CN103103766A - Real silk anti-yellowing finishing agent and preparation method thereof - Google Patents
Real silk anti-yellowing finishing agent and preparation method thereof Download PDFInfo
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- CN103103766A CN103103766A CN 201210443937 CN201210443937A CN103103766A CN 103103766 A CN103103766 A CN 103103766A CN 201210443937 CN201210443937 CN 201210443937 CN 201210443937 A CN201210443937 A CN 201210443937A CN 103103766 A CN103103766 A CN 103103766A
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Abstract
The invention discloses a real silk anti-yellowing finishing agent and a preparation method thereof. The real silk anti-yellowing finishing agent comprises the following components in parts by weight: 20-30 parts of dimethylaminoethyl methacrylate, 10-20 parts of polyacrylamide, 1-3 parts of potassium hydroxide, 1-3 parts of sodium polyphosphate, 10-20 parts of diethylene glycol, 3-5 parts of fatty alcohol-polyoxyethylene ether, 10-20 parts of dicyandiamide, 3-8 parts of polyethylene glycol, 10-20 parts of 1, 3-butanediol, and 100-180 parts of water. In comparison with the prior art, the real silk anti-yellowing finishing agent disclosed by the invention has the advantages of (1) good anti-yellowing effect, and incapability of affecting the style and the hand feeling of the real silk, and (2) good light fastness and incapability of yellowing and discoloring for a long-term preservation.
Description
Technical field
The invention belongs to the textile auxiliary technical field, more specifically relate to anti-yellowing finishing agent of a kind of real silk silk and preparation method thereof.
Background technology
Usually through real silk and silk broadcloth meeting yellowing variable color in storage process of refining bleaching, be mainly because the amino acid residue of the tryptophan in silk protein and TYR etc. is oxidized and painted in air.Favour impels this phenomenon to occur under the irradiation of light.Although the silk broadcloth of variable color can be bleached with sodium hydrosulfite, its character can occur deteriorated.
Summary of the invention
The object of the invention is to overcome the deficiency that prior art exists, provide a kind of real silk silk to prevent the yellowing finishing agent.
Another object of the present invention is to provide the preparation method of the anti-yellowing finishing agent of this real silk silk.
For achieving the above object, the present invention has taked following technical scheme:
A kind of real silk silk is prevented the yellowing finishing agent, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 20～30, polyacrylamide: 10～20,
Potassium hydroxide: 1～3, sodium polyphosphate: 1～3, diethylene glycol (DEG): 10～20,
Fatty alcohol-polyoxyethylene ether: 3～5, dicyandiamide: 10～20, polyethylene glycol: 3～8,
1,3-BDO: 10～20, water: 100～180.
In technique scheme, the preparation technology of the anti-yellowing finishing agent of described real silk silk is as follows:
(1) by proportioning, Dimethylaminoethyl Methacrylate, fatty alcohol-polyoxyethylene ether, diethylene glycol (DEG), dicyandiamide and polyethylene glycol are mixed, stirred 1～3 hour;
(2) polyacrylamide and sodium polyphosphate are added to the water, mix;
(3) product with step (1) mixes with the product of step (2), is warming up to 40～60 ℃, reacts 2～3 hours;
(4) be cooled to room temperature, add all the other components, get final product to get product after mixing.
Compared with prior art, the present invention has following beneficial effect:
(1) have the good yellowing effect that prevents, and harmless its style and feel;
(2) light resistance is good, and long preservation also can the yellowing variable color.
The specific embodiment
The invention will be further described below in conjunction with specific embodiment, but the present invention's scope required for protection is not limited to the scope that embodiment describes.
Embodiment 1
A kind of real silk silk is prevented the yellowing finishing agent, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 20, polyacrylamide: 10,
Potassium hydroxide: 1, sodium polyphosphate: 1, diethylene glycol (DEG): 10,
Fatty alcohol-polyoxyethylene ether: 3, dicyandiamide: 10, polyethylene glycol: 3,
1,3-BDO: 10, water: 100.
Embodiment 2
A kind of real silk silk is prevented the yellowing finishing agent, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 30, polyacrylamide: 20,
Potassium hydroxide: 3, sodium polyphosphate: 3, diethylene glycol (DEG): 20,
Fatty alcohol-polyoxyethylene ether: 5, dicyandiamide: 20, polyethylene glycol: 8,
1,3-BDO: 20, water: 180.
Embodiment 3
A kind of real silk silk is prevented the yellowing finishing agent, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 25, polyacrylamide: 16,
Potassium hydroxide: 2, sodium polyphosphate: 2, diethylene glycol (DEG): 16,
Fatty alcohol-polyoxyethylene ether: 4, dicyandiamide: 15, polyethylene glycol: 6,
1,3-BDO: 16, water: 160.
In above-described embodiment, the preparation method of the anti-yellowing finishing agent of described a kind of real silk silk comprises the steps:
(1) by proportioning, Dimethylaminoethyl Methacrylate, fatty alcohol-polyoxyethylene ether, diethylene glycol (DEG), dicyandiamide and polyethylene glycol are mixed, stirred 1～3 hour;
(2) polyacrylamide and sodium polyphosphate are added to the water, mix;
(3) product with step (1) mixes with the product of step (2), is warming up to 40～60 ℃, reacts 2～3 hours;
(4) be cooled to room temperature, add all the other components, get final product to get product after mixing.
Claims (5)
1. the anti-yellowing finishing agent of real silk silk, is characterized in that, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 20～30, polyacrylamide: 10～20,
Potassium hydroxide: 1～3, sodium polyphosphate: 1～3, diethylene glycol (DEG): 10～20,
Fatty alcohol-polyoxyethylene ether: 3～5, dicyandiamide: 10～20, polyethylene glycol: 3～8,
1,3-BDO: 10～20, water: 100～180.
2. the anti-yellowing finishing agent of a kind of real silk silk according to claim 1, is characterized in that, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 20, polyacrylamide: 10,
Potassium hydroxide: 1, sodium polyphosphate: 1, diethylene glycol (DEG): 10,
Fatty alcohol-polyoxyethylene ether: 3, dicyandiamide: 10, polyethylene glycol: 3,
1,3-BDO: 10, water: 100.
3. the anti-yellowing finishing agent of a kind of real silk silk according to claim 1, is characterized in that, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 30, polyacrylamide: 20,
Potassium hydroxide: 3, sodium polyphosphate: 3, diethylene glycol (DEG): 20,
Fatty alcohol-polyoxyethylene ether: 5, dicyandiamide: 20, polyethylene glycol: 8,
1,3-BDO: 20, water: 180.
4. the anti-yellowing finishing agent of a kind of real silk silk according to claim 1, is characterized in that, and is in weight portion, composed of the following components:
Dimethylaminoethyl Methacrylate: 25, polyacrylamide: 16,
Potassium hydroxide: 2, sodium polyphosphate: 2, diethylene glycol (DEG): 16,
Fatty alcohol-polyoxyethylene ether: 4, dicyandiamide: 15, polyethylene glycol: 6,
1,3-BDO: 16, water: 160.
5. the preparation method of the anti-yellowing finishing agent of a kind of real silk silk claimed in claim 1, is characterized in that, comprises the steps:
(1) by proportioning, Dimethylaminoethyl Methacrylate, fatty alcohol-polyoxyethylene ether, diethylene glycol (DEG), dicyandiamide and polyethylene glycol are mixed, stirred 1～3 hour;
(2) polyacrylamide and sodium polyphosphate are added to the water, mix;
(3) product with step (1) mixes with the product of step (2), is warming up to 40～60 ℃, reacts 2～3 hours;
(4) be cooled to room temperature, add all the other components, get final product to get product after mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210443937 CN103103766A (en) | 2012-11-08 | 2012-11-08 | Real silk anti-yellowing finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210443937 CN103103766A (en) | 2012-11-08 | 2012-11-08 | Real silk anti-yellowing finishing agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103103766A true CN103103766A (en) | 2013-05-15 |
Family
ID=48311941
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201210443937 Withdrawn CN103103766A (en) | 2012-11-08 | 2012-11-08 | Real silk anti-yellowing finishing agent and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN103103766A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103911857A (en) * | 2014-03-24 | 2014-07-09 | 灵山县桂合丝业有限公司 | Production method of anti-yellow anti-bacterial silk quilt cover |
| CN106223011A (en) * | 2016-08-25 | 2016-12-14 | 代长华 | A kind of real silk softness crease-shedding finishing agent and preparation method thereof |
| CN111172740A (en) * | 2020-03-05 | 2020-05-19 | 南通大学 | Anti-yellowing antibacterial real silk fabric and preparation method thereof |
-
2012
- 2012-11-08 CN CN 201210443937 patent/CN103103766A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103911857A (en) * | 2014-03-24 | 2014-07-09 | 灵山县桂合丝业有限公司 | Production method of anti-yellow anti-bacterial silk quilt cover |
| CN103911857B (en) * | 2014-03-24 | 2016-03-09 | 灵山县桂合丝业有限公司 | A kind of production method of anti-yellowing anti-bacteria real silk quilt cover |
| CN106223011A (en) * | 2016-08-25 | 2016-12-14 | 代长华 | A kind of real silk softness crease-shedding finishing agent and preparation method thereof |
| CN111172740A (en) * | 2020-03-05 | 2020-05-19 | 南通大学 | Anti-yellowing antibacterial real silk fabric and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C04 | Withdrawal of patent application after publication (patent law 2001) | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20130515 |