CN103030819A - Preparation method of emulsifying wax - Google Patents
Preparation method of emulsifying wax Download PDFInfo
- Publication number
- CN103030819A CN103030819A CN 201110299516 CN201110299516A CN103030819A CN 103030819 A CN103030819 A CN 103030819A CN 201110299516 CN201110299516 CN 201110299516 CN 201110299516 A CN201110299516 A CN 201110299516A CN 103030819 A CN103030819 A CN 103030819A
- Authority
- CN
- China
- Prior art keywords
- temperature
- emulsifying
- wax
- preparation
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Colloid Chemistry (AREA)
Abstract
The invention discloses a preparation method of emulsifying wax, belongs to the technical field of chemical industry, and particularly relates to a preparation method of emulsifying wax. The invention provides the preparation method of the emulsifying wax with little irritation and reliable performance. The technical scheme adopted by the invention comprises the following steps of placing paraffin wax, beeswax and carnauba wax into a beaker, heating the beaker in a constant temperature water bath at the temperature of 90 to 95 DEG C; placing the molten wax in the magnetic stirring apparatus for stirring; adding vegetable oil (solvent oil) which is preheated at the temperature of 75 DEG C; evenly stirring the mixture, then adding compound emulsifier in sequence; evenly stirring the mixture again, adding hot water of the temperature of 90 to 95 DEG C and cold water of the temperature of 25 DEG C in sequence for emulsifying, wherein the emulsifying temperature is between 70 and 90 DEG C, the emulsifying time is controlled to be 10-40 minutes; and after the emulsion is cooled to the temperature of about 50 DEG C, adding an abraser, stirring and cooling the emulsion to the temperature of 25 DEG C to obtain a product.
Description
Technical field:
The invention belongs to chemical technology field, in particular, relate to a kind of preparation method of emulsifying wax.
Background technology:
Paraffin is valuable petrochemical complex resource, not only can directly use, and can also be used to the high value-added products such as production special wax, Wax special.Along with developing rapidly of automotive industry, China Auto Market entered take the Growth Development phase of mass consumption as the basis, and China will become one of Car Consumption state the biggest in the world.Vehicle particularly private car is vigorous with polishing wax and the rumbling compound series products market requirement.
At present, the product of polishing wax mainly is to make thinner with organic solvent on the market, and unpleasant taste is not only arranged, and skin, eyes and respiratory tract are had certain hormesis, simultaneously environment is also polluted.
Summary of the invention:
The present invention is exactly for the problems referred to above, provides that a kind of pungency is little, the preparation method of the emulsifying wax of stable performance.
In order to realize above-mentioned purpose of the present invention, the present invention adopts following technical scheme, preparation process of the present invention is: first paraffin, beeswax, carnauba wax are put into beaker, in constant water bath box, be heated to 90～95 ℃, after wax melts, be placed on the magnetic stirring apparatus and stir, adding is preheating to 75 ℃ vegetables oil (solvent oil), adds successively composite emulsifier after stirring; After again stirring, add successively 90～95 ℃ hot water and 25 ℃ cold water and carry out emulsification, emulsifying temperature is 70～90 ℃, and emulsification times is controlled at 10～40min; Treat that emulsion is cooled to about 50 ℃, add abrasive, stirring is cooled to 25 ℃ and namely gets product.
Beneficial effect of the present invention:
1. water consumption substitution organic solvent of the present invention is made thinner, the light wax on the preparation emulsion-type automobile, and pungency is little, toxicity is low;
2. the emulsified olefin stable performance of the present invention's preparation.
Embodiment:
Preparation process of the present invention is: first paraffin, beeswax, carnauba wax are put into beaker, in constant water bath box, be heated to 90～95 ℃, after wax melts, be placed on the magnetic stirring apparatus and stir, adding is preheating to 75 ℃ vegetables oil (solvent oil), adds successively composite emulsifier after stirring; After again stirring, add successively 90～95 ℃ hot water and 25 ℃ cold water and carry out emulsification, emulsifying temperature is 70～90 ℃, and emulsification times is controlled at 10～40min; Treat that emulsion is cooled to about 50 ℃, add abrasive, stirring is cooled to 25 ℃ and namely gets product.
The present invention selects emulsifying temperature and emulsification times as the factor that affects emulsifying wax stability, can see Table 1, table 2.
Table 1 emulsifying temperature is on the impact of emulsifying wax stability
| Sequence number | Temperature/℃ | Stability |
| 1 | 70 | 3 |
| 2 | 75 | 2 |
| 3 | 80 | 2 |
| 4 | 85 | 1 |
| 5 | 90 | 1 |
Table 2 emulsification times is on the impact of emulsifying wax stability
| Sequence number | Time/min | Stability |
| 1 | 10 | 2 |
| 2 | 20 | 1 |
| 3 | 30 | 1 |
| 4 | 40 | 1 |
Numeral the stability of emulsification system and the phenomenon that emulsification system is: 1 is good homogeneity; 2 is that preliminary visible denseness is uneven; 3 is to inhomogeneous clear conversion; 4 is the separation of preliminary visible phase; 5 is the separation of obviously visible phase; 6 are two separates mutually fully.
As a kind of preferred version, preparation process of the present invention is: in the emulsion process, emulsifying temperature is 85 ℃, and emulsification times is 20min.
Claims (2)
1. the preparation method of an emulsifying wax, it is characterized in that, the present invention adopts following technical scheme, preparation process is: first paraffin, beeswax, carnauba wax are put into beaker, in constant water bath box, be heated to 90～95 ℃, be placed on the magnetic stirring apparatus after wax melts and stir, adding is preheating to 75 ℃ vegetables oil (solvent oil), adds successively composite emulsifier after stirring; After again stirring, add successively 90～95 ℃ hot water and 25 ℃ cold water and carry out emulsification, emulsifying temperature is 70～90 ℃, and emulsification times is controlled at 10～40min; Treat that emulsion is cooled to about 50 ℃, add abrasive, stirring is cooled to 25 ℃ and namely gets product.
2. the preparation method of a kind of emulsifying wax according to claim 1 is characterized in that, preparation process of the present invention is: in the emulsion process, emulsifying temperature is 85 ℃, and emulsification times is 20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110299516 CN103030819A (en) | 2011-10-08 | 2011-10-08 | Preparation method of emulsifying wax |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110299516 CN103030819A (en) | 2011-10-08 | 2011-10-08 | Preparation method of emulsifying wax |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103030819A true CN103030819A (en) | 2013-04-10 |
Family
ID=48018249
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110299516 Pending CN103030819A (en) | 2011-10-08 | 2011-10-08 | Preparation method of emulsifying wax |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103030819A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103409069A (en) * | 2013-07-24 | 2013-11-27 | 吴江市利达上光制品有限公司 | Preparation method of nano emulsified shoe polish |
| CN103468151A (en) * | 2013-09-05 | 2013-12-25 | 常熟市三新红木家具厂 | Cleaning solution for redwood furniture |
| CN103468152A (en) * | 2013-09-05 | 2013-12-25 | 常熟市三新红木家具厂 | Preparation method of cleaning solution for redwood furniture |
| CN103614083A (en) * | 2013-12-03 | 2014-03-05 | 沈阳化工大学 | Automobile cleaning water wax and preparation method thereof |
| CN104789263A (en) * | 2015-03-27 | 2015-07-22 | 辽宁科技大学 | Multifunctional emulsifying wax and preparation method thereof |
| CN107629702A (en) * | 2017-10-10 | 2018-01-26 | 苏州百益倍肯新材料科技有限公司 | A kind of leather is except net taste brightener of aldehyde and preparation method thereof |
-
2011
- 2011-10-08 CN CN 201110299516 patent/CN103030819A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103409069A (en) * | 2013-07-24 | 2013-11-27 | 吴江市利达上光制品有限公司 | Preparation method of nano emulsified shoe polish |
| CN103468151A (en) * | 2013-09-05 | 2013-12-25 | 常熟市三新红木家具厂 | Cleaning solution for redwood furniture |
| CN103468152A (en) * | 2013-09-05 | 2013-12-25 | 常熟市三新红木家具厂 | Preparation method of cleaning solution for redwood furniture |
| CN103614083A (en) * | 2013-12-03 | 2014-03-05 | 沈阳化工大学 | Automobile cleaning water wax and preparation method thereof |
| CN104789263A (en) * | 2015-03-27 | 2015-07-22 | 辽宁科技大学 | Multifunctional emulsifying wax and preparation method thereof |
| CN107629702A (en) * | 2017-10-10 | 2018-01-26 | 苏州百益倍肯新材料科技有限公司 | A kind of leather is except net taste brightener of aldehyde and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103030819A (en) | Preparation method of emulsifying wax | |
| JP2019151659A (en) | Production of partially refined waste glycerol | |
| GB2596482A (en) | A method and feedstock for producing hydrocarbons | |
| CN103878017B (en) | A kind of base metal isomerization catalyst and method for making thereof and application | |
| CN104232160B (en) | A kind of low viscosity white oil | |
| CN103420413B (en) | A kind of method of purification and recover titanium tetrachloride from titaniferous waste liquid | |
| CN108265089B (en) | Oil and fat composition containing 1, 3-dioleoyl-2-palmitic acid triglyceride and preparation method thereof | |
| CN105349257A (en) | Butter refining deodorizing process | |
| CN104084089A (en) | Preparation method of rosin emulsifying agent | |
| CN108239301B (en) | Emulsion type composite antioxidant and preparation method thereof | |
| CN103937616A (en) | Method for extracting high-purity unsaturated fatty acid from soybean oil | |
| CN102140254A (en) | Method for preparing high-efficiency modified asphalt | |
| JP6179901B2 (en) | Method for producing an oil composition | |
| CN107417933A (en) | The preparation method of high stability paraffin wax emulsions | |
| CN112655778B (en) | Preparation method of transesterification rice bran fixed-ester mold release oil | |
| WO2011109465A3 (en) | High shear system and process for the production of halogenated and/or sulfonated paraffins | |
| CN107541255A (en) | A kind of method of alumina composite graphene carrier hydrogenation catalyst Porous deproteinized bone production isoheptane solvent naphtha | |
| CN101928482B (en) | Water-soluble low-temperature immobilized metal, glass baking varnish and preparation method thereof | |
| CN112111026B (en) | Method for coagulating isoprene rubber solution | |
| CN105802730A (en) | Method for deacidifying rice bran oil by using enzymic method | |
| CN105154222A (en) | Phosphatide removal method for grease | |
| CN105602451B (en) | A kind of production method of offset litho printing ink gel varnish | |
| TH146806A (en) | Method for producing oil composition | |
| CN105614432A (en) | Functional food composition and preparation method thereof | |
| CN107541253A (en) | A kind of method of aluminum oxide, calcium powder complex carrier hydrogenation catalyst Porous deproteinized bone production isoheptane solvent naphtha |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| DD01 | Delivery of document by public notice |
Addressee: Wang Haiqing Document name: Notification that Application Deemed to be Withdrawn |
|
| C05 | Deemed withdrawal (patent law before 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130410 |