CN103044968B - Disperse yellow dye formula - Google Patents
Disperse yellow dye formula Download PDFInfo
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- CN103044968B CN103044968B CN201310010793.0A CN201310010793A CN103044968B CN 103044968 B CN103044968 B CN 103044968B CN 201310010793 A CN201310010793 A CN 201310010793A CN 103044968 B CN103044968 B CN 103044968B
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- Prior art keywords
- disperse yellow
- dye
- chromatid
- mass percent
- rgfl
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- VGKYEIFFSOPYEW-UHFFFAOYSA-N 2-methyl-4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound Cc1cc(ccc1O)N=Nc1ccc(cc1)N=Nc1ccccc1 VGKYEIFFSOPYEW-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 239000001043 yellow dye Substances 0.000 title claims abstract description 15
- 239000000126 substance Substances 0.000 claims abstract description 10
- 108091060290 Chromatid Proteins 0.000 claims description 31
- 210000004756 chromatid Anatomy 0.000 claims description 31
- 239000000975 dye Substances 0.000 abstract description 17
- 238000004043 dyeing Methods 0.000 abstract description 10
- 239000000203 mixture Substances 0.000 abstract description 4
- 239000000314 lubricant Substances 0.000 abstract description 3
- 239000004576 sand Substances 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 2
- 239000000178 monomer Substances 0.000 abstract 6
- 239000000986 disperse dye Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 239000012752 auxiliary agent Substances 0.000 description 6
- 239000000835 fiber Substances 0.000 description 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 2
- 229920002301 cellulose acetate Polymers 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- KTHUKEZOIFYPEH-UHFFFAOYSA-N 1-benzylnaphthalene Chemical compound C=1C=CC2=CC=CC=C2C=1CC1=CC=CC=C1 KTHUKEZOIFYPEH-UHFFFAOYSA-N 0.000 description 1
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 description 1
- RTZYVAQWQXPIAC-UHFFFAOYSA-N 4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound C1=CC(O)=CC=C1N=NC1=CC=C(N=NC=2C=CC=CC=2)C=C1 RTZYVAQWQXPIAC-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000012932 acetate dye Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920005552 sodium lignosulfonate Polymers 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
Abstract
The invention relates to a disperse dye formula, particularly a disperse yellow dye formula. The disperse yellow dye is prepared by mixing the following components in percentage by mass: 60-70% of dyeing monomer A with the chemical formula disclosed in the specification, 10-15% of dyeing monomer B with the chemical formula disclosed in the specification, and 20-25% of dyeing monomer C with the chemical formula disclosed in the specification. The dye mixed according to the formula can substitute disperse yellow RGFL, has the same dyeing effect as the disperse yellow RGFL, and keeps the ratio of the dyeing monomer B-dyeing monomer C mixture to the dyeing monomer A at 3:7-4:6. The method for preparing the finished product dye comprises the following steps: adding assistants and water or any other lubricant, milling with a sand mill, and drying the finished product to synthesize the color of the disperse yellow RGFL. The finished product can be used directly to completely substitute the disperse yellow dye RGFL.
Description
Technical field
The present invention relates to a kind of dispersed dye formula, especially a kind of disperse yellow dye.
Background technology
Dispersed dye are the water-soluble lower nonionic dyes of a class.For the dyeing of cellulose acetate fibre, be called cellulose acetate dye the earliest.Along with the development of synthon, polyamide fibre, terylene occur in succession, terylene especially, the characteristic such as permutation degree is high owing to having, and fiber gap is few, and hydrophobicity is strong, have under carrier or high temperature, thermosol, make swelling of fiber, dyestuff just can enter fiber and on dye.Therefore, dyestuff has been proposed to new requirement, require to have the dyestuff of better hydrophobicity and certain dispersiveness and resistance to distillation etc., in dyeing and printing process, the dispersed dye for polyester piece good dyeing possess these performances substantially at present, but because kind is more, during use, also must select according to processing request choosing row.
From European Union, Disperse Yellow RGFL being also referred to as to C.I. DISPERSE YELLOW 23 classifies as after violated dyestuff, find the substitute of Disperse Yellow RGFL, launch at home, but the achievement of making a breakthrough property not, and the substitute of development Disperse Yellow RGFL remains a larger problem.
Summary of the invention
The object of the invention is to, a kind of disperse yellow dye of alternative Disperse Yellow RGFL is provided.
The technical solution adopted for the present invention to solve the technical problems is: a kind of disperse yellow dye is 60-70% by mass percent, and chemical formula is
chromatid A, mass percent is 10-15%, chemical formula is
chromatid B, mass percent is 20-25%, chemical formula is
chromatid C, mix to form.
The further setting of the present invention is: the mass percent of chromatid A is 65%, and the mass percent of chromatid B is 10%, and the mass percent of chromatid C is 25%.
The further setting of the present invention is: the mass percent of chromatid A is 65%, and the mass percent of chromatid B is 15%, and the mass percent of chromatid C is 20%.
The dyestuff that mixes out according to such scheme formula just can replace Disperse Yellow RGFL, identical with the Color of Disperse Yellow RGFL, keeping chromatid B and chromatid C mixture is 3:7 to 4:6 with the ratio of chromatid A, when preparing finished product dyestuff, add auxiliary agent, water or other lubricants, with sand mill, grind, then be dried finished product, just can synthesize the color of Disperse Yellow RGFL, then just can directly use, can replace Disperse Yellow RGFL completely.
Embodiment
Embodiment mono-
A disperse yellow dye, is 60% by mass percent, and chemical formula is
chromatid A, mass percent is 15%, chemical formula is
chromatid B, quality percentage
Embodiment bis-
The chromatid A that a disperse yellow dye is 70% by mass percent, the chromatid B that mass percent is 10%, the chromatid C that mass percent is 20% mixes formation.
Embodiment tri-
The chromatid A that a disperse yellow dye is 65% by mass percent, the chromatid B that mass percent is 10%, the chromatid C that mass percent is 25% mixes formation.
Embodiment tetra-
The chromatid A that a disperse yellow dye is 65% by mass percent, the chromatid B that mass percent is 15%, the chromatid C that mass percent is 20% mixes formation.
Above-mentioned four kinds of embodiment institute proportionings dispersed dye out, adding auxiliary agent, water or other lubricants, grind with sand mill, then dry, just can obtain final dispersed dye finished product.
It should be noted that dyestuff and auxiliary agent in the present invention, to mix according to the ratio between 1:10 to 1:0.5, in reality use, auxiliary agent is changeable, and the dyestuff in the present invention will coordinate ability effective use with auxiliary agent, described auxiliary agent is one of following or its mixture: 1. naphthalene sulfonic acidformaldehyde condensation product, 2. condensation compound of methyl naphthalene sulfonic acid and formaldehyde, 3. benzyl naphthalene sulfonic formaldehyde condensation compound, 4. sodium lignosulfonate.
Obviously, above-described embodiment is only used to done giving an example is clearly described, and the not restriction to embodiment.To those of ordinary skill in the art, can also make other changes in different forms on the basis of the above description.Here exhaustive without also giving all embodiments.And the apparent variation of being extended out thus or change are still in protection scope of the present invention.
Claims (3)
1. a disperse yellow dye, is characterized in that: by mass percent, be 60-70%, chemical formula is
chromatid A, mass percent is 10-15%, chemical formula is
chromatid B, quality percentage
2. according to disperse yellow dye claimed in claim 1, it is characterized in that: the mass percent of chromatid A is 65%, the mass percent of chromatid B is 10%, and the mass percent of chromatid C is 25%.
3. according to disperse yellow dye claimed in claim 1, it is characterized in that: the mass percent of chromatid A is 65%, the mass percent of chromatid B is 15%, and the mass percent of chromatid C is 20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310010793.0A CN103044968B (en) | 2013-01-11 | 2013-01-11 | Disperse yellow dye formula |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310010793.0A CN103044968B (en) | 2013-01-11 | 2013-01-11 | Disperse yellow dye formula |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103044968A CN103044968A (en) | 2013-04-17 |
| CN103044968B true CN103044968B (en) | 2014-10-22 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310010793.0A Active CN103044968B (en) | 2013-01-11 | 2013-01-11 | Disperse yellow dye formula |
Country Status (1)
| Country | Link |
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| CN (1) | CN103044968B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104016880B (en) * | 2014-06-09 | 2016-07-13 | 苏州大学 | The presoma of special azo reactive disperse dyes and purposes |
| CN107603273B (en) * | 2017-09-08 | 2019-05-03 | 浙江龙盛集团股份有限公司 | A kind of disperse yellow dye composition and its product |
| CN112876876B (en) * | 2020-12-31 | 2023-05-23 | 绍兴市上虞金冠化工有限公司 | Disperse yellow-orange dye composition and dye product thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4062645A (en) * | 1975-05-21 | 1977-12-13 | Montedison S.P.A. | Acid dyes useful for dyeing streaked nylon |
| JPH0593044A (en) * | 1991-08-02 | 1993-04-16 | Sumitomo Chem Co Ltd | Curable resin composition |
| CN1125240A (en) * | 1995-12-20 | 1996-06-26 | 大连理工大学化工学院 | Monoazo type pyridone series compound dye |
| WO2001017349A1 (en) * | 1999-09-10 | 2001-03-15 | Smithkline Beckman Corporation | Thrombopoietin mimetics |
| US6203581B1 (en) * | 1999-11-12 | 2001-03-20 | Everlight Usa, Inc. | Yellow reactive dye composition |
| EP0978544B1 (en) * | 1994-02-19 | 2001-05-02 | DyStar Textilfarben GmbH & Co. Deutschland KG | Reactive dye mixtures and their use for dyeing and printing fibrous materials containing hydroxyl and/or carbonamide groups |
-
2013
- 2013-01-11 CN CN201310010793.0A patent/CN103044968B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4062645A (en) * | 1975-05-21 | 1977-12-13 | Montedison S.P.A. | Acid dyes useful for dyeing streaked nylon |
| JPH0593044A (en) * | 1991-08-02 | 1993-04-16 | Sumitomo Chem Co Ltd | Curable resin composition |
| EP0978544B1 (en) * | 1994-02-19 | 2001-05-02 | DyStar Textilfarben GmbH & Co. Deutschland KG | Reactive dye mixtures and their use for dyeing and printing fibrous materials containing hydroxyl and/or carbonamide groups |
| CN1125240A (en) * | 1995-12-20 | 1996-06-26 | 大连理工大学化工学院 | Monoazo type pyridone series compound dye |
| WO2001017349A1 (en) * | 1999-09-10 | 2001-03-15 | Smithkline Beckman Corporation | Thrombopoietin mimetics |
| US6203581B1 (en) * | 1999-11-12 | 2001-03-20 | Everlight Usa, Inc. | Yellow reactive dye composition |
Non-Patent Citations (2)
| Title |
|---|
| Ajay Singh等.Synthesis and properties of some novel pyrazolone-based heterocyclic azo disperse dyes containing a fluorosulfonyl group.《Dyes and Pigments 》.2012,第95卷(第3期),580-586. |
| Synthesis and properties of some novel pyrazolone-based heterocyclic azo disperse dyes containing a fluorosulfonyl group;Ajay Singh等;《Dyes and Pigments 》;20121231;第95卷(第3期);580-586 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103044968A (en) | 2013-04-17 |
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Effective date of registration: 20181107 Address after: 223500 heggou town (Chemical Industrial Park), Gunan County, Lianyungang, Jiangsu Patentee after: JIANGSU DIAN CHEMICAL Co.,Ltd. Address before: 318000 three mountain village, Jiaojiang District, Taizhou, Zhejiang Patentee before: ZHEJIANG SHANYU TECHNOLOGY CO.,LTD. |
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Effective date of registration: 20231010 Address after: 333300 Tashan Industrial Zone, Leping Industrial Park, Jingdezhen City, Jiangxi Province Patentee after: LEPING SAFELY PHARMACEUTICAL Co.,Ltd. Address before: 223500 heggou town (Chemical Industrial Park), Gunan County, Lianyungang, Jiangsu Patentee before: JIANGSU DIAN CHEMICAL Co.,Ltd. |
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