08 2019-02-14 Kultevat, Inc. System and method for continuous stirred tank solvent extraction using feedstock
US11833448B2 (en) 2017-08-08 2023-12-05 Kultevat, Inc. System and method for continuous stirred tank solvent extraction using feedstock
EP3664908B1 (en) * 2017-08-08 2025-04-09 Kultevat, Inc. System and method for continuous stirred tank solvent extraction using feedstock
CN107597330A (en) * 2017-10-13 2018-01-19 海南大学 Tropical plants biological effective components extraction reducing mechanism and extraction element
CN108744584A (en) * 2018-07-10 2018-11-06 山东端信堂大禹药业有限公司 A kind of device and its extracting method extracting scutelloside from radix scutellariae
CN110721496A (en) * 2019-11-05 2020-01-24 邳州富通生物制品有限公司 Plant extraction element
CN111604020A (en) * 2020-05-23 2020-09-01 江西思派思香料化工有限公司 Multistage filtration reation kettle of natural spices production usefulness

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