CN102951791A - Convex-surface low-pressure air glass, flat low-pressure air glass and preparation method thereof - Google Patents

Convex-surface low-pressure air glass, flat low-pressure air glass and preparation method thereof Download PDF

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CN102951791A
CN102951791A CN2012100756128A CN201210075612A CN102951791A CN 102951791 A CN102951791 A CN 102951791A CN 2012100756128 A CN2012100756128 A CN 2012100756128A CN 201210075612 A CN201210075612 A CN 201210075612A CN 102951791 A CN102951791 A CN 102951791A
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glass
solder
low
low latitude
temperature
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CN102951791B (en
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戴长虹
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Haining Yuanhua Town Industrial Investment Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

Abstract

The invention provides low-pressure air glass which comprises upper glass and lower glass, wherein the peripheries of the upper glass and lower glass are welded together by low-temperature solder; a closed low-pressure air layer is formed between the upper glass and the lower glass; the upper glass and the lower glass are flat glass or convex-surface glass; and the convex surface of the convex-surface glass faces to the outer side. A preparation method of the low-pressure air glass provided by the invention is simple in technology; the prepared low-pressure air glass and toughened low-pressure air glass can overcome the shortcomings of the existing hollow glass, effectively guarantee the air tightness of the low-pressure air glass, prolong the service life of the low-pressure air glass, enhance the strength as well as the heat insulation and sound insulation performance, and reduce light pollution of a glass curtain wall.

Description

Convex surface low latitude glass, dull and stereotyped low latitude glass and preparation method thereof
Technical field
The present invention relates to the glass processing technical field, relate in particular to a kind of low latitude glass and preparation method thereof.
Background technology
Along with the reinforcement of environmental protection and energy saving consciousness, double glazing has obtained applying widely, Effective Raise the insulation of door and window, sound insulation property.Distance between two sheet glass of double glazing, be the effect that the thickness of gas cloud has determined insulation, sound insulation, gas cloud is thicker, and then insulation and defening effect are better, but the thickness that increases gas cloud can increase the thickness of sash, thereby can increase the cost of manufacture of door and window; Other method is as adopting coated glass, pad pasting and fill the measure such as rare gas element in the middle of double glazing, though certain effect is arranged, cost is very high, is not suitable for generally using.
Existing double glazing mostly is to use the interval box with siccative to separate peripheral glasswork with organic sealant sealing in the middle of the glass more than two or two.Owing to organic seal gum self contains the reasons such as moisture, ageing resistance is relatively poor, resistance to air loss is bad, cause double glazing that failure phenomenon often occurs, had a strong impact on the work-ing life of double glazing.
Air in the double glazing gas cloud is sealed between two blocks of glass, because the variation of outside temperature, can cause the pressure of gas cloud to change, pressure was greater than normal atmosphere, glass evagination when outside temperature was high, pressure was less than normal atmosphere, glass indent when outside temperature was low, produce so-called " breathing " phenomenon, thereby affect the normal working life of double glazing.
Present many City Buildings adopt glass curtain wall to make extraneous adornment, but there is serious reflective harm in glass curtain wall, wherein white bright pollution is the most general light pollution that glass curtain wall causes, and also has same problem when adopting existing double glazing to make curtain wall material.
Summary of the invention
Technical problem to be solved by this invention is the defective that is for existing double glazing existence, a kind of novel subatmospheric double glazing is provided---low latitude glass, tempering low latitude glass and preparation method thereof, the making method technique of this low latitude glass is simple, prepared low latitude glass and tempering low latitude glass can overcome the deficiency of existing double glazing, can effectively guarantee low latitude glass resistance to air loss, increase the service life, and can gain in strength and heat insulation, sound-proofing properties and alleviate the glass curtain wall light pollution.
In order to solve the problems of the technologies described above, the invention provides a kind of convex surface low latitude glass, it comprises: upper glass, lower-glass, the periphery of described upper glass and described lower-glass welds together by solder, form the subatmospheric hollow layer of a sealing between described upper glass and the described lower-glass---low dead level, described upper glass and described lower-glass are convex glasses, and convex surface toward the outer side.
Wherein, described low dead level be at high temperature edge sealing, be down to self-assembling formation after the room temperature, the air pressure in the described low dead level is determined by the fusing point of solder, is generally 0.01 ~ 0.09MPa, is preferably 0.02 ~ 0.07MPa.
Wherein, the convex surface of described convex glass bow height is not less than 0.1mm, is preferably 1 ~ 200mm.
Wherein, have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass.
Wherein, described convex surface low latitude glass can also comprise one flat plate glass, and described sheet glass is clipped between described upper glass and the described lower-glass, and described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass.
In order to solve the problems of the technologies described above, the invention provides the preparation method of above-mentioned convex surface low latitude glass, it comprises:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove;
The 3rd step evenly was coated with solder with two blocks of glass of second step acquisition or the face of weld periphery of a glass, evenly leaves several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, and sent in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
In order to solve the problems of the technologies described above, the invention provides the preparation method of above-mentioned convex surface low latitude glass, when described convex surface low latitude glass was convex surface tempering low latitude glass, the preparation method was as follows:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing;
The 3rd step, two blocks of glass of second step acquisition or the face of weld periphery of a glass evenly are coated with solder, evenly leave several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
In order to solve the problems of the technologies described above, the invention provides a kind of dull and stereotyped low latitude glass, it comprises: upper and lower glass, described upper and lower glass is sheet glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, have in the described low dead level to be the upholder that dot matrix is arranged, have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass.
Wherein, described dull and stereotyped low latitude glass can also comprise one flat plate glass, and described sheet glass is clipped between described upper glass and the described lower-glass, and described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass.
Wherein, described edge band frame adopts the preparation of printing cryogenic glass powder.
Wherein, above support is made by metal, pottery or glass, and the preferred printing cryogenic glass powder that adopts prepares.
In order to solve the problems of the technologies described above, the invention provides the preparation method of above-mentioned dull and stereotyped low latitude glass, it comprises:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology and cryogenic glass powder to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, after guaranteeing upper and lower glass alignment, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, solder is a little more than the edge band frame, evenly distributing on it, several pass through the groove of solder or slit as production well, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
In order to solve the problems of the technologies described above, the invention provides the preparation method of above-mentioned dull and stereotyped tempering low latitude glass, it comprises:
The first step according to the shape of the low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, at least one in the glass after two processing is utilized printing technology and cryogenic glass powder to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, after guaranteeing upper and lower glass alignment, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass; And two blocks of glass are sent into carry out tempering in the annealing furnace and process;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, solder is a little more than the edge band frame, evenly distributing on it, several pass through the groove of solder or slit as production well, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
The invention has the beneficial effects as follows:
Low latitude of the present invention glass is a kind of novel glass between double glazing and vacuum glass, utilizes high temperature edge sealing sealing, is down to after the room temperature and automatically forms the subatmospheric gas cloud between the upper and lower glass.Compare with double glazing, replace organic adhesive and normal temperature edge sealing with inorganic scolder and high temperature edge sealing, greatly improved sealing property and prolonged work-ing life; The air rarefaction of low dead level, water molecules and oxygen equal size are lower, not only can not haze, frosting, and the oxidation that has alleviated low-radiation film, thin air also make heat insulation and sound-proofing properties better; The air pressure of low dead level is all the time less than normal atmosphere, so there is not " breathing " phenomenon.Compare with existing vacuum glass, do not need to vacuumize, few with or without upholder, production technique is more simple, cost is lower, the pressure that bears in the glass use procedure is less, longer service life.
Low latitude of the present invention is on glass, lower-glass is convex glass, because glass itself has very high ultimate compression strength, resist normal atmosphere so rely on the shape of convex glass, can not put or put less upholder, not only simplify low latitude glass manufacture craft, reduce production costs, so that the production of low latitude glass is more easy, and can improve transparency, intensity and heat insulation, sound insulation and the resisting wind press capacity of low latitude glass.The low latitude is on glass, the periphery of lower-glass contains the edge band frame, so that the edge sealing of low latitude glass is easier, the mutual chimeric sealing effectiveness of glass under deformation that guaranteed of edge band frame up and down, have the bonding strength higher than solder between edge band frame and the upper lower-glass, sealing surface area and airtight layer thickness between the upper lower-glass have been increased, sticking power and the adhesion strength of sealing-in have greatly been strengthened, on having increased, the tightness of low dead level between the lower-glass, improved the life-span of low latitude glass, realize that single stage method prepares low latitude glass and tempering low latitude glass, promote the suitability for industrialized production of low latitude glass and tempering low latitude glass, greatly improve productivity and the qualification rate of low latitude glass, reduce the production cost of low latitude glass.In addition, convex glass can with light scatter, effectively alleviate the light pollution of glass curtain wall.
 
Description of drawings
Fig. 1 is convex surface of the present invention low latitude glass structure synoptic diagram;
Fig. 2 is the convex surface low latitude glass structure synoptic diagram that lower-glass of the present invention has the edge band frame;
Fig. 3 is the convex surface low latitude glass structure synoptic diagram that upper lower-glass of the present invention all has the edge band frame;
Fig. 4 is that upper lower-glass of the present invention all has edge band frame and lower-glass that the dull and stereotyped low latitude glass structure synoptic diagram of upholder is arranged;
Fig. 5 is that upper lower-glass of the present invention all has edge band frame and lower-glass that the low latitude glass structure synoptic diagram of upholder is arranged;
Fig. 6 is the dull and stereotyped low latitude glass structure synoptic diagram that upper lower-glass of the present invention all has edge band frame and upholder;
Fig. 7 is the convex surface low latitude glass structure synoptic diagram of two low dead levels of the present invention;
Fig. 8 is the convex surface low latitude glass structure synoptic diagram of upper lower-glass of the present invention two low dead levels that the edge band frame is all arranged.
Among the figure: 1. upper glass, 2. lower-glass, 3. solder, 4. the edge band frame on the lower-glass, 5. the edge band frame of upper glass, the 6. upholder on the lower-glass, the 7. upholder on the upper glass, 8. intermediate glass.
 
Embodiment
The invention provides a kind of convex surface low latitude glass, it comprises: upper glass, lower-glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, air pressure in the described low dead level is 0.01 ~ 0.09MPa, described upper glass and described lower-glass are convex glasses, and the bow height of described convex glass is not less than 0.1mm, and convex surface toward the outer side.
Described convex surface low latitude glass can also comprise one flat plate glass, and described sheet glass is clipped between described upper glass and the described lower-glass, and described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass.
Described convex surface low latitude glass may further include polylith sheet glass, thereby comprises the low dead level of a plurality of sealings.
The convex shape that the upper glass of convex surface low latitude glass and lower-glass utilize glass is resisted normal atmosphere, makes two blocks of glass can not press together, keep low dead level between two glass, has saved the very large upholder of making and installation difficulty; Do not had stopping of upholder, transparency and the visibility of low latitude glass are better; Do not had the conduction of upholder, the heat insulation and sound-proofing properties of low latitude glass is better; Convex configuration makes glass that higher ultimate compression strength and bending strength be arranged, and the resisting wind press capacity of low latitude glass is better; Convex configuration makes low dead level that larger space be arranged, and more can keep for a long time the life-span of low dummy status, low latitude glass longer, even lose the low latitude, its performance also is better than general double glazing.
Air pressure in the described low dead level is preferably 0.02 ~ 0.07MPa, more preferably 0.03 ~ 0.05MPa.
The convex surface bow height of upper and lower two blocks of convex glasses of described low latitude glass is preferably 1~200mm, and more preferably 3~20mm is advisable not protrude from outside the sash during as windowpane.
Described upper and lower glass can have identical bow height, also can have according to the difference of width inside and outside the sash different bows high.
Described upper and lower glass is prepared from by sheet glass, and its preparation method further comprises: utilize mould by the gravity of glass self or the pressure that adds sheet glass to be prepared into convex glass in bending furnace.
Described preparation method further comprises:
The first step is cut two blocks of sheet glass of required size according to the shape and size of the convex surface low latitude glass of required making, carries out edging, chamfering, cleaning and drying treatment;
Second step, two blocks of sheet glass after processing are respectively charged into forming mould, put into bending furnace, be warming up to glass transition temperature, rely on the gravity of glass self to make glass form convex surface downwards, subsequently furnace temperature is down to room temperature, namely obtains to be shaped as the upper and lower glass of convex glass.
Be toughened glass if obtain the material of upper and lower glass, in described second step, two blocks of sheet glass after processing are respectively charged into forming mould, put into bending furnace, be warming up to glass transition temperature, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing, namely acquisition is shaped as convex glass, material is the upper and lower glass of toughened glass.
Described glass transition temperature is preferably 550 ℃~750 ℃.
The convex surface bow of described convex surface low latitude glass high shape and size and purposes decision by glass, under the prerequisite that satisfies opposing normal atmosphere and purposes, bow is high as small as possible, be advisable with 3 ~ 9mm when being used for the common door window glass, the space that 6 ~ 18mm is namely arranged between two blocks of glass, be equivalent to existing double glazing, under atmospheric pressure almost plane is best, to obtain preferably visual effect and to reduce the cost of described low latitude glass and the space that takies.
Described solder comprises commercially available low temperature glass solder and low melting point metal or solder, described low temperature glass solder preferred molten temperature is 400 ℃~450 ℃ crown glass scolder, the preferred tin of described low melting point metal or solder and tin alloy, zinc and zinc alloy, Magnesium and magnesium alloys etc., its shape or form are powder, cream, silk, paper tinsel etc.
Described solder is coated on one or two face of weld periphery and the face of weld periphery of described sheet glass of upper and lower glass at least.
The formation of described single low dead level convex surface low latitude glass can adopt single stage method to form, and described single stage method comprises the steps:
With the even coating solder of one in the upper and lower glass or two face of weld periphery, evenly leave several grooves that pass through the eutectic welding strip or slit on the solder as production well; Upper and lower glass consistency from top to bottom is stacked together, sends in the high temperature edge sealing stove; Heating rises to more than the melt temperature of solder the interior temperature of stove, reaches the edge sealing temperature, and production well disappears; Stopped heating reduces furnace temperature to room temperature, and described solder welds together upper and lower glass is bubble-tight, thereby obtains needed convex surface low latitude glass.
It is as follows that the single stage method of described two low dead level convex surface low latitude glass forms step:
The periphery of upper convex glass, lower convex glass and middle sheet glass face of weld evenly is coated with solder, evenly leave several grooves that pass through the eutectic welding strip or slit on the solder as production well, and three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove; Heating makes that temperature rises to more than the melt temperature of solder in the stove, reaches the edge sealing temperature, and production well disappears, stopped heating, with the stove cooling, and solder hermetic welds together two blocks of glass, opens fire door and obtains required convex surface low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
Described high temperature edge sealing stove or the single-unit furnace of batch production, or the tunnel kiln of continous way production, preferred tunnel kiln.
Atmosphere or air in the described high temperature edge sealing stove, or the neutral atmospheres such as nitrogen, argon gas, preferred argon gas.
When the atmosphere in the high temperature edge sealing stove is neutral atmosphere, by transmission and the exchange of gas under the high temperature, can reduces moisture and oxygen content in the low dead level of low latitude glass, thereby further improve the performance of low latitude glass.
 
Described high temperature edge sealing stove or the single-unit furnace of batch production, or the tunnel kiln of continous way production, preferred tunnel kiln.
Atmosphere or air in the described high temperature edge sealing stove, or the neutral atmospheres such as nitrogen, argon gas, preferred argon gas.
When the atmosphere in the high temperature edge sealing stove is neutral atmosphere, by transmission and the exchange of gas under the high temperature, can reduces moisture and oxygen content in the low dead level of low latitude glass, thereby further improve the performance of low latitude glass.
When preparation be toughened glass the time, preferentially select low melting point metal or solder, to select lower edge sealing temperature.
When the preparation be toughened glass the time, the problem of annealing because welding temperature is too high, high temperature edge sealing stove can have basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, high temperature edge sealing furnace interior and glass heats to a basal temperature are preferably 280~320 ℃; The modes such as recycling resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating are that local heating is carried out in the edge sealing position to the periphery of glass, reach the purpose that at short notice solder is heated to melting.
The mode of employing automatic edge sealing in high temperature edge sealing stove has been simplified technological process, has lowered production cost, has shortened the production cycle, has been improved production efficiency.
Because tempering and semi-tempered glass have higher intensity, so under identical shape and size, the convex surface of tempering or half tempered convex glass bow height can be less, tempering or half tempered convex glass can be more flat.Owing to utilize forming mould with upper and lower mould, glass clamp is relied on the moulding of exerting pressure between upper and lower mould, so convex glass has more regular shape, and prevent distortion in toughening process, so edge sealing is simpler, sealing property and intensity are also higher.Because high temperature edge sealing stove and accessory has basic heating system and local heating system, the temperature of glass edge is rapidly heated to welding temperature, and tempering or semi-tempered glass are under lower basal temperature, in the long period and higher local temperature, in short time phenomenon can not occur significantly to anneal, so can guarantee to obtain tempering or half tempered low latitude glass.
In the described low dead level, when high large, the convex shape that can rely on glass self of less or convex surface bow and intensity opposing normal atmosphere, can not establish upholder when the planar dimension of upper and lower glass; When upper and lower glass can not rely on the convex shape of self and during intensity opposing normal atmosphere, the upholder of a small amount of necessity should be set, upholder is resisted normal atmosphere jointly with glass.
Do not had stopping of upholder, transparency and the visibility of convex surface low latitude glass are better; Do not had the conduction of upholder, the heat insulation and sound-proofing properties of convex surface low latitude glass is better.
The material of above support is metal, pottery, glass or plastics, is preferably low temperature glass.
The above support minimum unit can be that the dot matrix of equilateral triangle is arranged, and the leg-of-mutton length of side is about 30~300mm, is preferably 50~150mm; Upholder is strip, its length is 0.3~5.0 mm, be preferably 0.5~2.0 mm, width is 0.1~2.0mm, be preferably 0.2~1.0mm, be 0.1~10.0mm highly, be preferably 0.5~3.0mm, the height of upholder be higher than the edge band frame height 0.1~2.0mm, be preferably 0.1~0.5mm; Upholder also can be for cylindric, its diameter is 0.1~3.0mm, be preferably 0.3~2.0mm, be 0.1~5.0 mm highly, be preferably 0.5~3.0mm, two blocks of glass closed sheet rear support thing position spatial altitude 0~0.3 mm, are preferably 0.1~0.2mm about the height of upholder was higher than.
Upholder preferably adopts cryogenic glass powder or low temperature glass solder to utilize printing technology to make, and the sintering temperature of described low temperature glass solder is lower than cryogenic glass powder.
When upholder is printed on one when on glass, be preferably cylindric; When upholder is printed on up and down two when on glass simultaneously, be preferably strip.
When upholder was printed before glass tempering, preferred cryogenic glass powder was made; When upholder was printed behind glass tempering, preferred low temperature glass solder was made.
When upper lower-glass all has the strip upholder, the upholder vertical pile supports, upper lower-glass still is the some contact by upholder, and contact for line between upholder and the glass, increased contact area, reduced the tension stress of glass in support place, thus the quantity of upholder can be reduced, thus further improve the transparency of glass, heat insulation and sound-proofing properties.
The material of described upper and lower glass can be simple glass or toughened glass or semi-tempered glass or low emissivity glass or wire glass or rolled glass or hot melt glass, or the combination of above any two or three kinds of glass, more preferably toughened glass, semi-tempered glass and low emissivity glass.
The shape and size of described low latitude glass determine that by the purposes of low latitude glass satisfying under the prerequisite of service requirements, its shape is preferably square or circular.
Have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass.
The height of described edge band frame is preferably 0.1~10mm, 0.1~1mm more preferably, and width is preferably 0.2~5mm, more preferably 1~2mm.
Can leave several production wells on the described edge band frame, namely perpendicular to the edge band frame and along the equally distributed groove of edge band frame or slit, quantity determines that by the girth of upper and lower glass the about 50~150mm of spacing is advisable, and can seal described production well after described solder fusing; Also can not reserve pore, the passage that discharge as gas between glass in the formed space, rough surface of the solder that utilize to apply, but the contingent displacement of upper glass when leaving production well and can prevent that when gases are heated, they expand.
When only containing an edge band frame, described solder is in the outside of described edge band frame, when containing a plurality of edge band frame, described solder is in centre or centre and the outside of described edge band frame, described edge band frame is when the upper surface of the middle sheet glass of the convex glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
When only containing an edge band frame, the periphery of preferred described lower-glass contains an edge band frame, the periphery edge of edge band frame and described lower-glass has the space of 5mm~10mm, be used for being coated with described solder, described edge band frame is when the upper surface of the middle sheet glass of the convex glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
When upper glass and lower-glass respectively contain an edge band frame, the shape of two edge band frames and size or identical or different, it is identical to be preferably shape, vary in size, at this moment, little edge band frame is included in the large edge band frame, described edge band frame is when the upper surface of the middle sheet glass of the convex glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
Further, the edge band frame of described lower-glass is Duoed one than the edge band frame of described upper glass, be that described upper glass contains an edge band frame at least, described lower-glass contains two edge band frames at least, the edge band frame of described upper glass is inserted in the middle of the edge band frame of described lower-glass, the edge band frame of described upper lower-glass is entrenched togather mutually, low dead level is carried out labyrinth seal, described edge band frame is when the upper surface of the middle sheet glass of the convex glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
The introducing of edge band frame not only can limit solder and dissolve and randomly flow, make edge sealing neatly good-looking afterwards, and play good supporting role, make solder keep certain thickness, reinforced seal effect, the more important thing is that its Heating temperature is high, with upper lower-glass more reliable bonding is arranged, surface irregularity, have more firmly with solder and to be combined, thereby improve resistance to air loss and the reliability of low latitude glass.
Adopt the edge band frame, can be easy to utilize low melting point metal or alloy to realize the solder bonding metal of low latitude glass, because the selectable scope of brazing temperature is very large, so not only can wholely heat glass, reduce the cost of process furnace and simplify production technique, and can decrease edge sealing temperature, shorten heat-up time, thereby reduce production costs, enhance productivity, the more important thing is to guarantee tempering or the semi-tempered glass phenomenon of in heat-processed, can not annealing.
Described edge band frame is made by the mode of squeezing, etching or printing, and described edge band frame comprises fin and groove, the preferred fin that adopts the printing cryogenic glass powder to make.
Described squeezing mode is to pack sheet glass into internal surface with in depression or the mold cavity of protruding lines, after pyroprocessing makes glass softening, sheet glass is exerted pressure, and forms fin and groove at the periphery of sheet glass.
Described etching mode is known prior art, utilizes method for printing screen that acid-proof ink is printed on sheet glass and does not need etched place, will not have the acid-proof ink place to erode away groove on the sheet glass with corrosive acids such as hydrofluoric acid.
Described mode of printing is the method that adopts silk screen printing or mould printing or printer, cryogenic glass powder is imprinted on forms the fin that is raised in surface of plate glass on the sheet glass.
When described edge band frame adopts the printing cryogenic glass powder to prepare, can be one-step print, also can be repeatedly to print.
Make the solder that its melt temperature of cryogenic glass powder of edge band frame is used far above edge sealing, not only low price, performance are good, and with glass better bonding strength are arranged; After the edge band frame of upper lower-glass is mutually chimeric, not only reduced the edge sealing solder consumption, reduced the requirement to the edge sealing solder, and increased air retaining wall thickness, improved the sealing strength of upper lower-glass, the more important thing is to solve the sealing problem that the buckling deformation that produces because of glass brings in toughening process, thereby improve the qualification rate of product.
When preparation be tempering low latitude glass, the problem of annealing because welding temperature is too high when solving tempering low latitude glazing gasket can adopt low melting point metal or solder.
Described low melting point metal or solder can be tin or tin alloy, zinc or zinc alloy, aluminum or aluminum alloy, magnesium or magnesium alloy etc.
The present invention also provides a kind of convex surface low latitude glass, it comprises: upper glass, lower-glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, described upper glass and described lower-glass are convex glasses, and convex surface toward the outer side.
The preparation method of the convex surface low latitude glass of described low dead level with a sealing is as follows:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove;
The 3rd step evenly was coated with solder with two blocks of glass of second step acquisition or the face of weld periphery of a glass, leaves several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, and sent in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of convex surface low latitude glass, it comprises: upper glass, lower-glass and sheet glass, described sheet glass is clipped between described upper glass and the described lower-glass, described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass, the periphery of described upper glass, described lower-glass and described sheet glass welds together by solder, described upper glass and described lower-glass are convex glasses, and convex surface toward the outer side;
The preparation method of the convex surface low latitude glass of described low dead level with two sealings is as follows:
The first step according to the shape of the convex surface low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove;
The 3rd step, two blocks of glass or the face of weld periphery of a glass and the even coating of the face of weld periphery solder of remaining one flat plate glass with the second step acquisition, leave several production wells on the solder, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together three blocks of glass, the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of preparation method with convex surface low latitude glass of a low dead level, and it comprises:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove;
The 3rd step evenly was coated with solder with two blocks of glass of second step acquisition or the face of weld periphery of a glass, leaves several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, and sent in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of preparation method with convex surface low latitude glass of two low dead levels, and it comprises:
The first step according to the shape of the convex surface low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove;
The 3rd step, two blocks of glass or the face of weld periphery of a glass and the even coating of the face of weld periphery solder of remaining one flat plate glass with the second step acquisition, leave several production wells on the solder, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together three blocks of glass, the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of convex surface tempering low latitude glass, it comprises: the upper glass of tempering, the lower-glass of tempering, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, described upper glass and described lower-glass are convex glasses, and convex surface toward the outer side;
The preparation method of the convex surface tempering low latitude glass of described low dead level with a sealing is as follows:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing;
The 3rd step, two blocks of glass of second step acquisition or the face of weld periphery of a glass evenly are coated with solder, leave several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The present invention also provides a kind of convex surface tempering low latitude glass, it comprises: the sheet glass of the upper glass of tempering, the lower-glass of tempering and tempering, described sheet glass is clipped between described upper glass and the described lower-glass, described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass, the periphery of described upper glass, described lower-glass and described sheet glass welds together by solder, described upper glass and described lower-glass are convex glasses, and convex surface toward the outer side;
The preparation method of the convex surface tempering low latitude glass of described low dead level with two sealings is as follows:
The first step according to the shape of the convex surface low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing wherein pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing;
The 3rd step, two blocks of glass or the face of weld periphery of a glass and the even coating of the face of weld periphery solder of remaining one flat plate glass with the second step acquisition, leave several production wells on the solder, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower glass, middle sheet glass integral body are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together three blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The preparation method that the present invention has also offered a kind of convex surface tempering low latitude glass with a low dead level is as follows:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing;
The 3rd step, two blocks of glass of second step acquisition or the face of weld periphery of a glass evenly are coated with solder, leave several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The present invention also provides the preparation method of the convex surface tempering low latitude glass with two low dead levels as follows:
The first step according to the shape of the convex surface low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing wherein pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing;
The 3rd step, two blocks of glass or the face of weld periphery of a glass and the even coating of the face of weld periphery solder of remaining one flat plate glass with the second step acquisition, leave several production wells on the solder, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that upper and lower glass and middle sheet glass peripheral position are carried out local heating, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together three blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The present invention also provides a kind of dull and stereotyped low latitude glass, it comprises, upper and lower glass, described upper and lower glass is sheet glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, have in the described low dead level to be the upholder that dot matrix is arranged, have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass.
The height of described edge band frame is preferably 0.1~10mm, 0.1~1mm more preferably, and width is preferably 0.2~5mm, more preferably 1.0~2.0mm.
Several production wells can be left on the described edge band frame, after described solder fusing, described production well can be sealed.
When only containing an edge band frame, described solder is in the outside of described edge band frame, when containing a plurality of edge band frame, described solder is in centre or centre and the outside of described edge band frame, described edge band frame is when the upper surface of the middle sheet glass of the sheet glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
When only containing an edge band frame, the periphery of preferred described lower-glass contains an edge band frame, the periphery edge of edge band frame and described lower-glass has the space of 5mm~10mm, be used for being coated with described solder, described edge band frame is when the upper surface of the middle sheet glass of the sheet glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
When upper glass and lower-glass respectively contain an edge band frame, the shape of two edge band frames and size or identical or different, it is identical to be preferably shape, vary in size, at this moment, little edge band frame is included in the large edge band frame, described edge band frame is when the upper surface of the middle sheet glass of the sheet glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
Further, the edge band frame of described lower-glass is Duoed one than the edge band frame of described upper glass, be that described upper glass contains an edge band frame at least, described lower-glass contains two edge band frames at least, the edge band frame of described upper glass is inserted in the middle of the edge band frame of described lower-glass, the edge band frame of described upper lower-glass is entrenched togather mutually, low dead level is carried out labyrinth seal, described edge band frame is when the upper surface of the middle sheet glass of the sheet glass with two low dead levels, identical with described lower-glass, when the lower surface of described sheet glass, identical with described upper glass.
Described edge band frame is made by the mode of squeezing, etching or printing, and described edge band frame comprises fin and groove, and the preferred printing cryogenic glass powder that adopts is made.
Described squeezing mode is to pack sheet glass into internal surface with in depression or the mold cavity of protruding lines, after pyroprocessing makes glass softening, sheet glass is exerted pressure, and forms fin and groove at the periphery of sheet glass.
Described etching mode is known prior art, utilizes method for printing screen that acid-proof ink is printed on sheet glass and does not need etched place, will not have the acid-proof ink place to erode away groove on the sheet glass with corrosive acids such as hydrofluoric acid.
Described mode of printing is the method that adopts silk screen printing or mould printing or printer, cryogenic glass powder is imprinted on forms the fin that is raised in surface of plate glass on the sheet glass.
When described edge band frame adopts the printing cryogenic glass powder to prepare, can be one-step print, also can be repeatedly to print.
Described dull and stereotyped low latitude glass can also comprise one flat plate glass, and described sheet glass is clipped between described upper glass and the described lower-glass, and described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass.
Described dull and stereotyped low latitude glass may further include polylith sheet glass, thereby comprises the low dead level of a plurality of sealings.
The formation of the dull and stereotyped low latitude of described single low dead level glass can adopt single stage method to form, and described single stage method comprises the steps:
With the even coating solder of one in the upper and lower glass or two face of weld periphery, evenly leave several grooves that pass through the eutectic welding strip or slit on the solder as production well; Also can not reserve pore, the passage that discharge as gas between glass in the formed space, rough surface of the solder that utilize to apply, but the contingent displacement of upper glass when leaving production well and can prevent that when gases are heated, they expand; Upper and lower glass consistency from top to bottom is stacked together, sends in the high temperature edge sealing stove; Heating rises to more than the melt temperature of solder the interior temperature of stove, reaches the edge sealing temperature, and production well disappears; Stopped heating reduces furnace temperature to room temperature, and described solder welds together upper and lower glass is bubble-tight, thereby obtains needed dull and stereotyped low latitude glass.
It is as follows that the single stage method of described two low dead levels forms step:
The periphery of upper glass, lower-glass and middle sheet glass face of weld evenly is coated with solder, leaves several production wells on the solder, and three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove; Heating rises to more than the melt temperature of solder temperature, reaches the edge sealing temperature, and production well disappears, stopped heating, with the stove cooling, and solder hermetic welds together three blocks of glass, opens fire door and obtains required dull and stereotyped low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
When preparation be toughened glass the time, preferentially select low melting point metal or solder, to select lower edge sealing temperature.
When the preparation be toughened glass the time, the problem of annealing because welding temperature is too high, high temperature edge sealing stove can have basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or adopt the mode of circulating air heating, with 280~320 ℃ of high temperature edge sealing furnace interior and glass heats to basal temperatures; The modes such as recycling resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating are that local heating is carried out in the edge sealing position to the periphery of glass, reach the purpose that at short notice solder is heated to melting.
In described low dead level upholder can be set, upholder is resisted normal atmosphere jointly with glass.
The material of above support is metal, pottery, glass or plastics, is preferably low temperature glass.
The above support minimum unit can be that the dot matrix of equilateral triangle is arranged, and the leg-of-mutton length of side is about 30~300mm, is preferably 50~150mm; Upholder is strip, its length is 0.3~5.0 mm, be preferably 0.5~2.0 mm, width is 0.1~2.0mm, be preferably 0.2~1.0mm, be 0.1~10.0mm highly, be preferably 0.2~3.0mm, the height of upholder be higher than the edge band frame height 0.1~2.0mm, be preferably 0.1~0.5mm; Upholder also can be for cylindric, its diameter is 0.1~3.0mm, be preferably 0.3~2.0mm, be 0.1~5.0 mm highly, be preferably 0.5~3.0mm, two blocks of glass closed sheet rear support thing position spatial altitude 0.0~0.3 mm, are preferably 0.1~0.2mm about the height of upholder was higher than.
The material of described upper and lower glass can be simple glass or toughened glass or semi-tempered glass or low emissivity glass or wire glass or rolled glass or hot melt glass, or the combination of above any two or three kinds of glass, more preferably toughened glass, semi-tempered glass and low emissivity glass.
The shape and size of described low latitude glass determine that by the purposes of low latitude glass satisfying under the prerequisite of service requirements, its shape is preferably square or circular.
Described solder comprises low temperature glass solder and low melting point metal or solder, and described solder is coated on one or two face of weld periphery and the face of weld periphery of described sheet glass of upper and lower glass at least.
Described solder directly contacts with upper and lower glassy phase, perhaps contacts with upper and lower glass and the sheet glass that is clipped between the upper lower-glass.
The present invention also provides a kind of dull and stereotyped low latitude glass with a low dead level, it comprises: upper glass, lower-glass, described upper and lower glass is sheet glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, have in the described low dead level to be the upholder that dot matrix is arranged, have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass;
The preparation method of the dull and stereotyped low latitude glass of described low dead level with a sealing is as follows:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, guarantee upper and lower glass alignment after, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of dull and stereotyped low latitude glass with two low dead levels, it comprises: upper glass, lower-glass and sheet glass, on described, lower-glass is sheet glass, described sheet glass is clipped between described upper glass and the described lower-glass, described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass, just all have in the described low dead level and be the upholder that dot matrix is arranged, the periphery of described upper glass and described lower-glass welds together by solder, has at least the periphery of a glass to contain at least an edge band frame in described two low dead levels;
The preparation method of the dull and stereotyped low latitude glass of described low dead level with two sealings is as follows:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, at least two in the glass after three processing are utilized printing technology to prepare edge band frame and upholder, if at three edge band frames that all prepare on glass, after guaranteeing upper and lower glass alignment, between the edge band frame of sheet glass, the edge band frame of middle sheet glass can be embedded between the edge band frame of lower-glass in the middle of the edge band frame of upper glass can be embedded in;
The 3rd step, the solder of packing between the edge band frame of the glass that second step is obtained, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together three blocks of glass, the fire door of opening high temperature edge sealing stove obtains required low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of preparation method with dull and stereotyped low latitude glass of a low dead level, and it comprises:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, guarantee upper and lower glass alignment after, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of preparation method with dull and stereotyped low latitude glass of two low dead levels, and it comprises:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, at least two in the glass after three processing are utilized printing technology to prepare edge band frame and upholder, if at three edge band frames that all prepare on glass, after guaranteeing upper and lower glass alignment, between the edge band frame of sheet glass, the edge band frame of middle sheet glass can be embedded between the edge band frame of lower-glass in the middle of the edge band frame of upper glass can be embedded in;
The 3rd step, the solder of packing between the edge band frame of the glass that second step is obtained, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together three blocks of glass, the fire door of opening high temperature edge sealing stove obtains required low latitude glass.
Described edge sealing temperature is preferably 150~550 ℃, further is preferably 290~350 ℃ when adopting low melting point metal or solder; When adopting low temperature glass solder, further be preferably 380~470 ℃.
The present invention also provides a kind of dull and stereotyped tempering low latitude glass with a low dead level, it comprises: the upper glass of tempering, the lower-glass of tempering, described upper and lower glass is sheet glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, have in the described low dead level to be the upholder that dot matrix is arranged, have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass;
The preparation method of the dull and stereotyped tempering low latitude glass of described low dead level with a sealing is as follows:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, guarantee upper and lower glass alignment after, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass; And two blocks of glass are sent into carry out tempering in the annealing furnace and process;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt the modes such as resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The present invention also provides a kind of dull and stereotyped tempering low latitude glass with two low dead levels, and it comprises:
The sheet glass of the upper glass of tempering, the lower-glass of tempering and tempering, described upper and lower glass is sheet glass, described sheet glass is clipped between described upper glass and the described lower-glass, described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass, the periphery of described upper glass and described lower-glass welds together by solder, has at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass;
The preparation method of the dull and stereotyped tempering low latitude glass of described low dead level with two sealings is as follows:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, at least two in the glass after three processing are utilized printing technology to prepare edge band frame and upholder, if at three edge band frames that all prepare on glass, after guaranteeing upper and lower glass alignment, between the edge band frame of sheet glass, the edge band frame of middle sheet glass can be embedded between the edge band frame of lower-glass in the middle of the edge band frame of upper glass can be embedded in; And will at least two blocks upper and lower glass send into and carry out tempering in the annealing furnace and process;
The 3rd step, the solder of packing between the edge band frame of the glass that second step is obtained, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
Described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt the modes such as resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that upper and lower glass, middle sheet glass peripheral position are carried out local heating, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together three blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped tempering low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The present invention also provides a kind of preparation method with dull and stereotyped tempering low latitude glass of a low dead level, and it comprises:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, guarantee upper and lower glass alignment after, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass; And two blocks of glass are sent into carry out tempering in the annealing furnace and process;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt the modes such as resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
The present invention also provides a kind of preparation method of dull and stereotyped tempering low latitude glass of the low dead level with two sealings, and it comprises:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and three blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, at least two in the glass after three processing are utilized printing technology to prepare edge band frame and upholder, if at three edge band frames that all prepare on glass, after guaranteeing upper and lower glass alignment, between the edge band frame of sheet glass, the edge band frame of middle sheet glass can be embedded between the edge band frame of lower-glass in the middle of the edge band frame of upper glass can be embedded in; And will at least two blocks upper and lower glass send into and carry out tempering in the annealing furnace and process;
The 3rd step, the solder of packing between the edge band frame of the glass that second step is obtained, and described three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
Described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt the modes such as resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that upper and lower glass, middle sheet glass peripheral position are carried out local heating, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together three blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped tempering low latitude glass.
The scope of described basic Heating temperature is preferably 280~320 ℃, and the scope of melt temperature is preferably 380~470 ℃.
Below adopt embodiment and accompanying drawing to describe embodiments of the present invention in detail, how the utilisation technology means solve technical problem to the present invention whereby, and the implementation procedure of reaching technique effect can fully understand and implements according to this.
Embodiment 1: referring to Fig. 1, low latitude glass is comprised of upper convex glass 1 and lower convex glass 2, and the periphery of two blocks of glass welds together by low temperature glass solder 3, and is middle for hanging down dead level.Its making method is as follows: at first according to the shape of made low latitude glass and two blocks of sheet glass of size cutting desired size, and carry out edging, chamfering, cleaning, drying; Secondly two blocks of glass are packed into mould, be placed in the bending furnace, be warming up to softening temperature 550-750 ℃ of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove; Periphery with two blocks of glass or a glass evenly is coated with low temperature glass solder again, evenly leaves several production wells on the low temperature glass solder, and two glass consistencies from top to bottom are stacked together, and sends in the high temperature edge sealing stove; Be warming up to the melt temperature of low temperature glass solder more than 450 ℃, production well disappears, stopped heating, with the stove cooling, and low temperature glass solder hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Innovative point of the present invention is: low latitude glass utilizes the convex shape of glass to resist normal atmosphere, makes two blocks of glass can not press together, keep low dead level between two glass, has saved the very large upholder of manufacture difficulty; The mode of employing automatic edge sealing in high temperature edge sealing stove has been simplified technological process, has lowered production cost, has shortened the production cycle, has been improved production efficiency; Do not had stopping of upholder, transparency and the visibility of low latitude glass are better; Do not had the conduction of upholder, the heat insulation and sound-proofing properties of low latitude glass is better; Convex configuration makes glass that higher ultimate compression strength and bending strength be arranged, and the resisting wind press capacity of low latitude glass is better; Convex configuration makes low dead level that larger space be arranged, and more can keep for a long time the life-span of low dummy status, low latitude glass longer, even lose the low latitude, its performance also is better than general double glazing.
Embodiment 2: referring to Fig. 1, one in two blocks of glass is low emissivity glass, and other all are same as embodiment 1.
Embodiment 3: referring to Fig. 1, two blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, its making method is as follows: at first according to the shape of made low latitude glass and one flat plate glass and low emissivity glass of size cutting desired size, and carry out edging, chamfering, clean, drying; Secondly two blocks of glass are respectively charged in two forming moulds, this forming mould has mold and bed die (being formpiston and former), glass clamp is between mold and bed die, and can exert pressure and make upper and lower mould closed, the forming mould that glass is housed is placed in the bending furnace, is warming up to 650 ℃ of the softening temperature of glass, rely on the pressure that puts on the forming mould to make the glass in the forming mould form convex surface, remove immediately the mold cold tempering of sector-style of going forward side by side, obtain tempering or semi-tempered glass; Periphery with two blocks of glass or a glass evenly is coated with low temperature glass solder again, evenly leave several production wells on the low temperature glass solder, and two glass consistencies from top to bottom are stacked together, to send in the high temperature edge sealing stove, high temperature edge sealing stove and accessory has basic heating system and local heating system; At first utilize basic heating system heating, after basal temperature rises to 300 ℃, recycling local heating system such as far infra-red heater are heated to melt temperature more than 450 ℃ with low temperature glass solder, production well disappears, the low temperature glass solder of melting with two glass cementations together, stopped heating, with stove cooling, low temperature glass solder hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Because tempering and semi-tempered glass have higher intensity, so under identical shape and size, the convex curvature of tempering or half tempered convex glass can be larger.Because utilize the upper and lower die pressure moulding of forming mould, so convex glass has more regular shape, and prevents the distortion in toughening process, so edge sealing is simpler, sealing property and intensity are also higher.Because high temperature edge sealing stove and accessory has basic heating system and local heating system, the temperature of glass edge is rapidly heated to welding temperature, and tempering or semi-tempered glass are under lower basal temperature, in the long period and higher local temperature, in short time phenomenon can not occur significantly to anneal, so can guarantee to obtain tempering or half tempered low latitude glass.
Embodiment 4: referring to Fig. 2, two blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, one on glassly also has an edge band frame therein, its making method is as follows: at first according to the shape of made low latitude glass and one flat plate glass and low emissivity glass of size cutting desired size, carry out edging, chamfering, clean, after the drying, a preferred lower-glass on glass utilizes printing technology that cryogenic glass powder cream is printed to the edge band frame therein, the width of edge band frame is 1.2mm, highly be 0.7mm, with the edge of glass the distance of 7mm arranged; Other all are same as embodiment 3.
The introducing of edge band frame not only can limit low temperature glass solder and dissolve and randomly flow, make edge sealing neatly good-looking afterwards, and play good supporting role, make low temperature glass solder keep certain thickness, reinforced seal effect, the more important thing is that its Heating temperature is high, with upper lower-glass more reliable bonding is arranged, surface irregularity, have more firmly with low temperature glass solder and to be combined, thereby improve resistance to air loss and the reliability of low latitude glass.In addition, the edge band frame also is the key that single stage method prepares low latitude glass.
Embodiment 5: referring to Fig. 3, two blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, on glassly all has an edge band frame at two, its making method is as follows: at first according to the shape of made low latitude glass and one flat plate glass and low emissivity glass of size cutting desired size, carry out edging, chamfering, clean, after the drying, two printing technologies of utilizing on glass cryogenic glass powder cream is printed to the edge band frame, wherein upper glass has an edge band frame, lower-glass has two edge band frames, the size of upper glass edge band frame is between two edge band frames of lower-glass, after upper lower-glass closed sheet, the edge band frame of upper glass can be embedded between two edge band frames of lower-glass; Secondly two blocks of glass are packed into mould, be placed in the bending furnace, be warming up to temperature 550-750 ℃ that glass softens, rely on the gravity of glass self to make glass form convex surface downwards, the edge band frame also is in softening molten state and glassy bond together, carry out immediately wind-cooling reinforcing, obtain tempering or semi-tempered glass; Again evenly be coated with full low temperature glass solder between two edge band frames with lower-glass, and two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, high temperature edge sealing stove and accessory has basic heating system and local heating system; At first utilize basic heating system heating, after basal temperature rises to 300 ℃, recycling local heating system such as far infra-red heater are heated to melt temperature more than 450 ℃ with the low temperature glass solder in the edge band frame, the edge band frame of upper glass embeds under action of gravitation between two edge band frames of lower-glass, the low temperature glass solder of melting with two glass cementations together, stopped heating, lower the temperature with stove, low temperature glass solder hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Make the low temperature glass solder that its melt temperature of cryogenic glass powder of edge band frame is used far above edge sealing, not only low price, performance are good, and with glass better bonding strength are arranged; After the edge band frame of upper lower-glass is mutually chimeric, not only reduced the edge sealing low temperature glass solder consumption, reduced the requirement to the edge sealing low temperature glass solder, and increased air retaining wall thickness, improved the sealing strength of upper lower-glass, the more important thing is to solve the sealing problem that the buckling deformation that produces because of glass brings in toughening process, thereby improve the qualification rate of product.
Embodiment 6: referring to Fig. 4, two blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, on glassly all has an edge band frame at two, its making method is as follows: at first according to the shape of made low latitude glass and one flat plate glass and low emissivity glass of size cutting desired size, carry out edging, chamfering, clean, after the drying, two printing technologies of utilizing on glass cryogenic glass powder cream is printed to the edge band frame, wherein upper glass has two edge band frames, lower-glass has three edge band frames, the size of upper glass edge band frame is between two edge band frames of lower-glass, after upper lower-glass closes sheet, the edge band frame of upper glass can be embedded between two edge band frames of lower-glass, and the width of each edge band frame is 1.5mm, highly be 0.7mm; And on lower-glass, print simultaneously upholder, upholder is that minimum unit is the dot matrix arrangement of equilateral triangle, and the leg-of-mutton length of side is 100mm, and upholder is cylindric, its diameter is 0.6mm, highly is 0.8mm that the height of upholder is higher than the height 0.1mm of edge band frame; Secondly two blocks of glass are sent into respectively annealing furnace, in the softening melting of the high temperature action lower seal edge strip frame of annealing furnace and glassy bond together, carry out immediately wind-cooling reinforcing, obtain having tempering or the semi-tempered glass of edge band frame; Again fill the brazing metal glass putty or spread tinfoil paper or the tin silk between three edge band frames with lower-glass, and two glass consistencies from top to bottom are stacked together and leave certain space of giving vent to anger, send in the high temperature edge sealing stove; It is above as 240 ℃ to be warming up to the melting temperature of metallic tin, and metallic tin will melt, and two edge band frames of upper glass embed under action of gravitation between three edge band frames of lower-glass, and the metallic tin of melting with two glass cementations together; Stopped heating, with stove cooling, brazing metal tin hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Adopt the edge band frame, can be easy to utilize low melting point metal or alloy to realize the solder bonding metal of low latitude glass, because the selectable scope of brazing temperature is very large, so not only can wholely heat glass, reduce the cost of process furnace and simplify production technique, and can decrease edge sealing temperature, shorten heat-up time, thereby reduce production costs, enhance productivity, the more important thing is to guarantee tempering or the semi-tempered glass phenomenon of in heat-processed, can not annealing.
Embodiment 7: referring to Fig. 5, two blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, on glassly all has an edge band frame at two, its making method is as follows: at first according to the shape of made low latitude glass and one flat plate glass and low emissivity glass of size cutting desired size, carry out edging, chamfering, clean, after the drying, two printing technologies of utilizing on glass cryogenic glass powder cream is printed to the edge band frame, wherein upper glass has an edge band frame, lower-glass has two edge band frames, the size of upper glass edge band frame is between two edge band frames of lower-glass, after upper lower-glass closed sheet, the edge band frame of upper glass can be embedded between two edge band frames of lower-glass; Secondly two blocks of glass are packed into mould, be placed in the bending furnace, be warming up to the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, the edge band frame also is in softening molten state and glassy bond together, carry out immediately wind-cooling reinforcing, obtain tempering or semi-tempered glass; Again evenly be coated with full low temperature glass solder between two edge band frames with lower-glass, and at upper or lower-glass employing low temperature glass solder printing upholder, upholder is that the dot matrix parallel with the edge band frame arranged, distance between 2 is 150mm, upholder is cylindric, its diameter is 1.2mm, two blocks of glass close sheet rear support thing position spatial altitude 0.1mm highly to be to be higher than 2.0mm, the height of upholder up and down; Two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, high temperature edge sealing stove and accessory has basic heating system and local heating system; At first utilize basic heating system heating, after basal temperature rises to 300 ℃ of the softening sintering temperatures of upholder, recycling local heating system such as far infra-red heater are heated to the low temperature glass solder in the edge band frame more than the melt temperature, the edge band frame of upper glass embeds under action of gravitation between two edge band frames of lower-glass, the low temperature glass solder of melting with two glass cementations together, upholder also with two glass sinterings up and down together, stopped heating, lower the temperature with stove, low temperature glass solder hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Upholder adopts low temperature glass solder to make, and lower sintering temperature is arranged, and makes it can sintering in the edge sealing process, and by means of its slightly high height, upper lower-glass can be bonded together reliably, thereby plays effective supporting role; The existing outward appearance that is similar to sheet glass of the curved surface that curvature is larger has again the intensity higher than sheet glass, thereby can greatly reduce to reduce the quantity of upholder, further improves the transparency of glass, heat insulation and sound-proofing properties.
Embodiment 8: referring to Fig. 6, two blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, on glassly all has an edge band frame at two, its making method is as follows: at first according to the shape of made low latitude glass and one flat plate glass and low emissivity glass of size cutting desired size, carry out edging, chamfering, clean, after the drying, two printing technologies of utilizing on glass cryogenic glass powder cream is printed to the edge band frame, wherein upper glass has two edge band frames, lower-glass has three edge band frames, the size of upper glass edge band frame is between two edge band frames of lower-glass, after upper lower-glass closes sheet, the edge band frame of upper glass can be embedded between two edge band frames of lower-glass, and the width of each edge band frame is 1.5mm, highly be 0.7mm; Secondly two blocks of glass are sent into respectively annealing furnace, in the softening melting of the high temperature action lower seal edge strip frame of annealing furnace and glassy bond together, carry out immediately wind-cooling reinforcing, obtain having tempering or the semi-tempered glass of edge band frame; Again fill the brazing metal glass putty or spread tinfoil paper between three edge band frames with lower-glass, and at the upper and lower low temperature glass solder printing upholder that adopts simultaneously on glass, upholder is that minimum unit is the dot matrix arrangement of equilateral triangle, the leg-of-mutton length of side is 120mm, upholder is strip, its length is that 2 mm, width are 0.60mm, highly are 0.5mm, and the upholder of upper lower-glass is orthogonal, and it is crosswise shape that upper lower-glass closes sheet rear support thing overlapping; Two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove; The melting temperature that is warming up to metallic tin is above such as 240 ℃, metallic tin melts, two edge band frames of upper glass embed under action of gravitation between three edge band frames of lower-glass, the metallic tin of melting with two glass cementations together, the upholder of upper lower-glass is in contact with one another, overlappingly be crosswise shape; Stopped heating, with stove cooling, brazing metal tin hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Upper lower-glass all has the strip upholder, the upholder vertical pile supports, upper lower-glass still is the some contact by upholder, and contact for line between upholder and the glass, increased contact area, reduced the tension stress of glass in support place, thus the quantity of upholder can be reduced, thus further improve the transparency of glass, heat insulation and sound-proofing properties.
Embodiment 9: referring to Fig. 7, low latitude glass is comprised of upper convex glass 1, middle sheet glass 8 and lower convex glass 2, and the periphery of per two blocks of glass welds together by low temperature glass solder, and the centre is two low dead levels.Its making method is as follows: at first according to the shape of made low latitude glass and three blocks of sheet glass of size cutting desired size, and carry out edging, chamfering, cleaning, drying; Secondly two blocks of glass are packed into mould, be placed in the bending furnace, be warming up to the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove; Periphery with three blocks of glass or two blocks of glass or middle sheet glass face of weld evenly is coated with low temperature glass solder again, evenly leaves several production wells on the low temperature glass solder, and three glass consistencies from top to bottom are stacked together, and sends in the high temperature edge sealing stove; Be warming up to the melt temperature of low temperature glass solder more than 450 ℃, production well disappears, stopped heating, with the stove cooling, and low temperature glass solder hermetic welds together two blocks of glass, opens fire door and obtains required low latitude glass.
Embodiment 10: referring to Fig. 8, three blocks of glass are toughened glass or semi-tempered glass, wherein one or low emissivity glass, on glassly all has an edge band frame at three, its making method is as follows: at first according to the shape of made low latitude glass and two blocks of sheet glass and low emissivity glass of size cutting desired size, carry out edging, chamfering, clean, after the drying, bonding surface at three blocks of glass utilizes printing technology that cryogenic glass powder cream is printed to the edge band frame, wherein upper glass has an edge band frame, the upper surface of intermediate glass has two edge band frame lower surfaces that an edge band frame is arranged, lower-glass has two edge band frames, the size of top edge band frame is between two following edge band frames, after upper, middle and lower glass closed sheet, top edge band frame can be embedded between two following edge band frames; Secondly will be up and down two blocks of glass pack into mould, be placed in the bending furnace, be warming up to the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, the edge band frame also is in softening molten state and glassy bond together, carry out immediately wind-cooling reinforcing, obtain tempering or semi-tempered glass with the edge band frame; Intermediate glass directly advances annealing furnace, obtains tempering or semi-tempered glass with the edge band frame; Again evenly be coated with full low temperature glass solder between two edge band frames with intermediate glass and lower-glass, and three glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, high temperature edge sealing stove and accessory has basic heating system and local heating system; At first utilize basic heating system heating, after basal temperature rises to 300 ℃, recycling local heating system such as far infra-red heater are heated to melt temperature more than 450 ℃ with the low temperature glass solder in the edge band frame, between two edge band frames below top edge band frame embeds under action of gravitation, the low temperature glass solder of melting with three glass cementations together, stopped heating, lower the temperature with stove, low temperature glass solder hermetic welds together three blocks of glass, opens fire door and obtains required low latitude glass.
This intellecture property of primary enforcement that all are above-mentioned is not set restriction this product innovation of other forms of enforcement and/or novel method.Those skilled in the art will utilize this important information, and foregoing is revised, to realize similar implementation status.But all modifications or transformation belong to the right of reservation based on product innovation of the present invention.
The above only is preferred embodiment of the present invention, is not to be the restriction of the present invention being made other form, and any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the equivalent embodiment of equivalent variations.But every technical solution of the present invention content that do not break away to any simple modification, equivalent variations and remodeling that above embodiment does, still belongs to the protection domain of technical solution of the present invention according to technical spirit of the present invention.

Claims (10)

1. convex surface low latitude glass, it is characterized in that comprising: upper glass, lower-glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, described upper glass and described lower-glass are convex glasses, and convex surface toward the outer side.
2. convex surface as claimed in claim 1 low latitude glass is characterized in that having at least in the described upper and lower glass periphery of a glass to contain at least an edge band frame.
3. convex surface as claimed in claim 1 or 2 low latitude glass, it is characterized in that described convex surface low latitude glass can also comprise one flat plate glass, described sheet glass is clipped between described upper glass and the described lower-glass, and described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass.
4. ,The preparation method of each described convex surface low latitude glass of claims 1 to 3 is characterized in that comprising:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, and be down to room temperature with stove;
The 3rd step evenly was coated with solder with two blocks of glass of second step acquisition or the face of weld periphery of a glass, leaves several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, and sent in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
5. such as the preparation method of each described convex surface low latitude glass of claims 1 to 3, it is characterized in that the preparation method is as follows when described convex surface low latitude glass is convex surface tempering low latitude glass:
The first step according to the shape of the convex surface low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, with the glass after two processing pack into mould, be placed in the bending furnace, be warming up to 550~750 ℃ of the softening temperature of glass, rely on the gravity of glass self to make glass form convex surface downwards, carry out subsequently wind-cooling reinforcing;
The 3rd step, two blocks of glass of second step acquisition or the face of weld periphery of a glass evenly are coated with solder, leave several production wells on the solder, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt mode such as the nichrome wire of resistive heating, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, the modes such as microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required convex surface low latitude glass.
6. dull and stereotyped low latitude glass, it is characterized in that comprising: upper and lower glass, described upper and lower glass is sheet glass, the periphery of described upper glass and described lower-glass welds together by solder, form the low dead level of a sealing between described upper glass and the described lower-glass, have in the described low dead level to be the upholder that dot matrix is arranged, have at least the periphery of a glass to contain at least an edge band frame in the described upper and lower glass.
7. dull and stereotyped low latitude as claimed in claim 6 glass, it is characterized in that described dull and stereotyped low latitude glass can also comprise one flat plate glass, described sheet glass is clipped between described upper glass and the described lower-glass, and described upper glass and described lower-glass form respectively the low dead level of two sealings with described sheet glass.
8. such as claim 6 or 7 described dull and stereotyped low latitude glass, it is characterized in that described edge band frame adopts the preparation of printing cryogenic glass powder.
9. the preparation method of each described dull and stereotyped low latitude glass of claim 6 to 8 is characterized in that comprising:
The first step according to the shape of the dull and stereotyped low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, guarantee upper and lower glass alignment after, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove;
The 4th step was warming up to described high temperature edge sealing stove more than the melt temperature of solder, reached the edge sealing temperature, production well disappears, stopped heating, with stove cooling, solder hermetic welds together two blocks of glass, the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
10. the preparation method of each described dull and stereotyped low latitude glass of claim 6 to 8 is characterized in that the preparation method is as follows when described low latitude glass is dull and stereotyped tempering low latitude glass:
The first step according to the shape of the low latitude glass of required making and two blocks of sheet glass of size cutting desired size, and is carried out edging, chamfering, cleans, drying treatment;
Second step, in the glass after two processing at least one utilizes printing technology to prepare edge band frame and upholder, if at two edge band frames that all prepare on glass, guarantee upper and lower glass alignment after, the edge band frame of upper glass can be embedded between the edge band frame of lower-glass; And two blocks of glass are sent into carry out tempering in the annealing furnace and process;
The 3rd step, the solder of packing between two blocks of glass that second step is obtained or the edge band frame of a glass, and described two glass consistencies from top to bottom are stacked together, send in the high temperature edge sealing stove, described high temperature edge sealing stove and accessory has basic heating system and local heating system, the basis heating system can adopt the mode of resistive heating such as nichrome wire, electrothermal tube, hot plate etc., or the mode that adopts circulating air to heat, the local heating system can adopt the modes such as resistive heating, infrared heating, LASER HEATING, Electromagnetic Heating, microwave heating;
The 4th step, adopt first basic heating system that described high temperature edge sealing furnace interior and upper and lower bulk glass are heated to a basal temperature, adopt again the local heating system that local heating is carried out in upper and lower glass periphery position, reach the purpose that at short notice solder is heated to melting, thereby reach the edge sealing temperature, production well disappears, stopped heating, lower the temperature with stove, solder hermetic welds together two blocks of glass, and the fire door of opening high temperature edge sealing stove obtains required dull and stereotyped low latitude glass.
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CN113032911A (en) * 2021-04-16 2021-06-25 中国空气动力研究与发展中心超高速空气动力研究所 Aircraft heat-proof tile gap structure, design method and heat-proof tile
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Effective date of registration: 20191211

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Denomination of invention: Convex low altitude glass, flat low altitude glass and its preparation method

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