CN103083937B - Micro-bubble cyclone elution extraction device and technology - Google Patents
Micro-bubble cyclone elution extraction device and technology Download PDFInfo
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- CN103083937B CN103083937B CN201110340615.5A CN201110340615A CN103083937B CN 103083937 B CN103083937 B CN 103083937B CN 201110340615 A CN201110340615 A CN 201110340615A CN 103083937 B CN103083937 B CN 103083937B
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Abstract
The invention aims at providing a micro-bubble cyclone elution extraction device and a micro-bubble cyclone elution extraction technology. The device has the advantages of simple structure and reliable operation. The device is composed of a first micro-bubble elution tank, a second micro-bubble elution tank, and a third micro-bubble elution tank with a same structure; a first cyclone, a second cyclone, and a third cyclone with a same structure; a first water pump, a second water pump, and a third water pump with a same structure; an upper raw material tank, a lower raw material tank; an upper liquid tank; a lower liquid tank; and coupling pipes. In the device, solid raw material to be processed and liquid used for elution extraction perform countercurrent opposite movements; the solid raw material to be processed is cavitated and eluted by the micro-bubbles in the micro-bubble elution tanks; the components obtained by elution are subjected to cyclone separation in the cyclones, such that elution extraction task is completed.
Description
Technical field
The present invention relates to field of fine chemical, particularly a kind of Micro-bubble cyclone elution extraction device and technique.
Technical background
In field of fine chemical, a kind of liquid of frequent utilization is washed Off and is extracted a certain composition from the processed raw material of a kind of solid, such as, when producing active carbon with chemical method, need from carbon feedstock, to wash Off activator with water, when such as extracting camptothecine by homogenate method from common camptotheca leaf again, need from common camptotheca leaf defibrination, to extract camptothecine with ethanol.
Utilize ultrasonic cavitation effect, can improve and wash Off extraction efficiency, patent ZL03211143.6 " negative pressure-cavitation homogenous solid-liquid phase equipment for separating liquid from solid " just provide one more Jane victory wash Off extraction equipment.
Summary of the invention
The object of the invention is to provide the clean reliable Micro-bubble cyclone elution extraction device of a kind of structure Jane, it washes Off bucket by the first microbubble that three structures are identical, second microbubble washes Off bucket, 3rd microbubble washes Off bucket, the first cyclone that three structures are identical, second cyclone, three cuff technique, the first water pump that three structures are identical, second water pump, 3rd water pump and upper Raw material pail, lower Raw material pail, upper liquid bath, lower liquid bath and connection pipeline are formed, it is characterized in that on the cylindric staving that microbubble washes Off bucket, there is top material inlet mouth on top, upper feeding mouth is arranged at cylindrical barrel body sidewall top, lower discharge port is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle is housed, microbubble shower nozzle connects the oil-free compressed air assembly of known features by air inlet pipe,
Cyclone be known device by body, upper inlet, upper liquid outlet, lower liquid outlet form;
Water pump and upper Raw material pail, lower Raw material pail, upper liquid bath, lower liquid bath is known common equipment;
Described water pump can select clarified water pump, underflow pump, a kind of in the homogeneous tubing pump of high shear;
Three microbubbles wash Off bucket, three cyclones, three water pumps and upper Raw material pail, lower Raw material pail, upper liquid bath, and lower liquid bath is realized as lower link by pipeline:
The upper feeding mouth that lower liquid bath and the first microbubble wash Off bucket connects, the lower discharge port that first microbubble washes Off bucket connects with the first unit fixed on water pump suction, first exit of pump connects with the upper inlet of the first cyclone, the upper feeding mouth that upper liquid outlet and second microbubble of the first cyclone wash Off bucket connects, the lower discharge port that second microbubble washes Off bucket connects with the second unit fixed on water pump suction, second exit of pump connects with the upper inlet of the second cyclone, the upper feeding mouth that upper liquid outlet and the 3rd microbubble of the second cyclone wash Off bucket connects, the lower discharge port that 3rd microbubble washes Off bucket connects with the 3rd unit fixed on water pump suction, 3rd exit of pump connects with the upper inlet of three cuff technique, the upper liquid outlet of three cuff technique connects with upper liquid bath,
The top material inlet mouth that upper Raw material pail washes Off bucket with the 3rd microbubble connects, the top material inlet mouth that lower liquid outlet and second microbubble of three cuff technique wash Off bucket connects, the top material inlet mouth that lower liquid outlet and first microbubble of the second cyclone wash Off bucket connects, and the lower liquid outlet of the first cyclone connects with lower Raw material pail;
Described water pump can select clarified water pump, underflow pump, a kind of in the homogeneous tubing pump of high shear;
First microbubble is washed microbubble shower nozzle and the second microbubble on Off bucket and is washed microbubble shower nozzle on Off bucket, and the 3rd microbubble is washed microbubble shower nozzle on Off bucket and is connected on the oil-free compressed air assembly of known features by respective Jin Qi Guan And.
The said equipment is utilized to carry out washing Off extraction process as follows:
1) processed for solid raw material is loaded upper Raw material pail, the liquid being used for washing Off extraction is loaded lower liquid bath;
2) oil-free compressed air assembly is started;
3) start the first water pump, the second water pump, the 3rd water pump, upwards wash Off bucket → the first cyclone → the second microbubble along the first microbubble from lower liquid bath and wash Off bucket → the second cyclone → the 3rd microbubble for washing liquid that Off extracts and wash Off bucket → the three cuff technique → upper liquid bath and move;
The processed raw material of solid is washed Off bucket → the three cuff technique → the second microbubble along the 3rd microbubble downwards from upper Raw material pail and is washed Off bucket → the second cyclone → the first microbubble and wash Off bucket → the first cyclone → lower Raw material pail and move;
The processed raw material of solid is adverse current move toward one another with the liquid extracted for washing Off, the processed raw material of solid is washed in Off bucket by microbubble cavitation wash-out at each microbubble, elute composition cyclonic separation in each cyclone, elute composition and increase step by step to the 3rd eddy flow from the first cyclone contained by washing in liquid that Off extracts, and the contained composition that eluted is washed Off bucket from the 3rd microbubble and washed Off bucket to the first microbubble and reduce step by step in the processed raw material of solid, thus complete and from the processed raw material of a kind of solid, wash the task that Off extracts a certain composition with a kind of liquid.
According to real work needs, can analogize and set up Pyatyi, the more multistage Micro-bubble cyclone elution extraction device such as seven grades.
Accompanying drawing explanation
Fig. 1 is that the microbubble that three structures are identical washes Off Tong Knot structure schematic diagram,
First microbubble is washed on Off bucket (10) top material inlet mouth (15), upper feeding mouth (14), lower discharge port (13), microbubble shower nozzle (12), air inlet pipe (11),
Second microbubble is washed on Off bucket (20) top material inlet mouth (25), upper feeding mouth (24), lower discharge port (23), microbubble shower nozzle (22), air inlet pipe (21),
3rd microbubble is washed on Off bucket (30) top material inlet mouth (35), upper feeding mouth (34), lower discharge port (33), microbubble shower nozzle (32), air inlet pipe (31);
Fig. 2 is the Xuan Liu Qi Knot structure schematic diagram that three structures are identical, and cyclone is known device,
First cyclone (16) there are upper inlet (18), upper liquid outlet (17), lower liquid outlet (19),
Second cyclone (26) there are upper inlet (28), upper liquid outlet (27), lower liquid outlet (29),
Three cuff technique (36) there are upper inlet (38), upper liquid outlet (37), lower liquid outlet (39);
Fig. 3 washes Off bucket (10) by the first microbubble that three structures are identical, second microbubble washes Off bucket (20), 3rd microbubble washes Off bucket (30), the first cyclone (16) that three structures are identical, second cyclone (26), three cuff technique (36), the first water pump (07) that three structures are identical, second water pump (08), 3rd water pump (09) and upper Raw material pail (01), lower Raw material pail (02), upper liquid bath (04), lower liquid bath (03) and connection pipeline form the equipment schematic diagram that a kind of Micro-bubble cyclone elution is extracted.
Fig. 4
Be that the first microbubble is washed the upper microbubble shower nozzle (12) of Off bucket (10) and washed the upper microbubble shower nozzle (22) of Off bucket (20) with the second microbubble, the 3rd microbubble washes the upper microbubble shower nozzle (32) of Off bucket (30) by respective air inlet pipe (11) (21) (structural representation on the oil-free compressed air assembly that 31) And are connected in known features.
Detailed description of the invention
Below in conjunction with accompanying drawing, the invention will be further described, but be not limit the present invention.
The clean reliable Micro-bubble cyclone elution extraction device of a kind of structure Jane, it washes Off bucket (10) by the first microbubble that three structures are identical, second microbubble washes Off bucket (20), 3rd microbubble washes Off bucket (30), the first cyclone (16) that three structures are identical, second cyclone (26), three cuff technique (36), the first water pump (07) that three structures are identical, second water pump (08), 3rd water pump (09) and upper Raw material pail (01), lower Raw material pail (02), upper liquid bath (04), lower liquid bath (03) and connection pipeline are formed,
Above there is top material inlet mouth (15) on top, upper feeding mouth (14) is arranged at cylindrical barrel body sidewall top, lower discharge port (13) is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle (12), microbubble shower nozzle (12) connect known features oil-free compressed air assembly by air inlet pipe (11) is housed to it is characterized in that washing Off bucket (10) by the first microbubble;
Second microbubble washes Off bucket (20), and above there is top material inlet mouth (25) on top, upper feeding mouth (24) is arranged at cylindrical barrel body sidewall top, lower discharge port (23) is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle (22), microbubble shower nozzle (22) connect known features oil-free compressed air assembly by air inlet pipe (21) is housed;
3rd microbubble washes Off bucket (30), and above there is top material inlet mouth (35) on top, upper feeding mouth (34) is arranged at cylindrical barrel body sidewall top, lower discharge port (33) is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle (32), microbubble shower nozzle (32) connect known features oil-free compressed air assembly by air inlet pipe (31) is housed;
Cyclone is known device;
First cyclone (16) there are upper inlet (18), upper liquid outlet (17), lower liquid outlet (19),
Second cyclone (26) there are upper inlet (28), upper liquid outlet (27), lower liquid outlet (29),
Three cuff technique (36) there are upper inlet (38), upper liquid outlet (37), lower liquid outlet (39);
First water pump (07), the second water pump (08), the 3rd water pump (09) and upper Raw material pail (01), lower Raw material pail (02), upper liquid bath (04), lower liquid bath (03) is known common equipment;
First microbubble washes Off bucket (10), and the second microbubble washes Off bucket (20), and the 3rd microbubble washes Off bucket (30),
First cyclone (16), second cyclone (26), three cuff technique (36), first water pump (07), the second water pump (08), the 3rd water pump (09) and upper Raw material pail (01), lower Raw material pail (02), upper liquid bath (04), lower liquid bath (03), is realized as lower link by pipeline:
The upper feeding mouth (14) that lower liquid bath (03) and the first microbubble wash Off bucket (10) connects, the lower discharge port (13) that first microbubble washes Off bucket (10) connects with the first water pump (07) import, first water pump (07) outlet connects with the upper inlet (18) of the first cyclone (16), the upper feeding mouth (24) that upper liquid outlet (17) and second microbubble of the first cyclone (16) wash Off bucket (20) connects, the lower discharge port (23) that second microbubble washes Off bucket (20) connects with the second water pump (08) import, second water pump (08) outlet connects with the upper inlet (28) of the second cyclone (26), the upper feeding mouth (34) that upper liquid outlet (27) and the 3rd microbubble of the second cyclone (26) wash Off bucket (30) connects, the lower discharge port (33) that 3rd microbubble washes Off bucket (30) connects with the 3rd water pump (09) import, 3rd water pump (09) outlet connects with the upper inlet (38) of three cuff technique (36), the upper liquid outlet of three cuff technique (36) connects with upper liquid bath (04),
The top material inlet mouth (35) that upper Raw material pail (01) and the 3rd microbubble wash Off bucket (30) connects, the top material inlet mouth (25) that lower liquid outlet (39) and second microbubble of three cuff technique (36) wash Off bucket (20) connects, the top material inlet mouth (15) that lower liquid outlet (29) and first microbubble of the second cyclone (26) wash Off bucket (10) connects, and the lower liquid outlet (19) of the first cyclone (16) connects with lower Raw material pail (02);
Described water pump (07) (08) (09) can select clarified water pump, underflow pump, a kind of in the homogeneous tubing pump of high shear;
First microbubble is washed the upper microbubble shower nozzle (12) of Off bucket (10) and is washed the upper microbubble shower nozzle (22) of Off bucket (20) with the second microbubble, and the 3rd microbubble washes the upper microbubble shower nozzle (32) of Off bucket (30), and by respective air inlet pipe (11) (21), (31) And are connected on the oil-free compressed air assembly of known features.
The said equipment is utilized to carry out washing Off extraction process as follows:
4) processed for solid raw material is loaded upper Raw material pail (01), the liquid being used for washing Off extraction is loaded lower liquid bath (03);
5) oil-free compressed air assembly is started;
6) start the first water pump (07), the second water pump (08), the 3rd water pump (09), upwards wash Off bucket (10) → first cyclone (16) → second microbubble along the first microbubble from lower liquid bath (03) and wash Off bucket (20) → second cyclone (26) → the 3rd microbubble for washing liquid that Off extracts and wash Off bucket (30) → three cuff technique (36) → upper liquid bath (04) motion;
The processed raw material of solid is downwards washed Off bucket (30) → three cuff technique (36) → second microbubble along the 3rd microbubble from upper Raw material pail (01) and is washed Off bucket (20) → second cyclone (26) → first microbubble and wash Off bucket (10) → first cyclone (16) → lower Raw material pail (02) motion;
The processed raw material of solid is adverse current move toward one another with the liquid extracted for washing Off, the processed raw material of solid is washed in Off bucket by microbubble cavitation wash-out at each microbubble, elute composition cyclonic separation in each cyclone, elute composition and increase step by step to the 3rd eddy flow from the first cyclone contained by washing in liquid that Off extracts, and the contained composition that eluted is washed Off bucket from the 3rd microbubble and washed Off bucket to the first microbubble and reduce step by step in the processed raw material of solid, thus complete and from the processed raw material of a kind of solid, wash the task that Off extracts a certain composition with a kind of liquid.
According to real work needs, can analogize and set up Pyatyi, the more multistage Micro-bubble cyclone elution extraction device such as seven grades, wash Off extraction effect to improve.
Embodiment 1
Original chemical method produces activated carbon process main flow: wood chip soaks activator → heating carbonization-activation → wash-out activator; Present the present embodiment will complete heating carbonization-activation operation, upper Raw material pail (01) is contained in containing activator carbon feedstock, water is contained in lower liquid bath (03), in the invention described above equipment, water pump adopts Gong Zhi Knot structure underflow pump, through the invention described above technological process, collects containing activator water in upper liquid bath (04), in lower Raw material pail (02), collect the active carbon that oneself removes activator, thus complete wash-out activator operation.
Embodiment 2
Original ethanol homogenate method extracts camptothecine technique main flow from common camptotheca leaf: common camptotheca leaf adds ethanol and grind → adds ethanol high-shear homogenate → Separation of Solid and Liquid again; Present the present embodiment will complete grinding step, common camptotheca leaf slurry containing camptothecine and ethanol is contained in upper Raw material pail (01), ethanol is contained in lower liquid bath (03), in the invention described above equipment, water pump adopts the homogeneous tubing pump of Gong Zhi Knot structure high shear, through the invention described above technological process, the ethanol containing camptothecine is collected in upper liquid bath (04), in lower Raw material pail (02), collect the common camptotheca leaf recrement that oneself removes camptothecine, thus complete high-shear homogenate and solid-liquid separation process.
Embodiment 3
Originally from the root of kudzu vine, be separated kudzuvine root starch, technique main flow is that: Pao Silk → washing is separated; The Ji Pao Silk root of kudzu vine is contained in upper Raw material pail (01) by present the present embodiment, water is contained in lower liquid bath (03), in the invention described above equipment, water pump adopts Gong Zhi Knot structure underflow pump, through the invention described above technological process, collect in upper liquid bath (04) containing kudzuvine root starch water, in lower Raw material pail (02), collect the root of kudzu vine recrement that oneself removes kudzuvine root starch, thus complete washing separation circuit.
Embodiment 4
Original EtOH Sonicate ripple method is Ti Qu Bai Quinoa reed alcohol from giant knotweed, and technique main flow is: giant knotweed adds the process of ethanol grinding → ultrasonic wave, → Separation of Solid and Liquid; The giant knotweed slurry completing grinding step Han Bai Quinoa reed alcohol and ethanol is contained in upper Raw material pail (01) by present the present embodiment, ethanol is contained in lower liquid bath (03), in the invention described above equipment, water pump adopts the homogeneous tubing pump of Gong Zhi Knot structure high shear, through the invention described above technological process, the ethanol of Han Bai Quinoa reed alcohol is collected in upper liquid bath (04), in lower Raw material pail (02), collect the giant knotweed recrement that oneself removes Bai Quinoa reed alcohol, thus complete alternative original ultrasonic wave process and solid-liquid separation process.
Claims (3)
1. a Micro-bubble cyclone elution extraction device, above there is top material inlet mouth (15) on top, upper feeding mouth (14) is arranged at cylindrical barrel body sidewall top, lower discharge port (13) is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle (12), microbubble shower nozzle (12) connect known features oil-free compressed air assembly by air inlet pipe (11) is housed to it is characterized in that washing Off bucket (10) by the first microbubble;
Second microbubble washes Off bucket (20), and above there is top material inlet mouth (25) on top, upper feeding mouth (24) is arranged at cylindrical barrel body sidewall top, lower discharge port (23) is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle (22), microbubble shower nozzle (22) connect known features oil-free compressed air assembly by air inlet pipe (21) is housed;
3rd microbubble washes Off bucket (30), and above there is top material inlet mouth (35) on top, upper feeding mouth (34) is arranged at cylindrical barrel body sidewall top, lower discharge port (33) is arranged at cylindrical barrel body sidewall bottom, microbubble is washed at the bottom of the bucket of Off bucket inverted cone-shaped and microbubble shower nozzle (32), microbubble shower nozzle (32) connect known features oil-free compressed air assembly by air inlet pipe (31) is housed;
Cyclone is known device;
First cyclone (16) there are upper inlet (18), upper liquid outlet (17), lower liquid outlet (19),
Second cyclone (26) there are upper inlet (28), upper liquid outlet (27), lower liquid outlet (29),
Three cuff technique (36) there are upper inlet (38), upper liquid outlet (37), lower liquid outlet (39);
First water pump (07), the second water pump (08), the 3rd water pump (09) and upper Raw material pail (01), lower Raw material pail (02), upper liquid bath (04), lower liquid bath (03) is known common equipment;
First microbubble washes Off bucket (10), second microbubble washes Off bucket (20), 3rd microbubble washes Off bucket (30), first cyclone (16), second cyclone (26), three cuff technique (36), first water pump (07), second water pump (08), 3rd water pump (09) and upper Raw material pail (01), lower Raw material pail (02), upper liquid bath (04), lower liquid bath (03), is realized as lower link by pipeline:
The upper feeding mouth (14) that lower liquid bath (03) and the first microbubble wash Off bucket (10) connects, the lower discharge port (13) that first microbubble washes Off bucket (10) connects with the first water pump (07) import, first water pump (07) outlet connects with the upper inlet (18) of the first cyclone (16), the upper feeding mouth (24) that upper liquid outlet (17) and second microbubble of the first cyclone (16) wash Off bucket (20) connects, the lower discharge port (23) that second microbubble washes Off bucket (20) connects with the second water pump (08) import, second water pump (08) outlet connects with the upper inlet (28) of the second cyclone (26), the upper feeding mouth (34) that upper liquid outlet (27) and the 3rd microbubble of the second cyclone (26) wash Off bucket (30) connects, the lower discharge port (33) that 3rd microbubble washes Off bucket (30) connects with the 3rd water pump (09) import, 3rd water pump (09) outlet connects with the upper inlet (38) of three cuff technique (36), the upper liquid outlet of three cuff technique (36) connects with upper liquid bath (04),
The top material inlet mouth (35) that upper Raw material pail (01) and the 3rd microbubble wash Off bucket (30) connects, the top material inlet mouth (25) that lower liquid outlet (39) and second microbubble of three cuff technique (36) wash Off bucket (20) connects, the top material inlet mouth 1 (15) that lower liquid outlet (29) and first microbubble of the second cyclone (26) wash Off bucket (10) connects, and the lower liquid outlet (19) of the first cyclone (16) connects with lower Raw material pail (02);
Described water pump (07) (08) (09) selects clarified water pump, underflow pump, a kind of in the homogeneous tubing pump of high shear;
First microbubble is washed the upper microbubble shower nozzle (12) of Off bucket (10) and is washed the upper microbubble shower nozzle (22) of Off bucket (20) with the second microbubble, and the 3rd microbubble washes the upper microbubble shower nozzle (32) of Off bucket (30), and by respective air inlet pipe (11) (21), (31) And are connected on the oil-free compressed air assembly of known features.
2. want the Micro-bubble cyclone elution extraction device described in art 1 according to right, it is as follows to carry out washing Off extraction process: processed for solid raw material is loaded upper Raw material pail (01), will be used for washing the liquid that Off extracts and load lower liquid bath (03);
1) oil-free compressed air assembly is started;
2) start the first water pump (07), the second water pump (08), the 3rd water pump (09), upwards wash Off bucket (10) → first cyclone (16) → second microbubble along the first microbubble from lower liquid bath (03) and wash Off bucket (20) → second cyclone (26) → the 3rd microbubble for washing liquid that Off extracts and wash Off bucket (30) → three cuff technique (36) → upper liquid bath (04) motion;
The processed raw material of solid is downwards washed Off bucket (30) → three cuff technique (36) → second microbubble along the 3rd microbubble from upper Raw material pail (01) and is washed Off bucket (20) → second cyclone (26) → first microbubble and wash Off bucket (10) → first cyclone (16) → lower Raw material pail (02) motion;
The processed raw material of solid is adverse current move toward one another with the liquid extracted for washing Off, the processed raw material of solid is washed in Off bucket at each microbubble and is washed Off by microbubble cavitation, wash Off and go out composition cyclonic separation in each cyclone, elute composition and increase step by step to the 3rd eddy flow from the first cyclone contained by washing in liquid that Off extracts, and the contained composition that eluted is washed Off bucket from the 3rd microbubble and washed Off bucket to the first microbubble and reduce step by step in the processed raw material of solid, thus complete and from the processed raw material of a kind of solid, wash the task that Off extracts a certain composition with a kind of liquid.
3. want the Micro-bubble cyclone elution extraction device described in art 1 according to right, analogize and set up Pyatyi, the Micro-bubble cyclone elution extraction device of seven grades, wash Off extraction effect to improve.
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| CN2597047Y (en) * | 2003-01-22 | 2004-01-07 | 东北林业大学 | Negative pressure cavitation suspensoid solid-liquid extraction separator |
| CN101550377A (en) * | 2009-05-25 | 2009-10-07 | 侯梦斌 | Preparation method of simultaneously extracting tea-seed oil and tea saponin from the kernel |
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| CN2597047Y (en) * | 2003-01-22 | 2004-01-07 | 东北林业大学 | Negative pressure cavitation suspensoid solid-liquid extraction separator |
| CN101550377A (en) * | 2009-05-25 | 2009-10-07 | 侯梦斌 | Preparation method of simultaneously extracting tea-seed oil and tea saponin from the kernel |
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| C06 | Publication | ||
| PB01 | Publication | ||
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