CN102921368B - Horizontal internal recycle agitating reactor - Google Patents

Horizontal internal recycle agitating reactor Download PDF

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Publication number
CN102921368B
CN102921368B CN201210493027.XA CN201210493027A CN102921368B CN 102921368 B CN102921368 B CN 102921368B CN 201210493027 A CN201210493027 A CN 201210493027A CN 102921368 B CN102921368 B CN 102921368B
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reactor
horizontal internal
baffle plate
guide shell
diameter
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CN201210493027.XA
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CN102921368A (en
Inventor
沈春银
李瑞秋
张立忠
戴干策
赵玲
吕林昌
叶新国
奚桢浩
蔡惠斌
陈宝林
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NINGXIA BAOTA PETROCHEMICAL GROUP DESIGN INSTITUTE (CO LTD)
NINGXIA BAOTA PETROCHEMICAL GROUP CO Ltd
East China University of Science and Technology
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NINGXIA BAOTA PETROCHEMICAL GROUP DESIGN INSTITUTE (CO LTD)
NINGXIA BAOTA PETROCHEMICAL GROUP CO Ltd
East China University of Science and Technology
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Application filed by NINGXIA BAOTA PETROCHEMICAL GROUP DESIGN INSTITUTE (CO LTD), NINGXIA BAOTA PETROCHEMICAL GROUP CO Ltd, East China University of Science and Technology filed Critical NINGXIA BAOTA PETROCHEMICAL GROUP DESIGN INSTITUTE (CO LTD)
Priority to CN201210493027.XA priority Critical patent/CN102921368B/en
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Abstract

The invention relates to a horizontal internal recycle agitating reactor comprising a reactor shell, a flow guide cylinder mounted in the reactor shell, an agitating device with an agitating paddle, and an end cover end socket. The horizontal internal recycle agitating reactor is characterized in that the inner wall of the flow guide cylinder of a diameter-changing section of the reactor is provided with a baffle with a gradually-changed width. According to the horizontal internal recycle agitating reactor, a guide baffle with the diameter which is changed according to the cross section is mounted at a material inlet of the horizontal internal recycle agitating reactor according to the property requirements of flow mixing and dispersing of a reaction system, and is used for enhancing the cutting dispersion capability of a tail end material of circulating fluid and a newly-fed material; the fluid is guided to generate the axial circulating flow; and finally, the materials are rapidly and uniformly mixed, material distribution and mass transfer conditions needed by a reaction are met, and the quality of products is guaranteed.

Description

Horizontal internal circulating stirred reactor
Technical field
The present invention relates to a kind of Horizontal internal circulating stirred reactor.
Background technology
The structure of mechanical stirring kettle generally includes stirred tank structure and baffle arrangement.Any stationary parts being placed in outside impeller shaft all forms baffle plate.Thereby baffle plate can divide two classes: wherein modal baffle plate pattern is that positioned vertical is wall baffle plate in the member of wall; Another kind of is special baffle plate, and its shape, position are different, and as bottom baffle, surperficial baffle plate etc., heat exchanger tube and feed pipe are the inner members that a common class plays baffle effect.The basic role of baffle plate is to make liquid in rotation motion change into flip vertical, elimination whirlpool; Improve effective utilization of the power that applies simultaneously.Baffle plate has limited the tangential velocity of liquid, has increased axially and radial velocity component, and its clean effect is to make impeller discharge currents have wider mobile radius; Flow more " rule ", power can be predicted preferably, and dispersion and mobile immixture are sheared in strengthening.
Chinese patent CN 2565537Y has designed a kind of stirred reactor with line of rabbet joint baffle plate, and this stirred reactor comprises, container, is placed in the agitating device at container middle part and is vertically set on the baffle plate on container inner wall.It is characterized in that offering on addressed baffle plate the line of rabbet joint one or more line of rabbet joint paralleling with the plumb line of baffle plate, the width of its line of rabbet joint can equate, also can be unequal; Its position is symmetry or asymmetrical.
Chinese patent CN 102068955 A disclose a kind of flocculation reactor with special-shaped spoiler, the baffle plate of various cross sectional shapes being installed and being had certain thickness requirement is set at this reactor wall, and this baffle plate and reactor wall are smoothly connected, in order to improve flocculating effect and to avoid it to produce failure by shear effect to floc sedimentation.The feature of this patent is to avoid producing shear action.
Chinese patent CN 102302908 A have invented the baffle plate in a kind of tank diameter, at reactor wall, install by some small front aprons to keep each other gapped state to be arranged the baffle group forming, every small front apron all adopt stainless steel also embedded reinforcing bar it is directly connected with still wall.
Chinese patent CN 201415128Y has invented a kind of stirred tank with spiral line-shaped curved baffles, spiral line-shaped curved baffles is fixedly welded on inner wall of kettle, spiral line-shaped curved baffles and stirred tank axial clamp angular region are 30 °-60 °, spiral line-shaped curved baffles quantity is 3-6 and is uniformly distributed, and the width of spiral line-shaped curved baffles is 0.05 ~ 0. 15 with the ratio of kettle internal diameter: 1.The defect that this technology exists is: convection cell shearing dispersibility a little less than.
In above-mentioned patented technology, baffle arrangement and characteristic size continually varying horizontal reactor structure are incompatible, even also can weaken the shear action of baffle plate, therefore, are not suitable for Horizontal internal circulating stirred reactor.
Summary of the invention
The object of the invention is to overcome the defect of above-mentioned prior art, the shearing dispersibility in a kind of efficient hardening axial flow flow pattern is provided, thereby reach the Horizontal internal circulating stirred reactor of circulation and the mixing of fresh material Quick uniform.
The present invention adopts following technical scheme to realize:
A kind of Horizontal internal circulating stirred reactor, comprise reactor shell, be arranged on guide shell in reactor shell, with agitating device and the end cap end socket of stirrer paddle, it is characterized in that: on the described guide shell inwall of reactor reducer, be provided with the baffle plate with gradual change width.
Described barrier width is 1/12 ~ 1/8 times of each lateral cross section diameter of guide shell reducer.
Described baffle plate is 4 ~ 8, is evenly arranged.
Described baffle plate is installed from wall, and it is from span from being 1/120 ~ 1/80 times of each lateral cross section diameter of guide shell reducer.
Described guide shell adopts 4-6 bar axial diversion plate whole or splicing to be uniformly distributed support.
Described stirrer paddle is that a kind of projected outline of mounted blade is that one jiao of fan-shaped, blade outer rim is carried out crooked novel blade with certain curvature radius, and described radius of curvature is 1/4 ~ 3/4 of described diameter of propeller blade D.
Described end cap end socket forms by flange, bent bodies with the containment member of axis hole.
Described bent bodies is formed by connecting by three sections of circular arc bodies, and the ratio of the inside diameter D of the radius of curvature of each circular arc body and described end cap end socket is: R1/D=0.406 ~ 0.813, R2/D=0.166 ~ 0.250, R3/D=0.144 ~ 0.194; Corresponding 1=12 ° ~ 40 ° of central angle value α, α 2=36 ° ~ 101 °, α 3=34 ° ~ 120 °.
The present invention is according to the mobile mixing of reaction system and the characteristic requirements of dispersion, guide shell internal face at the material inlet position of Horizontal internal circulating stirred reactor is installed the deflector apron changing according to cross-sectional diameter, changed tangentially rotatablely moving that the fluid that accelerates because of cross-sectional constriction produces under the impeller induction of High Rotation Speed, make the fluid turbulization of main body axial flow shear simultaneously, thereby strengthened circulation of fluid end materials and newly entered the shearing dispersibility of material, and it is mobile to guide fluid to produce axial circulation, finally make material quick, evenly mix, meeting the required material of reaction distributes and mass transfer condition, guaranteed the quality of product.
Accompanying drawing explanation
Fig. 1: the present invention is with the Horizontal internal circulating stirred reactor structural representation of width gradual change baffle plate;
Fig. 2: stirrer paddle structural representation;
Fig. 3: the baffle arrangement schematic diagram of gradual change width;
Fig. 4: end cap end enclosure structure schematic diagram.
The specific embodiment
Referring to Fig. 1, Fig. 2, Fig. 3 and Fig. 4, Horizontal internal circulating stirred reactor 1 of the present invention by reactor shell 2, be installed on guide shell 3 in described reactor shell 2, with the end cap end socket 6 of the change fluid flow direction of the agitating device of stirrer paddle 4, the baffle plate with gradual change width 5 that guide shell reducer is installed and reactor enclosure end of body, form.
The diameter of described reactor shell 2 each sections is different, and diameter continually varying is partly called reducer.
Described guide shell 3 is installed in described reactor shell 2, its with reactor shell 2 similar shapes variations, each section of center line is identical and have reducer.Guide shell 3 and with 4-6 bar can be whole can be also that the axial diversion plate 7 of splicing is uniformly distributed support.The inside and outside Space Cross Section of guide shell amasss identical, to guarantee that fluid has identical flow velocity at correspondence position.The effect of deflector is that guide shell is fixed to support, circulation of fluid is separated to guiding simultaneously and is mixed to improve.
The projected outline that described stirrer paddle 4 is a kind of mounted blades is that one jiao of fan-shaped, blade outer rim is carried out crooked novel blade with certain curvature radius, and described radius of curvature is 1/4 ~ 3/4 of described diameter of propeller blade D.This blade power input capability is strong, delivery flow is large, immiscible liquid-liquid diphase is had to good shearing and disperse, mix and circulate ability.
The baffle plate 5 of described gradual change width is installed on guide shell 5 inwalls of reactor reducer.Barrier width is 1/12 ~ 1/8 times of each lateral cross section diameter of guide shell reducer.The quantity of described baffle plate 8 is 4-8, is evenly arranged.Described baffle plate 8 is installed from wall, described baffle plate 5 from span from being 1/120 ~ 1/80 times of each lateral cross section diameter of guide shell reducer.
Described end cap end socket 6 forms by flange 8, bent bodies 9 with the containment member 10 of axis hole.Described bent bodies 9 is formed by connecting by three sections of circular arc bodies.The characteristic size of three sections of described circular arcs comprises central angle alpha 1, α 2, the α 3 of radius of curvature R 1, R2, R3 and each circular arc of each circular arc.The radius of curvature of each described circular arc with the ratio of the inside diameter D of described end cap end socket be: R1/D=0.406 ~ 0.813, R2/D=0.166 ~ 0.250, R3/D=0.144 ~ 0.194; Corresponding 1=12 ° ~ 40 ° of central angle value α, α 2=36 ° ~ 101 °, α 3=34 ° ~ 120 °.

Claims (2)

1. a Horizontal internal circulating stirred reactor, comprise reactor shell (2), be arranged on guide shell (3) in reactor shell (2), with agitating device and the end cap end socket (6) of stirrer paddle (4), it is characterized in that: on described guide shell (3) inwall of reactor reducer, be provided with the baffle plate (5) with gradual change width;
The quantity of described baffle plate (5) is 4~8, is evenly arranged, and its width is 1/12 ~ 1/8 times of each lateral cross section diameter of guide shell reducer, and baffle plate (5) is installed from wall, and it is from span from being 1/120 ~ 1/80 times of each lateral cross section diameter of guide shell reducer;
Described stirrer paddle is that a kind of projected outline of mounted blade is that one jiao of fan-shaped, blade outer rim is carried out crooked blade with certain curvature radius, and described radius of curvature is 1/4 ~ 3/4 of described blade (4) diameter D;
Described end cap end socket (6) forms by flange (8), bent bodies (9) with the containment member (10) of axis hole, wherein bent bodies (9) is formed by connecting by three sections of circular arc bodies, and the ratio of the inside diameter D of the radius of curvature of each circular arc body and described end cap end socket is: R1/D=0.406 ~ 0.813, R2/D=0.166 ~ 0.250, R3/D=0.144 ~ 0.194; Corresponding 1=12 ° ~ 40 ° of central angle value α, α 2=36 ° ~ 101 °, α 3=34 ° ~ 120 °.
2. according to Horizontal internal circulating stirred reactor claimed in claim 1, it is characterized in that: described guide shell (3) adopts 4-6 bar axial diversion plate (7) whole or splicing to be uniformly distributed support.
CN201210493027.XA 2012-11-28 2012-11-28 Horizontal internal recycle agitating reactor Active CN102921368B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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CN102921368B true CN102921368B (en) 2014-10-01

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Publication number Priority date Publication date Assignee Title
CN106732290A (en) * 2017-01-25 2017-05-31 临沂远博化工有限公司 A kind of reactor of continuous production nitromethane

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* Cited by examiner, † Cited by third party
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US7410611B2 (en) * 2001-01-31 2008-08-12 Dennis L. Salbilla In-line method and apparatus to prevent fouling of heat exchangers
JP2008115321A (en) * 2006-11-07 2008-05-22 Japan Polypropylene Corp Polypropylene random copolymer, composition containing the same and manufacturing method of injection molded body
CN201801474U (en) * 2010-05-19 2011-04-20 北京华陆博机械技术开发有限公司 Impinging steam type butyl rubber polymerization kettle
CN102068955A (en) * 2010-12-15 2011-05-25 天津大学 Flocculation reactor with special-shaped spoiler
CN102698697A (en) * 2012-06-25 2012-10-03 江门市长优实业有限公司 Reaction kettle device for preparing and coating spherical nickel hydroxide
CN203209044U (en) * 2012-11-28 2013-09-25 宁夏宝塔石化集团有限公司 Horizontal type internal circulation stirred reactor

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