CN103043968A - Composite foamed cement insulation board for tile surface and preparation method thereof - Google Patents
Composite foamed cement insulation board for tile surface and preparation method thereof Download PDFInfo
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- CN103043968A CN103043968A CN2012105763787A CN201210576378A CN103043968A CN 103043968 A CN103043968 A CN 103043968A CN 2012105763787 A CN2012105763787 A CN 2012105763787A CN 201210576378 A CN201210576378 A CN 201210576378A CN 103043968 A CN103043968 A CN 103043968A
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- insulation board
- composite foamed
- foamed cement
- decorative surface
- composite
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- 239000002131 composite material Substances 0.000 title claims abstract description 52
- 239000004568 cement Substances 0.000 title claims abstract description 49
- 238000009413 insulation Methods 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000000835 fiber Substances 0.000 claims abstract description 26
- 238000003756 stirring Methods 0.000 claims abstract description 26
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 24
- 239000003381 stabilizer Substances 0.000 claims abstract description 22
- 239000010881 fly ash Substances 0.000 claims abstract description 18
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical group OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 26
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 24
- 239000000126 substance Substances 0.000 claims description 24
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 20
- 238000010792 warming Methods 0.000 claims description 16
- 238000005187 foaming Methods 0.000 claims description 15
- 239000003469 silicate cement Substances 0.000 claims description 15
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 14
- 239000001110 calcium chloride Substances 0.000 claims description 14
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 14
- 239000010775 animal oil Substances 0.000 claims description 13
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 12
- 235000017550 sodium carbonate Nutrition 0.000 claims description 12
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 12
- 238000010009 beating Methods 0.000 claims description 8
- 238000012856 packing Methods 0.000 claims description 8
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-M Formate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 claims description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- 229910052796 boron Inorganic materials 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- 239000004917 carbon fiber Substances 0.000 claims description 2
- 239000003365 glass fiber Substances 0.000 claims description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 2
- 238000000465 moulding Methods 0.000 claims description 2
- DGVVJWXRCWCCOD-UHFFFAOYSA-N naphthalene;hydrate Chemical group O.C1=CC=CC2=CC=CC=C21 DGVVJWXRCWCCOD-UHFFFAOYSA-N 0.000 claims description 2
- RAFRTSDUWORDLA-UHFFFAOYSA-N phenyl 3-chloropropanoate Chemical compound ClCCC(=O)OC1=CC=CC=C1 RAFRTSDUWORDLA-UHFFFAOYSA-N 0.000 claims description 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 2
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 2
- 239000002002 slurry Substances 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- 229960004418 trolamine Drugs 0.000 claims description 2
- 239000006260 foam Substances 0.000 abstract description 16
- 239000011398 Portland cement Substances 0.000 abstract description 8
- 238000005520 cutting process Methods 0.000 abstract description 7
- 239000004088 foaming agent Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 239000004743 Polypropylene Substances 0.000 description 13
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 12
- 239000002994 raw material Substances 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 238000012423 maintenance Methods 0.000 description 6
- 239000000843 powder Substances 0.000 description 5
- 238000004321 preservation Methods 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 238000010276 construction Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000011449 brick Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000011491 glass wool Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
Landscapes
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention relates to a composite foamed cement insulation board for a tile surface. The insulation board consists of the following components in part by weight: 100 parts of portland cement, 20 to 40 parts of fly ash, 60 to 65 parts of water, 0.3 to 0.5 part of fibers, 1 to 2 parts of early strength agent, 0.5 to 1 part of accelerator, 0.5 to 0.8 part of water reducing agent, 1.3 to 2.0 parts of foam stabilizer and 5.5 to 6.5 parts of foaming agent. A preparation method of the composite foamed cement insulation board comprises the following steps of: firstly, preparing the accelerator; then adding the portland cement, the fly ash, the water, the fibers, the early strength agent, the accelerator and the water reducing agent into a mixing tank to stir and pulp; and finally, adding the foam stabilizer and the foaming agent, pouring the mixture into a die after uniformly stirring, naturally carrying out foam forming in the die, maintaining in the natural state, and finally cutting into blocks and packaging. The composite foamed cement insulation board disclosed by the invention has the tensile bond strength greater than or equal to 0.2MPa and can be used for the tile surface.
Description
Technical field
The present invention relates to a kind of warming plate material, in particular, relate to a kind of composite foaming cement plate insulation that can be used for tile decorative surface and preparation method thereof.
Background technology
According to People's Republic of China's " covil construction outer heat preservation system and decoration of exterior wall fire prevention temporary provisions " second regulation, it is the material of A level that the covil construction heat insulating material for external must adopt combustionproperty, according to this regulation, the original XPS that extensively adopts of covil construction outer heat preservation system, the use that is under an embargo of the organic plates such as EPS, a hundred flowers blossom for the lagging material such as the various warming plates that can reach A level fire-protection standard such as rock cotton board, glass wool, foamed ceramic, multicellular glass, pearlstone on the market.Composite cement foam plate wherein, because it is cheap, raw material sources extensive, excellent performance, occupied higher share in market, yet, the tensile strength of composite foaming cement plate generally is no more than 0.15MPa, the tensile strength of the composite cement foam plate of most manufacturer production can not satisfy on the market the client to the preference of tile decorative surface about 0.10MPa.
Summary of the invention
It is low to the objective of the invention is to overcome the tensile strength that has the existence of composite cement foam plate now, can not be used for the defective of tile decorative surface, a kind of composite foamed cement insulation board is provided, it is large that this warming plate material has a tensile bond strength, satisfying on the basis of building thermal-insulation energy-saving, can be used for tile decorative surface.
For realizing purpose of the present invention, technical scheme of the present invention is:
A kind of composite foamed cement insulation board for tile decorative surface, described warming plate is comprised of the component of following weight part:
100 parts of silicate cements,
Flyash 20-40 part,
Water 60-65 part,
Fiber 0.3-0.5 part,
Hardening accelerator 1-2 part,
Accelerating chemicals 0.5-1 part,
Water reducer 0.5-0.8 part,
Suds-stabilizing agent 1.3-2.0 part,
Whipping agent 5.5-6.5 part.
In a preferred embodiment of the present invention, described silicate cement is 425R silicate cement or 525R silicate cement.
In a preferred embodiment of the present invention, described fiber is one or both and the two or more mixing in PP fiber, carbon fiber, boron fibre, silicon carbide fiber, the alkali resistant glass fibre.
In a preferred embodiment of the present invention, described whipping agent is hydrogen peroxide.
In a preferred embodiment of the present invention, described hardening accelerator is one or both and the two or more mixing in calcium chloride, calcium formiate, sodium sulfate, calcium nitrite, the trolamine.
In a preferred embodiment of the present invention, described accelerating chemicals is formed according to 1:1:2 is composite by yellow soda ash, clorox and calcium sulfate.
In a preferred embodiment of the present invention, described water reducer is naphthalene water reducer or poly carboxylic acid series water reducer.
In a preferred embodiment of the present invention, the aperture of the warming plate that described warming plate material makes is controlled between the 1.5-2.5mm uniformly, change the ratio of water, whipping agent and powder, can obtain the composite foamed cement insulation board of different unit weights, different pore size.
In a preferred embodiment of the present invention, described suds-stabilizing agent is the animal oil suds-stabilizing agent.
Another object of the present invention provides a kind of preparation method of the composite foamed cement insulation board for tile decorative surface, and the method may further comprise the steps:
(1) preparation accelerating chemicals: yellow soda ash, clorox, calcium sulfate are mixed fully according to the ratio of 1:1:2.
(2) will stir making beating in sour silicon salt cement, flyash, water, fiber, hardening accelerator, accelerating chemicals and the water reducer input stirring tank;
(3) add suds-stabilizing agent and whipping agent in the slurries of step (2) gained, after stirring, build to mould, natural foaming moulding in mould is maintained under the state of nature, is cut into piece, packing at last, obtains the composite foaming cement plate.
The present invention has improved its tensile strength by optimizing the prescription of composite cement foam plate, has strengthened the security of sticking brick facing thereon.Composite foamed cement insulation board material unit weight of the present invention is less than 300kg/m3, cost performance is high, the later strength decay is little, its tensile bond strength is much higher than the on the market tensile strength of most composite foaming cement plates more than or equal to 0.2MPa, has greatly improved the security of tiling facing on the thermal insulation layer, can be used for tile decorative surface, therefore, reach on the market under the requirement of heat preservation energy-saving having satisfied, also satisfied on the market the preference for tile decorative surface.
Embodiment
Further specify the present invention below by Comparative Examples and embodiment.
Comparative Examples 1
(1) raw material and proportioning thereof (this prescription is the production formula of our company's ordinary Portland cement foamed board in early stage)
Ordinary Portland cement 75kg,
Flyash 23.15kg,
Water reducer (polycarboxylic acid series) 0.05kg,
Calcium chloride hardening accelerator 1.50kg,
PP fiber 0.30kg,
Water 80.00kg,
Three-dimensional rubber powder 2.0kg,
Hydrogen peroxide 7.5kg,
Animal oil suds-stabilizing agent 2.0kg.
(2) preparation method
To stir in water, ordinary Portland cement, flyash, calcium chloride hardening accelerator, PP fiber, three-dimensional rubber powder and the poly carboxylic acid series water reducer input stirring tank, making beating 3min, then add hydrogen peroxide, animal oil suds-stabilizing agent, stir 5s, build to mould, maintenance, cutting, packing, obtain composite foaming cement board finished product plate.
The related data of gained composite cement foam warming plate sees Table 1.
Comparative Examples 2
This Comparative Examples is on the basis of Comparative Examples 1, change wherein water and the consumption of whipping agent.
(1) raw material and proportioning thereof
Ordinary Portland cement 75kg,
Flyash 23.15kg,
Water reducer (polycarboxylic acid series) 0.05kg,
Calcium chloride hardening accelerator 1.50kg,
PP fiber 0.30kg,
Water 75.00kg,
Three-dimensional rubber powder 2.0kg,
Hydrogen peroxide 6.5kg,
Animal oil suds-stabilizing agent 2.0kg;
(2) preparation method
To stir in water, ordinary Portland cement, flyash, calcium chloride hardening accelerator, PP fiber, three-dimensional rubber powder and the poly carboxylic acid series water reducer input stirring tank, making beating 3min, then add hydrogen peroxide, animal oil suds-stabilizing agent, stir 5s, build to mould, maintenance, cutting, packing, obtain composite foaming cement board finished product plate.
The related data of gained composite cement foam warming plate material sees Table 1.
Embodiment 1
(1) raw material and proportioning thereof
425R silicate cement 100kg,
Flyash 20kg,
Water reducer (polycarboxylic acid series) 0.06kg,
Calcium chloride hardening accelerator 2.0kg,
Accelerating chemicals 0.5kg,
PP fiber 0.4kg,
Water 60kg,
Hydrogen peroxide 6.0kg,
Animal oil suds-stabilizing agent 1.5kg.
Consisting of of accelerating chemicals wherein: yellow soda ash: clorox: calcium sulfate forms according to the ratio of 1:1:2 is composite.
(2) preparation method
Preparation accelerating chemicals: yellow soda ash, clorox, calcium sulfate are mixed fully according to the ratio of 1:1:2.
By above weight, to stir in 425R silicate cement, flyash, water, PP fiber, calcium chloride hardening accelerator, accelerating chemicals and water reducer (polycarboxylic acid series) the input stirring tank, making beating 5min, then add hydrogen peroxide and animal oil suds-stabilizing agent, stir 10s, build to mould, maintenance, cutting, packing, obtain composite foaming cement board finished product plate.
The related data of gained composite cement foam warming plate material sees Table 1.
Embodiment 2
(1) raw material and proportioning thereof
425R silicate cement 100kg,
Flyash 20kg,
Water reducer (naphthalene system) 0.5kg,
Calcium chloride hardening accelerator 2.0kg,
Accelerating chemicals 0.5,
PP fiber 0.4kg,
Water 60kg,
Hydrogen peroxide 6.0kg,
Animal oil suds-stabilizing agent 1.5kg;
Consisting of of accelerating chemicals wherein: yellow soda ash: clorox: calcium sulfate forms according to the ratio of 1:1:2 is composite.
(2) preparation method
Preparation accelerating chemicals: yellow soda ash, clorox, calcium sulfate are mixed fully according to the ratio of 1:1:2.
By above weight, to stir in 425R silicate cement, flyash, water, PP fiber, calcium chloride hardening accelerator, accelerating chemicals and water reducer (naphthalene system) the input stirring tank, making beating 5min, then add hydrogen peroxide and animal oil suds-stabilizing agent, stir 10s, build to mould, maintenance, cutting, packing, obtain composite foaming cement board finished product plate.
The related data of gained composite cement foam warming plate material sees Table 1.
Embodiment 3
(1) raw material and proportioning thereof
525R ordinary Portland cement 100kg,
Flyash 20kg,
Water reducer (naphthalene system) 0.5kg,
Calcium chloride hardening accelerator 1.0kg,
Accelerating chemicals 1.0kg,
PP fiber 0.4kg,
Water 60kg,
Hydrogen peroxide 6.0kg,
Animal oil suds-stabilizing agent 1.5kg;
Consisting of of accelerating chemicals wherein: yellow soda ash: clorox: calcium sulfate forms according to the ratio of 1:1:2 is composite.
(2) preparation method
Preparation accelerating chemicals: yellow soda ash, clorox, calcium sulfate is fully composite evenly according to the ratio of 1:1:2.
By above weight, to stir in 525R silicate cement, flyash, water, PP fiber, calcium chloride hardening accelerator, accelerating chemicals and water reducer (naphthalene system) the input stirring tank, making beating 5min, then add hydrogen peroxide and animal oil suds-stabilizing agent, stir 10s, build to mould, maintenance, cutting, packing, obtain composite foaming cement board finished product plate.
The related data of gained composite cement foam warming plate material sees Table 1.
Embodiment 4
(1) raw material and proportioning thereof
525R silicate cement 100kg,
Flyash 40kg,
Water reducer (naphthalene system) 0.8kg,
Calcium chloride hardening accelerator 0.75kg,
Accelerating chemicals 0.75kg,
PP fiber 0.4kg,
Water 65kg,
Hydrogen peroxide 6.5kg,
Animal oil suds-stabilizing agent 1.8kg.
Consisting of of accelerating chemicals wherein: yellow soda ash: clorox: calcium sulfate forms according to the ratio of 1:1:2 is composite.
(2) preparation method
Preparation accelerating chemicals: yellow soda ash, clorox, calcium sulfate are mixed fully according to the ratio of 1:1:2.
By above weight, to stir in 525R silicate cement, flyash, water, PP fiber, calcium chloride hardening accelerator, accelerating chemicals and water reducer (naphthalene system) the input stirring tank, making beating 15min, then add suds-stabilizing agent and whipping agent, stir 20s, build to mould, maintenance, cutting, packing, obtain composite foaming cement board finished product plate.
The related data of gained composite cement foam warming plate material sees Table 1.
The related data of the composite cement foam warming plate that Comparative Examples 1-2 and embodiment 1-4 produce is as shown in table 1.(according to the standard among the JC/T041-2011 of " composite foaming cement plate exterior wall external heat preservation system utilisation technology rules " Soviet Union):
Table 1
Enclose Jiangsu Province's foam cement plate standard
As can be seen from the above table, fire prevention composite foamed cement insulation board material of the present invention reaches the standard among the JC/T041-2011 of " composite foaming cement plate exterior wall external heat preservation system utilisation technology rules " Soviet Union fully, especially its tensile strength has reached 0.2MPa, has satisfied the requirement of sticking brick facing on the foam cement plate.
More than show and described ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that describes in above-described embodiment and the specification sheets just introduces principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (10)
1. composite foamed cement insulation board that is used for tile decorative surface is characterized in that described warming plate material is comprised of the component of following weight part:
100 parts of silicate cements,
Flyash 20-40 part,
Water 60-65 part,
Fiber 0.3-0.5 part,
Hardening accelerator 1-2 part,
Accelerating chemicals 0.5-1 part,
Water reducer 0.5-0.8 part,
Suds-stabilizing agent 1.3-2.0 part,
Whipping agent 5.5-6.5 part.
2. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described silicate cement is 425R silicate cement or 525R silicate cement.
3. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described fiber is one or both and the two or more mixing in PP fiber, carbon fiber, boron fibre, silicon carbide fiber, the alkali resistant glass fibre.
4. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described whipping agent is hydrogen peroxide.
5. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described hardening accelerator is one or both and the two or more mixing in calcium chloride, calcium formiate, sodium sulfate, calcium nitrite, the trolamine.
6. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described accelerating chemicals is formed according to 1:1:2 is composite by yellow soda ash, clorox and calcium sulfate.
7. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described water reducer is naphthalene water reducer or poly carboxylic acid series water reducer.
8. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, the aperture of the warming plate that described warming plate material makes is controlled between the 1.5-2.5mm uniformly.
9. the composite foamed cement insulation board for tile decorative surface according to claim 1 is characterized in that, described suds-stabilizing agent is the animal oil suds-stabilizing agent.
10. method for preparing the described composite foamed cement insulation board for tile decorative surface of each claim of claim 1 to 9 is characterized in that the method may further comprise the steps:
(1) preparation accelerating chemicals: yellow soda ash, clorox, calcium sulfate are mixed fully according to the ratio of 1:1:2.
(2) will stir making beating in sour silicon salt cement, flyash, water, fiber, hardening accelerator, accelerating chemicals and the water reducer input stirring tank;
(3) add suds-stabilizing agent and whipping agent in the slurries of step (2) gained, after stirring, build to mould, natural foaming moulding in mould is maintained under the state of nature, is cut into piece, packing at last, obtains the composite foaming cement plate.
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| CN201210576378.7A CN103043968B (en) | 2012-12-26 | 2012-12-26 | Composite foamed cement insulation board for tile surface and preparation method thereof |
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| CN201210576378.7A CN103043968B (en) | 2012-12-26 | 2012-12-26 | Composite foamed cement insulation board for tile surface and preparation method thereof |
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| CN103979895A (en) * | 2014-05-20 | 2014-08-13 | 潜山县新型工程建筑材料有限公司 | Composite foamed cement board and preparation method thereof |
| CN104058785A (en) * | 2014-06-30 | 2014-09-24 | 江苏新光环保工程有限公司 | Foamed cement insulation board |
| CN104108895A (en) * | 2014-06-19 | 2014-10-22 | 广东省建筑科学研究院 | Low-density foaming cement and preparation method thereof |
| CN104446631A (en) * | 2014-12-18 | 2015-03-25 | 无锡伊诺永利文化创意有限公司 | Composite foamed cement board |
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| CN115446982A (en) * | 2022-09-14 | 2022-12-09 | 李赞国 | Foamed cement material and manufacturing method thereof |
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Cited By (19)
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