CN103044968A - Disperse yellow dye formula - Google Patents
Disperse yellow dye formula Download PDFInfo
- Publication number
- CN103044968A CN103044968A CN2013100107930A CN201310010793A CN103044968A CN 103044968 A CN103044968 A CN 103044968A CN 2013100107930 A CN2013100107930 A CN 2013100107930A CN 201310010793 A CN201310010793 A CN 201310010793A CN 103044968 A CN103044968 A CN 103044968A
- Authority
- CN
- China
- Prior art keywords
- disperse yellow
- chromatid
- dye
- mass percent
- rgfl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- VGKYEIFFSOPYEW-UHFFFAOYSA-N 2-methyl-4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound Cc1cc(ccc1O)N=Nc1ccc(cc1)N=Nc1ccccc1 VGKYEIFFSOPYEW-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 239000001043 yellow dye Substances 0.000 title claims abstract description 15
- 239000000126 substance Substances 0.000 claims abstract description 12
- 108091060290 Chromatid Proteins 0.000 claims description 33
- 210000004756 chromatid Anatomy 0.000 claims description 33
- 239000000975 dye Substances 0.000 abstract description 17
- 238000004043 dyeing Methods 0.000 abstract description 10
- 239000000203 mixture Substances 0.000 abstract description 5
- 239000000314 lubricant Substances 0.000 abstract description 3
- 239000004576 sand Substances 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 2
- 239000000178 monomer Substances 0.000 abstract 6
- 239000000986 disperse dye Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 239000012752 auxiliary agent Substances 0.000 description 6
- 239000000835 fiber Substances 0.000 description 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 2
- 229920002301 cellulose acetate Polymers 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- KTHUKEZOIFYPEH-UHFFFAOYSA-N 1-benzylnaphthalene Chemical compound C=1C=CC2=CC=CC=C2C=1CC1=CC=CC=C1 KTHUKEZOIFYPEH-UHFFFAOYSA-N 0.000 description 1
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 description 1
- RTZYVAQWQXPIAC-UHFFFAOYSA-N 4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound C1=CC(O)=CC=C1N=NC1=CC=C(N=NC=2C=CC=CC=2)C=C1 RTZYVAQWQXPIAC-UHFFFAOYSA-N 0.000 description 1
- 0 C*C(C=CCN=N[*@](*)C=C[C@](*)CCC*)NC Chemical compound C*C(C=CCN=N[*@](*)C=C[C@](*)CCC*)NC 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000012932 acetate dye Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229920005552 sodium lignosulfonate Polymers 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
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- Coloring (AREA)
Abstract
The invention relates to a disperse dye formula, particularly a disperse yellow dye formula. The disperse yellow dye is prepared by mixing the following components in percentage by mass: 60-70% of dyeing monomer A with the chemical formula disclosed in the specification, 10-15% of dyeing monomer B with the chemical formula disclosed in the specification, and 20-25% of dyeing monomer C with the chemical formula disclosed in the specification. The dye mixed according to the formula can substitute disperse yellow RGFL, has the same dyeing effect as the disperse yellow RGFL, and keeps the ratio of the dyeing monomer B-dyeing monomer C mixture to the dyeing monomer A at 3:7-4:6. The method for preparing the finished product dye comprises the following steps: adding assistants and water or any other lubricant, milling with a sand mill, and drying the finished product to synthesize the color of the disperse yellow RGFL. The finished product can be used directly to completely substitute the disperse yellow dye RGFL.
Description
Technical field
The present invention relates to a kind of dispersed dye prescription, especially a kind of disperse yellow dye prescription.
Background technology
Dispersed dye are the water-soluble lower nonionic dyes of a class.Be used for the earliest the dyeing of cellulose acetate fibre, be called cellulose acetate dye.Along with the development of synthon, polyamide fibre, terylene occur in succession, and terylene especially because the characteristic such as it is high to have a permutation degree, and fiber gap is few, and hydrophobicity is strong, make swelling of fiber having under carrier or high temperature, the thermosol, dyestuff just can enter fiber and on dye.Therefore, dyestuff has been proposed Secretary, namely require to have the dyestuff of better hydrophobicity and certain dispersiveness and anti-distillation etc., the dispersed dye that are used at present polyester piece good dyeing in the dyeing and printing process possess these performances basically, but because kind is more, also must select according to processing request choosing row during use.
After European Union also is referred to as Disperse Yellow RGFL C.I. DISPERSE YELLOW 23 and classifies the dyestuff of violating a ban as, seek the substitute of Disperse Yellow RGFL, launch at home, but the achievement of making a breakthrough property not, and the substitute of development Disperse Yellow RGFL remains a larger problem.
Summary of the invention
The object of the invention is to, a kind of disperse yellow dye prescription of alternative Disperse Yellow RGFL is provided.
The technical solution adopted for the present invention to solve the technical problems is: a kind of disperse yellow dye prescription is 60-70% by mass percent, and chemical formula is
Chromatid A, mass percent is 10-15%, chemical formula is
Chromatid B, mass percent is 20-25%, chemical formula is
Chromatid C, mix to consist of.
The further setting of the present invention is: the mass percent of chromatid A is 65%, and the mass percent of chromatid B is 10%, and the mass percent of chromatid C is 25%.
The further setting of the present invention is: the mass percent of chromatid A is 65%, and the mass percent of chromatid B is 15%, and the mass percent of chromatid C is 20%.
The dyestuff that mixes out according to the such scheme prescription just can replace Disperse Yellow RGFL, identical with the Color of Disperse Yellow RGFL, keeping chromatid B and chromatid C mixture and the ratio of chromatid A is 3:7 to 4:6, in preparation finished product dyestuff, then add auxiliary agent, water or other lubricants, grind with sand mill, then dry finished product, just can synthesize the color of Disperse Yellow RGFL, then just can directly use, can replace Disperse Yellow RGFL fully.
Embodiment
Embodiment one
A kind of disperse yellow dye prescription is 60% by mass percent, and chemical formula is
Chromatid A, mass percent is 15%, chemical formula is
Chromatid B, mass percent is 25%, chemical formula is
Chromatid C, mix to consist of.
Embodiment two
A kind of disperse yellow dye prescription is 70% chromatid A by mass percent, and mass percent is 10% chromatid B, and mass percent is that 20% chromatid C mixes and consists of.
Embodiment three
A kind of disperse yellow dye prescription is 65% chromatid A by mass percent, and mass percent is 10% chromatid B, and mass percent is that 25% chromatid C mixes and consists of.
Embodiment four
A kind of disperse yellow dye prescription is 65% chromatid A by mass percent, and mass percent is 15% chromatid B, and mass percent is that 20% chromatid C mixes and consists of.
Above-mentioned four kinds of embodiment institute proportionings dispersed dye out adding auxiliary agent, water or other lubricants, grind with sand mill, and are then dry, just can obtain final dispersed dye finished product.
It should be noted that dyestuff and auxiliary agent among the present invention, to mix according to the ratio between the 1:10 to 1:0.5, because in actual the use, auxiliary agent is changeable, and the dyestuff among the present invention will cooperate the ability effective use with auxiliary agent, described auxiliary agent is one of following or its mixture: 1. naphthalene sulfonic acidformaldehyde condensation product, 2. condensation compound of methyl naphthalene sulfonic acid and formaldehyde, 3. benzyl naphthalene sulfonic formaldehyde condensation compound, 4. sodium lignosulfonate.
Obviously, above-described embodiment only be for explanation clearly do for example, and be not restriction to embodiment.To those of ordinary skill in the art, can also make other changes in different forms on the basis of the above description.Here need not also can't give all embodiments exhaustive.And the apparent variation of being extended out thus or change still are in protection scope of the present invention.
Claims (3)
1. disperse yellow dye prescription is characterized in that: be 60-70% by mass percent, chemical formula is
Chromatid A, mass percent is 10-15%, chemical formula is
Chromatid B, mass percent is 20-25%, chemical formula is
Chromatid C, mix to consist of.
2. according to disperse yellow dye claimed in claim 1, it is characterized in that: the mass percent of chromatid A is 65%, and the mass percent of chromatid B is 10%, and the mass percent of chromatid C is 25%.
3. according to disperse yellow dye claimed in claim 1, it is characterized in that: the mass percent of chromatid A is 65%, and the mass percent of chromatid B is 15%, and the mass percent of chromatid C is 20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310010793.0A CN103044968B (en) | 2013-01-11 | 2013-01-11 | Disperse yellow dye formula |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310010793.0A CN103044968B (en) | 2013-01-11 | 2013-01-11 | Disperse yellow dye formula |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103044968A true CN103044968A (en) | 2013-04-17 |
| CN103044968B CN103044968B (en) | 2014-10-22 |
Family
ID=48057839
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310010793.0A Active CN103044968B (en) | 2013-01-11 | 2013-01-11 | Disperse yellow dye formula |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103044968B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104016880A (en) * | 2014-06-09 | 2014-09-03 | 苏州大学 | Special precursor for azo reactive disperse dyes and use of special precursor |
| CN107603273A (en) * | 2017-09-08 | 2018-01-19 | 浙江龙盛集团股份有限公司 | A kind of disperse yellow dye composition and its product |
| CN112876876A (en) * | 2020-12-31 | 2021-06-01 | 绍兴市上虞金冠化工有限公司 | Disperse yellow-orange dye composition and dye product thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4062645A (en) * | 1975-05-21 | 1977-12-13 | Montedison S.P.A. | Acid dyes useful for dyeing streaked nylon |
| JPH0593044A (en) * | 1991-08-02 | 1993-04-16 | Sumitomo Chem Co Ltd | Curable resin composition |
| CN1125240A (en) * | 1995-12-20 | 1996-06-26 | 大连理工大学化工学院 | Monoazo type pyridone series compound dye |
| WO2001017349A1 (en) * | 1999-09-10 | 2001-03-15 | Smithkline Beckman Corporation | Thrombopoietin mimetics |
| US6203581B1 (en) * | 1999-11-12 | 2001-03-20 | Everlight Usa, Inc. | Yellow reactive dye composition |
| EP0978544B1 (en) * | 1994-02-19 | 2001-05-02 | DyStar Textilfarben GmbH & Co. Deutschland KG | Reactive dye mixtures and their use for dyeing and printing fibrous materials containing hydroxyl and/or carbonamide groups |
-
2013
- 2013-01-11 CN CN201310010793.0A patent/CN103044968B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4062645A (en) * | 1975-05-21 | 1977-12-13 | Montedison S.P.A. | Acid dyes useful for dyeing streaked nylon |
| JPH0593044A (en) * | 1991-08-02 | 1993-04-16 | Sumitomo Chem Co Ltd | Curable resin composition |
| EP0978544B1 (en) * | 1994-02-19 | 2001-05-02 | DyStar Textilfarben GmbH & Co. Deutschland KG | Reactive dye mixtures and their use for dyeing and printing fibrous materials containing hydroxyl and/or carbonamide groups |
| CN1125240A (en) * | 1995-12-20 | 1996-06-26 | 大连理工大学化工学院 | Monoazo type pyridone series compound dye |
| WO2001017349A1 (en) * | 1999-09-10 | 2001-03-15 | Smithkline Beckman Corporation | Thrombopoietin mimetics |
| US6203581B1 (en) * | 1999-11-12 | 2001-03-20 | Everlight Usa, Inc. | Yellow reactive dye composition |
Non-Patent Citations (1)
| Title |
|---|
| AJAY SINGH等: "Synthesis and properties of some novel pyrazolone-based heterocyclic azo disperse dyes containing a fluorosulfonyl group", 《DYES AND PIGMENTS 》, vol. 95, no. 3, 31 December 2012 (2012-12-31), pages 580 - 586 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104016880A (en) * | 2014-06-09 | 2014-09-03 | 苏州大学 | Special precursor for azo reactive disperse dyes and use of special precursor |
| CN104016880B (en) * | 2014-06-09 | 2016-07-13 | 苏州大学 | The presoma of special azo reactive disperse dyes and purposes |
| CN107603273A (en) * | 2017-09-08 | 2018-01-19 | 浙江龙盛集团股份有限公司 | A kind of disperse yellow dye composition and its product |
| CN107603273B (en) * | 2017-09-08 | 2019-05-03 | 浙江龙盛集团股份有限公司 | A kind of disperse yellow dye composition and its product |
| CN112876876A (en) * | 2020-12-31 | 2021-06-01 | 绍兴市上虞金冠化工有限公司 | Disperse yellow-orange dye composition and dye product thereof |
| CN112876876B (en) * | 2020-12-31 | 2023-05-23 | 绍兴市上虞金冠化工有限公司 | Disperse yellow-orange dye composition and dye product thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103044968B (en) | 2014-10-22 |
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Address after: Three, 318000 mountain village, Jiaojiang District, Zhejiang, Taizhou Patentee after: ZHEJIANG SHANYU TECHNOLOGY CO.,LTD. Address before: Three, 317700 mountain village, Jiaojiang District, Zhejiang, Taizhou Patentee before: ZHEJIANG SHANYU DYESTUFF CHEMICAL Co.,Ltd. |
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Effective date of registration: 20181107 Address after: 223500 heggou town (Chemical Industrial Park), Gunan County, Lianyungang, Jiangsu Patentee after: JIANGSU DIAN CHEMICAL Co.,Ltd. Address before: 318000 three mountain village, Jiaojiang District, Taizhou, Zhejiang Patentee before: ZHEJIANG SHANYU TECHNOLOGY CO.,LTD. |
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Effective date of registration: 20231010 Address after: 333300 Tashan Industrial Zone, Leping Industrial Park, Jingdezhen City, Jiangxi Province Patentee after: LEPING SAFELY PHARMACEUTICAL Co.,Ltd. Address before: 223500 heggou town (Chemical Industrial Park), Gunan County, Lianyungang, Jiangsu Patentee before: JIANGSU DIAN CHEMICAL Co.,Ltd. |
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| TR01 | Transfer of patent right |